How to Purify by Recrystallization

[@NurdRage]

Why in Einstein's name does this have millions of views? It sucks. Seriously, i'm the guy who made it... and even i'll tell you; it SUCKS. If you want something actually COOL, watch me make glow sticks: kzbin.info/www/bejne/qnrXgIKmrq-Da80 or sodium metal: kzbin.info/www/bejne/eKSxoJx8n5iqotk or even a nuclear battery: kzbin.info/www/bejne/gXzHq5uGnrSkp8k Anything! But not this video.

[@EveryMistakeYouCanMake]

Hey boss, do you know how to recrystallize menthol crystals? I have a video I'm making that about meth, and the crystals I got in the mail today were liquefied. I froze them, it was a cloudy gummy mess. I melted them back and let them sit in a bowl to get to room temp naturally, but it all looks terrible (no crystals, just... I don't know, gross). Really need some help. Please respond as soon as you can. Thank you so much.

[@jonross377]

@@EveryMistakeYouCanMake What does menthol have to do with meth? Just curious. You probably would have gotten a reply if you had left out the meth part...

[@EveryMistakeYouCanMake]

@@jonross377 You are probably correct, lol. Looking back, my whole question looks suspicious. Alright, so meth, specifically the version known as "ice" looks very similar to menthol crystals. My channel on KZbin is dedicated to helping parents and children know everything about drugs. No scare tactics, just truth. In the first video I'm making, I need a substitute for meth because I don't want to actually go purchase meth. It's incredibly easy to get, but I don't want to put myself at risk anymore. Even just possession of the drug is a major felony. The script for that first video, for the actual show, is so powerful; the imagery needs to perfectly align with it. Thus, I need something that looks like meth and the menthol crystals that Amazon dropped me off yesterday, melted :(

[@jonross377]

@@EveryMistakeYouCanMake I just looked up meth crystals and menthol crystals and dang, they look EXACTLY the same.

[@EveryMistakeYouCanMake]

@@jonross377 Yep. The menthol shards are slightly skinnier and longer, but for the most part, that's what looks like. I hope the owner of this channel gets back to me. I need to get this done asap. I have no idea what I'm doing.

[@98JMA]

What we have are solubility tables, which tell us the solubility of our compound at different temperatures in different solvents. We look for a solvent where the compound has low solubility at room temperature (or colder) and high solubility at hotter temperatures. This is ideal, as the crystals will come out when the solvent cools from being heated, purifying them. This is the general idea of recrystallization.

[@NurdRage]

@myrdale I tried that but the purity just wasn't good enough to make phosphorescent powder.

[@AnyerPablo]

i want to ask if i want to make 100kg kclo3 what steps should i do?

[@Jend_docsellsontelegraam-f5f]

👆👆look up that handle, he ships swiftly, and he got shrooms, Dmt, lsd, mmda, psilocybin, adderall, morphine, edibles, fentanyl, cubensis, meth, gummies, SSRI, chocolate bars, he's got a lot.. 🍄 💊🍄🍫💯🔌

[@CannaPlant]

This is the first explanation of the process of recrystallization that makes 100% sense and answers all my questions. Thank you!

[@gregorteply9034]

I love him saying "product" all the time.

[@milotickz]

Of all the scientists on youtube, you NurdRage, are the BEST!!!

[@irxkep3349]

You can actually save the impure liquid that has been poured off and let it dry. This way you will have some pure and some impure product that can still be used in reactions that can tollerate impuritys

[@bonniejohnson5728]

They got spooked tbh

[@baguazhang2]

Thanks for the help. I'm purifying azides in different solvents and it's working well so far. I just added a bit too much solvent and need to evaporate some off.

[@sulkarnaink7160]

may I ask for a complete video with the ingredients needed and how to make it

[@love.88bdhjte]

can it be smoked like crystal?

[@Jack-r2v9b]

Yes

[@moonlight-yp1kx]

How is methcathinone made? please help

[@BoraDor-m1q]

Still interested?

[@markcamancho6248]

@@BoraDor-m1qI would love some help

[@BoraDor-m1q]

@@markcamancho6248 in what bro?

[@BoraDor-m1q]

@@markcamancho6248 still around bro?

[@NurdRage]

@personperson666 While it does improve the crystal growth somewhat, eventually you reach a limit where the size is dictated by other variables like size of the container, temperature, humidity, etc.etc.etc.

[@drahyden]

Recristalization, great technique. Thanks for positing this vids, you are really making a excellent service of inciting the love for chemistry on people.

[@bahaaamarat6603]

Wht is

[@Pipewing]

You make some great videos. I do wonder why you didn't heat the strontium nitrate just to speed evaporation. Where do you find solubility vs. temperature information? or is it something you just remember from doing so much?

[@NurdRage]

@tzermaan I'm actually trying to put together such a DVD myself. Once i have a few more videos, as well fix some mistakes and edit a few issues, i'll release such a DVD directly.

[@dalerockzsmith1510]

Can you rewash using just water?

[@spark893]

How do you know what solvents will be suitable for different starting products and weather they will require heat

[@ShirleyHathaway-hd8tu]

Anyone have a link to a video of how to use acetone to purify blow?

[@thecommonsenseconservative5576]

I wish! I've read though you have to use anhydrous acetone then dry slow with heat lamp

[@NurdRage]

@mafl25 yeah, but it's now chock full of impurities. After all, to make one portion purer the impurities have to go somewhere. Just save the discarded liquids and dry them. If you can find a use for them that isn't sensitive to impurities then go for it.

[@jamesslater529]

Soap making is my hobby and I want to use ash extracted lye to make soap but I don't want to go through the trouble of cleaning the impurities. Is this method the most cost effective way to get purified potassium hydroxide, from hard wood ashes or am I just better off buying my lye at a store. I'm a cheap skate, that's why I want to know.

[@Joe-fb4eg]

James Slater uLtrasonic cleaner and diluted or deionized water

[@Joe-fb4eg]

James Slater no soap at all added when cleaning said impurities

[@Joe-fb4eg]

James Slater no heat either

[@user-by6yc8yl7v]

I've done a similar process with acetone, Started with 1.5G and ended up with 430MG of pure product.

[@getmeoutofsanfrancisco9917]

What were you recrystallizing?

[@mobmob5944]

Loolol

[@johnkelly937]

😂

[@KristenHaass-fl9jk]

Acetone will take out the junk

[@paulobarcelos3630]

I run out of acetone

[@NurdRage]

@fedaikn the crystals are pure enough for the synthesis of phosphorescent powder. And you do get rid of most of the liquid, and thus of the impurities, when you decant off the liquid.

[@MARTELRA1983]

Chemistry is awesome, just like the narrator's voice of this video.

[@lyndafromcazw2303]

What is it used for or what did you make I'm curious I only caught this one video.

[@metalhead0jtk]

I have some Strontium Nitrate from an old road flare (I suspect it contains some sulfur too) and it doesn't seem to dissolve in water at all, blame the sulfur. How can I purify by crystallization with something that is hydrophobic and heat sensitive? Thank you

[@lotmom]

Is it possible to recrystallize red phosphorous?

[@lilshorty7945]

Lotmom BG li si 😀

[@J14e11s87u]

Hi thanks a lot; your videos are helping me to finish my thesis actually I´m recovering metallic manganese from spent batteries but I have some questions How long does it take to recistalize MnSO4 ? and How much do I have to boil the solucion up (in percentage)? I´ll be waiting your answer.

[@jonross377]

Are you still waiting?

[@planeiron241]

@@jonross377 I'm curious I think I will wait too, gotta run to the store hope I don't miss sumthin

[@DEATH_TO_TYRANTS]

😂​@@planeiron241

[@hyperbob101]

hehe i am following along with everything you do. right now i have lioke 5 glow sticks i made using your steps that i haven't even broken

[@reinerdursten8027]

You have to take in the recrystallization basically 20% of the water volume of the substance? Or is that depending on the solubility of the substance?

[@jerinsema6097]

Someone answer this shit !

[@Ori-lp2fm]

Try find something in the littature

[@fedaikn]

there is still liquid coating the crystals, even after the second purifying step. i think that one will not get rid of impurities unless one gets rid of the liquid phase. could you get rid of that by washing the crystals in a filter with some ethanol or isopropanol?

[@ambition9132]

Spoken like a true 2weaker. Lol JK jk

[@ThomasAndersonbsf]

ok I think I missed part of what I was looking for here, in that I expected FRACTIONAL recrystallization. but this is not very clear as to showing this process, where maybe a mixture of several salts (like sodium chloride and potassium chloride,) were used to show the two different salts in their stages due to their varying solubility rates, causing one to precipitate out before the other, and each stage a method of identifying each salt as well as the batch where the last of one was precipitated and first of the next salt began precipitating out. (like using a UV lamp to effect the compounds maybe so it might take different salts for good clean clear easy to tell differential color fluorescing to show the different salts)

[@Jend_docsellsontelegraam-f5f]

👆👆look up that handle, he ships swiftly, and he got shrooms, Dmt, lsd, mmda, psilocybin, adderall, morphine, edibles, fentanyl, cubensis, meth, gummies, SSRI, chocolate bars, he's got a lot.. 🍄 💊🍄🍫💯🔌

[@Jend_docsellsontelegraam-f5f]

👆👆look up that handle, he ships swiftly, and he got shrooms, Dmt, lsd, mmda, psilocybin, adderall, morphine, edibles, fentanyl, cubensis, meth, gummies, SSRI, chocolate bars, he's got a lot.. 🍄 💊🍄🍫💯🔌

[@ThomasAndersonbsf]

@vanessa jones sells what? sorry but you lost me. I was talking about the methods for identifying things and how to get them sorted by solubility reluctance like the temp for condensing various chemicals from vapor,

[@Nerflover10097]

Does it put the lotion on its skin?

[@JoeClouser]

Ist es gut in methylephedrin hydrochlorid machteren

[@Gilamunster777]

Being taught by Hulk Hogan about recrystallization..... Priceless lol.

[@rustybritches6747]

Yeah brother!

[@pena.3302]

Who Knew Terry Does Science stuff too.(Thats a Great lol.)

[@somebodysomething]

Look Brother ! I'm going show how to recryatalize

[@JamesAJ]

Am I the only one who's fascinated by this science here? Everyone else is disliking "cause Breaking Bad"...

[@mvrdamonxy7942]

ItsmeJamesAJ yea its really something.

[@deekay6902]

All I'm saying is 2 gases in Liquid form mixed with liquid pseudo and you are home

[@deekay6902]

It's up to you to find out what gases

[@StevenSchoolAlchemy]

This is perfect for me I've been working with copper nitrate and I plan to work with iron nitrate as well.

[@sammylopez7729]

I like the science behind that

[@nomitech7197]

Hi Nice video Can you explain Me How many chemicals need for made this And how can is possible to get these chemicals. .please explain me

[@chechebro1]

can i do this with mdma?

[@WilliamSussman]

Yep

[@SLIXICK]

Im curious could this method be use to extract Thc from plant matter and then crystallize it.

[@maggiep9007]

Most potheads just spray lighter fluid through plant matter, then smoke the crap that gets dissolved and shoved through. They call it "butane honey oil" if I recall.

[@Joker-f1u2g]

What is this used for. ?

[@bobbycoronasr1201]

I dropped 1 1/2 Oz's of work in a pyrex glass any tips on what to do next

[@habibt.5882]

Lmfaoooo 😂😂🤦🏻‍♂️

[@darkpigion]

Can the purification be made any more efficient than this? It seems like allot of product is wasted.

[@NurdRage]

MnO2 isn't soluble in water so it requires a chemical purification process. if i make ask, what do people use MnO2 for other than an h2o2 catalyst? if the use is interesting i might do a video on it.

[@themainstreamstereo]

when i did this the crystals turned back into the same white cloudy color. Does the Clarity of the crystals relate to their purity?

[@rock2b28]

I have a question that really want it to be solved as i cant find its solution. Can the slow evaporation recrystallization process be done normally under heating to make it evaporate faster?

[@ThomasAndersonbsf]

+ROCKET&SCIENCE EXPERIMENT he said he cant because the extra energy of the heat causes an effect that effects the solubility stablizing teh amount that will dissolve in differing temps, and my guess is that there is a temp where it will change but that will either be over boiling temp requiring a pressurized vessel or will cause the salt to thermally decompose, or take on atoms from the water. destroying your salt too.

[@666ppaaccoo]

Gente, cola na grade! Tô chegando agora, isso que está sendo purificado é Cloreto de potássio ou Salitre? Obrigado companheiros!

[@autisticghostdog8179]

pq ta comentando em português?

[@xtx7305]

How to make mitavitamin ???? Pliiiiiiiiz

[@TheCatapang]

is the nano nitrate also can be use in crystalizing met

[@deckondeadozodiaco]

Met de methanfetamina?

[@starshock01]

After heating, placing the heated solution in the beaker into a styrofoam or insulating container will yield larger crystals but will take longer to cool.

[@Hasn-Aml890]

التعليق،قبل عشر،سنوات،،،الله يعلم ميت عدل😲😳

[@استبرق96]

@@Hasn-Aml890 أي هسه لكيت كلشي

[@Hasn-Aml890]

@@استبرق96 زين إذا نجحتي،بالتجربه،ذكريني،بحصه،منه،هههههه

[@mohamedalfouqaha4899]

Is there anyone who can explain if this is a crystal dope or not.. and what are the materials used to manufacture it, please?

[@OmarOmar-sb1nm]

Nobody buys the recipe for free. If you want to have it, you have to pay and pay. I am ready

[@t88boost]

Just found a presentation for my sons 5th grade science class. Thanks for the video

[@TheBrunswicksfinest]

t88boost they use this with methamphetamines

[@maggiep9007]

We did this in 2nd grade. This is how you make rock candy. Just put a stick in it and you can grow a giant jagged lollipop.

[@simonhryhoruk1233]

@@TheBrunswicksfinestIs that where the crystal in crystal meth comes from?

[@artea1oo1]

is it possible to use the recrystallization method on pottasium nitrate and sulfur?

[@alekzanderkastrov1914]

Whoa there buddy :o

[@Sgt.Hartman]

do you know if aluminum acetate is dangerous at all?

[@Casual_laughter]

Just curious to see if you're still alive

[@Sgt.Hartman]

@@Casual_laughter Lmao I am. That was a LONG time ago I don't even remember why I asked this.

[@Casual_laughter]

@@Sgt.Hartman 🤣🤣

[@ChuicyProductions]

Would this work if you are trying to purify capsaicin?

[@aliacar5103]

hello good day, what are the materials needed for this crystal, exactly because I am a chemist, I want to try it

[@ressam2868]

Ülkenin üretime ihtiyacı var üretelim geliselim

[@LeslieLenchak]

Same here

[@BoraDor-m1q]

@@LeslieLenchak still interested? I can help you

[@nikola96uf]

Can i vacum filtrate and dy of vacum instead of dessicator bag?

[@wildfireman13]

This works for caffeine?

[@قاسمابوامير-س7ن]

Hello, can I learn how to make crystal shabu? May God bless you, my brother

[@donnawood3419]

Is this the recipe for methamphetamine?

[@BoraDor-m1q]

Nah, if your interested in it I can help you

[@AuliaRahman-oq6zr]

Kirimkan saya tertarik ​@@BoraDor-m1q

[@trainwreck3697]

How do you know that what crystallizes is actually your product? Is it possible for some impurities to crystallize before your product does?

[@NurdRage]

i was already planning a few more combustion videos (including kno3) but i've seen channels taken down because they showed that sort of thing. i guess we'll just have to see.

[@siamhossain6357]

How can I purify ketamine Crystal?

[@Psycotic.]

question if the contaminants can crystalise out before the chemical you want does cant you pour the solution out then crystalise that?

[@davidsscope]

"This guys got the knowledge, man. He's... he's the man. Few people have what this guy has. He's like a gold mine." Spyder Mike

[@mikeyinka]

Have you seen

[@NurdRage]

@ryan50ryan simply let it dry. But it will be chock full of impurities, and useless for making glow powder. If you have other uses that can tolerate the impurities then go for it, otherwise its best just to discard it.

[@hanvan1]

Co the cho minh bit từ A..Z nha nguyên liệu mua ở đâu

[@MarcusTheReverent]

how do you purify or extract ammonium nitrate from fertilizer?

[@chrisdavies3686]

Okay bin Ladin

[@feuerwerk1997hansl]

could you please tell me how much water i need for 100 gramms of bariumnitrat....and how can i find out how many water i need.....thanks

[@Mad_brown19]

What is the formula, Kleo?

[@nathanparcel]

Why is distilled water better than DI? I am very curious about this.

[@kraven713]

Tap water has a multitude of impurities. Minerals, random bacteria, yummy fluoride, ect. So distilled water won't add anything to the chemical you're trying to get junk out of. :)

[@nathanparcel]

Kovu Legar Exactly, so why would Deionized water be not as good for that application than distilled water? Thanks:)

[@joesilva8971]

+Nate Parcel Yeah, I wanted to know the same thing. I've read the opposite. Pity no useful reply has been forthcoming. Joe.

[@kraven713]

I imagine it's so you don't get added calcium, limestone, fluoride, chlorine, ect into whatever it is you're trying to purify. And while i really doubt there's much of any of these things in tap water, if you're doing something very precise or using exact measurements with sensitive lab equipment it'll effect your ending substance. There may be other reasons i'm not aware of, but this is what i imagine would be the strongest reason. I loose example is, the same reason why you don't want to drink river water or tap water and why we like to drink purified/bottled water.

[@nathanparcel]

Yea that's exactly the reason (15 months of lab work experience). But DI water is a "more pure" distilled water. So I'm questioning why a mid range pure water would do better in this application.

[@billytalentrocks345]

Will this method work for sodiumacetate trihydrate? Well, I maybe have to get rid of the trihydrate thing, making in nonhydrate (correct spelled?), but how do I do that?

[@ThomasAndersonbsf]

have you done a video on hydro-thermal synthesis? would be interesting but for video it would probably have to have a thick fused quartz chamber walled system to be able to see what is going on, which I am not sure could handle the chemical reaction of water at excessive temps trying to dissolve it like say it does for aluminum oxide for growing sapphire crystals :)

[@samdavies677]

Would this prossess work with cladestine made ketamine hcl

[@jestermelender8082]

Can you do this with silver fulminate i am scared of mixing because it might cause an explosion or murcury fulminate?

[@chitobubulubu4052]

Hey MY Name is chito i got a idea but a dont now what is for i just now that is for energy

[@flashplayerplugin11]

What is being used to filter it? That white cone shaped thing

[@TheChemicalGenius]

I have a question. If you synthesize Mercury (II) Fulminate and you get a powdery sort of yield, can you crystallize it by dissolving it in ethanol,and using the same methods as you demonstrate in the video? I understand that Fulminated Mercury's autoignition point is at 180 degrees Celsius. What should I do? I would really appreciate any sort of reply

[@BennettStevens22]

Do you snort it? What am I watching. This played after another video I was watching

[@owowwazwaz1617]

@@BennettStevens22 good question

Is there any place I can find a more specific crystalization procces for lysergic acids?

[@ایرانجدید]

How can I make methadone syrup?

[@NurdRage]

@renatadevin The sun?

[@jarheadwithm16]

Can you purify sodium acetate by recrystallization?

[@DhivyaPrasath]

After filtration also I'm getting same colour solution. So what can I do?

[@Bigshoots86]

Are you filtering down to .22um?

[@paulvigil6794]

Does CO2 make bigger crystals

[@Jend_docsellsontelegraam-f5f]

👆👆look up that handle, he ships swiftly, and he got shrooms, Dmt, lsd, mmda, psilocybin, adderall, morphine, edibles, fentanyl, cubensis, meth, gummies, SSRI, chocolate bars, he's got a lot.. 🍄 💊🍄🍫💯🔌...

[@blink182chase13]

So being tottaly serious, cai i use this to puify lye? cause i got the drano crap and i heard its not bery concerntrated. Please answer..any one.

[@PPRstudio]

Is it work with RO water?

[@Barskor1]

You can reclaim lost product it just takes work. you gather all the solution you poured off in the initial purification till you have enough to again filter and recrystallize. This is only cost or time effective when you do continuous or repeated operations of the same kind.

[@NurdRage]

actually you needed more water. the 1/5 thing only works for aluminum nitrate nonahydrate. for potassium nitrate you need 1/3 its weight in water.

[@coolliger]

Which method should be used to purify sodium nitrate?

[@cobrasniper555]

That would be something I'd like to do after the Army. I'm 18, and plan on going through college afterwards. I'm good with math and chemistry (organic as well). Any suggestions for classes or majors to take special interest in? Thanks

[@Spida-Jug]

Sheesh

[@dadme1493]

how can i make crystal ice ?

[@carlosperez4309]

How do you test when is good crystal meth with aseona.or bleach

[@maggiep9007]

The only way to know is to send it away to be tested. You can rinse it with acetone to wash some stuff away.

[@Hoangzane]

Đây là ma túy tổng hợp phải không

[@johnapplesmith5558]

Can you synthesize crystaline methamphetamine please? Nice vid

[@steadfast1984]

you can also use R/O water as long as the membranes and filters are high end.

[@Khodazmoon]

Where are you man? I've missed your videos

[@hadescorp1475]

Is that machine measuring? Boiling, Vibrating or what?

[@ssensasi660]

what's the material for the boss for methamphetamine

[@nikola96uf]

@NurdRage What means 90 % purity? For some tecnical chemicals like sulfuric acid are 90 % purity. I have technical grade H2SO4 and i did titration and it was 95 %. how then it is 90 % purity if it contains 95% H2SO4? Other is water. Does that inpurity is 10 % of that 5 % that contains water in this case?

[@cheloagain7228]

Can I smoke it or vape 🤔

[@samsuardy2440]

recipe info sir...

[@BoraDor-m1q]

I can give it to you

[@amjadali-ml2os]

purification of cobalt nitrate? ....please help sir