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@MichaelMasson-w6n 4 сағат бұрын
Williams Nancy Williams Eric Brown Patricia
@usmanchem08 6 сағат бұрын
thank you for this great stuff.
@WallisDawn-h8s 17 сағат бұрын
Miller Shirley Lee Barbara Martin Susan
@JuliusWill-y4w 2 күн бұрын
Harris Richard Lewis Scott Harris Jennifer
@MeriHatun-g3y 3 күн бұрын
Miller Amy Davis Eric Davis Kevin
@JeffersonRae-e2i 3 күн бұрын
Davis Matthew Johnson Jeffrey Hall Thomas
@GuebjfEuevbc 3 күн бұрын
Thomas Thomas Robinson Angela Anderson Jose
@Ahlg1990 5 күн бұрын
Which software do you recommend for this?
@LisaRamos-y4s 8 күн бұрын
Young Deborah Robinson John Walker Christopher
@mohamedfadhali9917 10 күн бұрын
can you share the excel template
@TeriHamilton-o4e 16 күн бұрын
Robinson Sandra Davis Matthew Jackson Laura
@SusiePerez-d7o 17 күн бұрын
Davis Anna Gonzalez Melissa Allen Ruth
@AndreiHernandez-d7b Ай бұрын
Hi Michael, do you count with a configuration for capillary samples? If yes, what configuration and program are you using?
@doremihungary8051 Ай бұрын
Hi. may i ask why my percentage does not appear?
@mmahjoori Ай бұрын
hello, thank you for your explanation and video. For some samples, some people add internal standards in the powder. Why it is necessary?
@GBViloger Ай бұрын
How d= h2+k2+l2 i means is it any formula?
@user-oj9mm9qs3z Ай бұрын
This is a really good video on XRD. Extemely underrated.
@touhamikawther3240 Ай бұрын
Thank you for this video , i find it very clear however i can not find the solver tolerance button in my Highscore Plus version ( 3.0d)
@pinkblossomsky 2 ай бұрын
Why did you not include O and its atomic coordinates? What if I had 4e Wyckoff positions, should I enter 4 sets of coordinates? Thanks in advance!
@pinkblossomsky 2 ай бұрын
Wait, I think I just answered my question. You said it was 0 oxidation. I still need an answer for the second question, though. Please.
@AlbertoFidi 2 ай бұрын
Which can it be the best way to fill it with water solutions? In particular to avoid bubbles when you use a syringe.
@user-kt6il78l67 2 ай бұрын
This tube alignment method assumes that the incidence beam divergence slit and the detector's central pixel are almost perfectly aligned in one line with the goniometer's center. Are the correct and reproducable positions of the slit and detector guaranteed by manufacturer forever or they are adjusted by a user somehow before the tube alignment?
@mathampula9085 3 ай бұрын
where i can find formula for calculating penetration depth? not in program, just formula, please
@gordtvradio3465 3 ай бұрын
I am a postdoc. This was one of the best xrd lectures I’ve ever seen Great work
@user-xw6br6nz2w 3 ай бұрын
Thank you very much for the video. I'm a new user with Empyrean. Coudl you please explain why the omega changes with different samples (at 4'30'')?
@rahulroy2861 3 ай бұрын
Are these sample holders specific to the device used? For e.g we have rigaku Smartlab. I am not sure if it would be compatible with this
@IAMMDiffractionFacility 3 ай бұрын
My apologies, but I'm also not sure as I have not used a Smartlab.
@manishsahu3686 3 ай бұрын
Thank you very much
@user-wq8ov4vk6q 3 ай бұрын
Thank you for sharing this helpful video. I appreciate your time and effort.
@MelodicRiddles 3 ай бұрын
Hello sir.. My sample is BaZrS3 I am not able to find this in the list what should I do then?
@AnaMerC 3 ай бұрын
What version of highscore is it.? Some parameters that you show do not appear in the one I have, and I can´t find where to look at the version you have.
@souravnaskar370 Ай бұрын
Same problem I am using version 3.0.0 many options not there.
@davislosowan5333 3 ай бұрын
Great explanation! Thank you so much!
@maryamarshad4792 4 ай бұрын
What is miller indices valye for 22 i followed your video for my calculations
@marasini 4 ай бұрын
I need your assistance regarding analyzing the data, can I get your email
@mohammadazimipor5392 4 ай бұрын
Hello. Many thanks for such an instructive video. I wanted to know what is your software version?
@furqanahmad535 4 ай бұрын
how much minimum amount of sample required for XRD ?
@amirhosseinfereidouninasab9278 4 ай бұрын
Thanks a lot for this informative video
@sheebasharon1360 4 ай бұрын
Thank you very much for the video sir. Can you share the software download link please?
@zikriyakhan2583 4 ай бұрын
Again above and beyond expectations. Thank you
@zikriyakhan2583 4 ай бұрын
Perfect. Thank you very much for putting your time into making those videos...
@user-gz9ij1xx3y 4 ай бұрын
You could buy a parallel press from stores like Bühler and Struers who support devices/equipment for materialographic analysis. You can still use the glass, but this will help you to apply an even pressure.
@user-gz9ij1xx3y 4 ай бұрын
Thanks for this and all your other videos! All your videos are highly valueable. How do you mount this capillary after closing it? I do have different Capillary holders like Anton Paar TTK600 or manual adjusstable goniometer. Always, the thick ending, which you took off, is the mounting part. What is your solution and is it a commercial one?
@jeongshim1018 5 ай бұрын
Thank you for this video and also other videos, too. I have a question about isopropanol or acetone when you prepare powder samples on the zero background holder. I am worrying whether they may react with samples or not. How do I know that they are no problem with my samples?
@IAMMDiffractionFacility 4 ай бұрын
Honestly, I rarely ever use isopropanol or acetone when preparing samples. For the vast majority of samples, pressing on the powder with a glass slide doesn't create any problems. If I was worried about texture due to pressing on it with the slide, I would probably try the back-loaded sample holder. There are other tricks that we can use if we still get texture due to sample preparation. If you really want to use the isopropanol or acetone method, I'd say that you are probably pretty safe if your sample is inorganic. If your sample IS organic, you could try preparing your sample the wet way and the dry way. You can then perform XRD on both to see if you can detect any structural changes.
@jeongshim1018 4 ай бұрын
@@IAMMDiffractionFacility I appreciate your kind answer for my questions. I am learning many information from your KZbin video about XRD analysis.
@Sasy07 5 ай бұрын
Hello! Thank for the video, very interesting... Can someone please just tell me which is the minimum amount of samples (in mg or g) I need for a reliable analysis?
@NitinSharma-su1bj 5 ай бұрын
i"m trying to analyze my rock mimeral sample, my target is Mineral Composition and Phase identification . @iamm can you help me out .
@ThangPVan_ 5 ай бұрын
Hi sir, if I just put an amount of powder that just exceeds a little and use straightforward the sample holder (to avoid pressing or rubbing too much the back surface of a powder sample), would it cause the upward sample displacement effect?
@IAMMDiffractionFacility 4 ай бұрын
Unless you are using parallel beam optics, any deviation from the ideal sample height will cause your peaks to shift due to sample displacement. You are never going to get a perfect sample height though. My sample heights usually refine to something like 0.02-0.06 mm.
@ThangPVan_ 4 ай бұрын
Thanks for your reply@@IAMMDiffractionFacility
@user-ei1ui4lw9r 5 ай бұрын
Can you please share the details of the paper that describe the anisotropic lattice expansion in zirconium oxide
@nasmboyd1573 5 ай бұрын
Are you still active on this ?
@YAHBOY-my8gx 5 ай бұрын
Thank u very much for your best explanation but for me I use 1% Sm doped Zno XRD result my question if will find tow or one unique phase of ZnO and if have one phase ZnO how I will select the best of patterns please anser me sir
@ZZZZzzzcccc 5 ай бұрын
Hi, Sir. Could you post a guide to build a PONKCS phases to quantify the amorphous content in Highscore? Seems no such guide online.
@user-id2ts6sn9i 5 ай бұрын
thanks a lot, i have a doubt. When I accept a candidate, the score in the pattern list automatically changes, but in your video they stay the same as in the candidate lists, how is it?