Home Distillation of ethanol - Very simple

This video was made to help explain a simple distillation. Do not attempt to duplicate, re-create, or perform the same or similar experiments at home, as personal injury or property damage may result. The producer of this video is not responsible for any such injury or damage

[@andrewtreat7371]

It’s important to note that water and ethanol form an azeotrope lower than the bp of each constituent (water = 100 C, EtOH = 78.4 C, azeotrope = 78.2 C). This makes it impossible to attain an ethanol concentration above ~95.5% when distilling. Further purification is required if a higher concentration is desired- such as using molecular sieves, adding sodium to the distilled azeotropic ethanol/water mixture, or using the benzene pressure swing method for larger scales.

[@dannythompson1948]

Chemist? Thanks for the fact!

[@atrumluminarium]

Possible DIY upgrades to this process: A fractional distillation column before the condenser: same reason why ethanol evaporates easier, water condenses easier. A fractional distillation column is basically a tube with glass shards in it that enable the vapour to experience multiple evaporation-condensation cycles each time biasing the process more to ethanol. Salting out: you can add salt to the mixture and the ethanol separates and sits as a layer on top of the salt water. Extract that layer and then distill it to remove the salt. Obviously it will still contain some water but it will save you a couple of distillation cycles.

[@lautaromorales2903]

I recomend to put some sand inside the jar or something with rough edges to have some nucleation points. I think some broken glass can be used too. If you dont have those nucleation points the alcohol can be at a temperature higher than the boiling point and the water from the water bath be boiling. If that happens that meas that you are waisting the energy in boiling the water from the water bath instead of using if for boiling the ethanol, and furthermore there is the risk of an explosion ocurring from the superheated ethanol sponteanously boiling. When I was doing this kind of distillation with a bottle, the ethanol wasn't boiling, so i added some sand into the bottle and it suddently boiled. Some ethanol scaped and splayed me in the hand, but luckly nothing more happened.

[@mjwarlock]

thanks alot this should help me alot whilest saving up for a real distiller

[@Alex_Seth_23_]

Банку надо нагревать на песчаной подушке. Тогда будет толк. Так спирты практически не испаряются

[@sameeramansour9062]

تقصد وضع الرمل داخل الجره ام تحتها في الماء؟

[@malachite072]

where do you get the plastic tubing????

[@GenovefaGerhild]

avoid plastic

[@bubbu6933]

First I thought it was green hand sanitizer 🤣🤣🤣 then it clicked ki isopropanol is present in hand sanitizer, not ethanol 🤣🤣

[@EricPham-gr8pg]

Thanks

[@visix8910]

Why with Midori, use a low cost vodka or ever clear that contains more alcol

[@kirkstinson7316]

Because it's NOT for drinking. Steel lid and plastic? A still for drinking alcohol is stainless or copper ONLY! Don't poison yourself

[@tobiasleybold9023]

Everclear is maximally distilled alcohol, at an alcohol concentration of around 95%, ethanol forms an azeotrope with water, which means they’ll have a homogeneous boiling point

[@moviekittyclips]

@@tobiasleybold9023 in many states in the usa the everclear is only 75-90% due to legal stuff and could be distilled further

[@patrickmanasco8772]

@@tobiasleybold9023What if I’m just tryna reclaim everclesr that was used as a solvent n want all the liquid back? Then it shouldn’t matter right?

[@typerightseesight]

Gas station vodka lol. ftw

[@jeremy-ez6nd]

this vid was stuuuuuuupit