Lec-12 || Thermo Spray Ionization (TSI) || Evaporative & Soft ionization || HPLC Coupled TSI

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#MassSpectrometry
Lec-1 || Intro to Mass Spectrometry || Molecular ion peak || Basic principle || m/e value
• Lec-1 || Intro to Mass...
Lec-2 || Parts of Mass spectrometer | Instrumentation | Functions of different parts of spectrometer
• Lec-2 || Parts of Mass...
Lec-3 || Sample introduction in Mass Spectrometer || Nature of analyte || Type of sample
• Lec-3 || Sample introd...
Lec-4 || Ionization techniques || El || CI || FAB || FD|| MALDI || ESI || TSI || APCI || APPI
• Lec-4 || Ionization te...
Lec-5 || Electron Ionization (EI) || Instrumentation || Advantages || Disadvantages
• Lec-5 || Electron Ioni...
Lec-6 || Chemical ionization || Mechanism of CI || Ionizing gases || Advantages || Disadvantages
• Lec-6 || Chemical ioni...
Lec-7 || Direct Analysis in Real Time (DART) || Open air Ionization technique|| Helium as carrier
• Lec-7 || Direct Analys...
Lect-8 || Field desorption Ionization || Evaporative Tech || Soft Ionization || Anode emitters
• Lect-8 || Field desorp...
Lec-9 || Fast Atom Bombardment (FAB) || Neutral atom bombardment || Matrix || Direct Probe method
• Lec-9 || Fast Atom Bom...
Lec-10 || Matrix-Assisted Laser Desorption Ionization (MALDI) || Types & Properties of matrix
• Lec-10 || Matrix-Assis...
Lec-11 || Electro Spray Ionization (ESI) || Evaporative|| Soft Ionization|| Nebulization to aerosol
• Lec-11 || Electro Spra...
Lec-12 || Thermo Spray Ionization (TSI) || Evaporative & Soft ionization || HPLC Coupled TSI
• Lec-12 || Thermo Spray...
Lec-13 || Atmospheric Pressure Chemical Ionization (APCI)|| Soft Ionization || Corona Discharge Lamp
• Lec-13 || Atmospheric ...
Lec-14 || Atmospheric Pressure Photo Ionization (APPI)|| Soft ionization || Xenon lamp| Evaporative
• Lec-14 || Atmospheric ...
Lec#15 || Molecular ion peak || Parent ion peak || Identification & stability of molecular ion peak
• Lec#15 || Molecular io...
Lec-16 || Isotopic peaks in mass spectrometry || Relative intensities of isotopic peaks of Cl and Br
• Lec-16 || Isotopic pea...
Lec#17 || Metastable ion peak || Fragmentation in field free region || Mass spectrometry
• Lec#17 || Metastable i...
Lec#18 || Fragmentation || Types of peaks || Base peak || Daughter peaks || Mass spectrometry
• Lec#18 || Fragmentatio...
Lec-19 || Stevenson rule || Ionization of molecule || Fragmentation and stability of carbocation
• Lec-19 || Stevenson ru...
Lec-20 || Types of bond cleavage in Mass spectrometry || Charge and radical site initiated cleavage
• Lec-20 || Types of bon...
Lec-21 || McLafferty Rearrangement || All classes which give Mclafferty Rearrangement
• Lec-21 || McLafferty R...
Lec-22 || Retro Diels Alder Reaction || Fragmentation in cylcoalkenes || Dienes || Dienophiles
• Lec-22 || Retro Diels ...
Lec-23 || Fragmentation pattern in alkanes || Stability of carbocations & Molecular ion peaks
• Lec-23 || Fragmentatio...
Lec-24 || Fragmentation pattern of cycloalkanes & bicycloalkanes || Intensity of molecular ion peak
• Lec-24 || Fragmentatio...
Lec-25 || Fragmentation pattern of alkene, cycloalkene & alkyne | Mass spectrum of limonene & ionone
• Lec-25 || Fragmentatio...
Lec-26 || Mass fragmentation in aromatic hydrocarbons || Tropylium ion || Mclafferty rearrangement
• Lec-26 || Mass fragmen...
Lec-27 || Mass Fragmentation Pattern in alcohols, phenols, cyclic alcohols & thio-alcohols
• Lec-27 || Mass Fragmen...
Lec-28 || Mass fragmentation pattern of aldehydes || Peaks in mass spectrum of aldehydes
• Lec-28 || Mass fragmen...
Lec-29 || Mass fragmentation of ketones || Mclafferty rearrangement || Mass spectrum of ketones
• Lec-29 || Mass fragmen...
Lec-30 || Fragmentation pattern of esters || Methyl & higher esters || MacLafferty rearrangement
• Lec-30 || Fragmentatio...
Lec-31 || Mass fragmentation pattern of carboxylic acids | McLafferty rearrangement | Alpha cleavage
• Lec-31 || Mass fragmen...
Lec-32 || Mass fragmentation pattern of amines || Alpha cleavage || Cyclic & aromatic amines
• Lec-32 || Mass fragmen...
Lec-33 || Mass fragmentation pattern of amides || McLafferty rearrangement || Acetanilide
• Lec-33 || Mass fragmen...
Lec-34 || Mass Fragmentation Pattern of Nitriles || McLafferty rearrangement || Nitrogen rule
• Lec-34 || Mass Fragmen...
Lec-35 || Mass Fragmentation pattern of nitro compounds || Nitropropane || Nitrobenzene
• Lec-35 || Mass Fragmen...
Lec-36 || Mass fragmentation pattern of alkyl halides || Alpha cleavage || Isotopic peaks
• Lec-36 || Mass fragmen...
Thermo Spray Ionization (TSI)
Evaporative technique
Soft ionization
HPLC Coupled TSI
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