how to calculate crystallinity from XRD data using OriginLab - 06

Reference paper:
doi.org/10.1088/2053-1591/ab0aaf
In this video, I have shown a simple approach to calculating the crystallinity of material from XRD data using OriginPro software and an Excel sheet. If you need any help or have any questions, then feel free to ask in the comment section below. For more videos, please subscribe to my channel. Thank you.
#NanoWorld
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[@thetthetswe3004]

Thanks a lot NanoWorld. This video helps me coz i got the reviewer's comment, it said to calculate the % of crystallinity. Thanks again.

[@imandankar4807]

me too and i am trying to calculate it, does it work with u using this software and method??

[@thetthetswe3004]

@@imandankar4807 yes, it worked.

[@alialahmad4448]

Thank you very much please we need more video like this ,about how to use our data to get more info about our crystals, we need to hear your voice too)

[@archana3057]

Thank you so much nanoworld. These videos are really helpful.

[@syedfarooqadil]

Your video was really very helpful, Thank you so much nanoworld. May ALLAH bless you immensely for spearding important knowledge. Aameen

[@MuhammadSadiq-2729]

Should I adjust the baseline so that it touches some base-part of XRD graph?

[@muhammadnisarqasim636]

sir you doing awesome job. please make video on reveilment method.

[@swapnitapatra3458]

Thank you so much for uploading this video🙏

[@OfficialNeeraj]

can I do it, with raw data or I have to do some pre-step before do it? because I'm facing baseline problem in my data, some values are fine but some peaks are coming below the baseline. so please try to clear my doubt.

[@lugoloobiishaq864]

Please answer, cause ive got the same problem

[@sheikhbazila8585]

thank u so so so much for this amazing video. It really helped and is presented in the most perfect manner.. keep the good work going

[@nanoworld6122]

Glad it helped!

[@Sajujohnskj]

Thank you very much. This video helped me a lot. If possible please upload videos explaining (i) how to index XRD peaks of a crystal (ii) how to index SAED pattern

[@learningofturkish7809]

great job thnx very much. please could you tell me how i choose the constant according to the data

[@rauloliveira9579]

Thanks guys of the NanoWorld, this helped me a lot. Greetings from Brazil :)

[@nanoworld6122]

Happy to hear that.

[@rauloliveira9579]

@@nanoworld6122 I just have one question. If I work with a very crystalline material, it will have many crystalline peaks. Should I calculate the area of all of them in the angular range? Because there are many :(

[@nanoworld6122]

@@rauloliveira9579 Yes, If all crystalline peaks belongs to to your material then you must calculate area of all the peaks. As i did in this video.

[@rauloliveira9579]

@@nanoworld6122 I understand. In fact, when the worked material has many crystalline peaks, the work becomes larger. For these cases would Rietveld's method be better?

[@nanoworld6122]

@@rauloliveira9579 Yes, Rietveld's refinement is an automatic and more reliable method as compare this manual method.

[@lugoloobiishaq864]

@NanoWorld Thanks for the great job. My question 1, does overlap of area for near peaks affect the calculated crystallinity? Question 2 , does making a smooth graph and correcting baseline affect the calculated crystallinity?

[@aram9167]

For future reference, smoothing shouldn't affect the results much as long as not too much information is lost in the process, but baseline correction obviously affects results. Generally, having a baseline that's too high will reduce the crystallinity percentage.

[@lomasssoliman5697]

thank you so much, this video is really helpful

[@joycelim9085]

How do we know where to set the baseline?

[@AmjadKhan-em8yt]

thanks i get more information from your video lecture..

[@nanoworld6122]

Thank you.

[@researchbook7031]

Amazing, Thanks a lot...I have learned very important thing. Once again, Thank You So much

[@ibrahimnazemqader9153]

Great job bro. دەستت خۆش بێت

[@victorruiz4331]

do you have a research article were this equation was applied? I can not find an article where the equation was used

[@learningofturkish7809]

thnx so much. could i know what is the benefit from calculating crystallinity of material

[@dahcari6548]

Hi, I have question about calculation crystalline index (CrI) I've seen this ref of inorganic compounds, so with this method 1/ Could we use for polymer materials? 2/ Is this a relative method ? 3/ Do we have another method to check this method? (I mean calculate CrI by another method and compare with this method? I hope I would receive you answer soon. Thanks so much.

[@mariappanmani4112]

Thank you very much, it is helping me more, once again thank a lot

[@arslanliaqat9858]

Thank you so much sir. Allah bless you always.

[@mehranalam1274]

Do u have video how to calculate volume fraction from XRD ?

[@sitihajarsaharudin5931]

Thank you so much for sharing this calculation. It is really useful.

[@kmaegawa6910]

Thank you so much for your work... It will very helpful for me!

[@nanoworld6122]

you are welcome

[@RehamAtyaa]

Thank You so much. It was very beneficial to me.

[@nanoworld6122]

My pleasure.

[@TheMafia48]

How to integrate from 10 to 90 to get the whole area? And how do you know that in thsi case - you have taken all the peaks ?

[@devarshivyaskshitij1599]

take all the area ...

[@mehranalam1274]

could you please suggest reference article on this medthod

[@abdulkaberalsseady1645]

the material was really useful,, Thanks alot

[@nanoworld6122]

Thanks

[@sudeeptiwari1]

Kindly upload videos on Raman and PL fitting using Fityk

[@gulleemaan903]

nicely done ❤

[@Dr.PoorvaJi]

Thank you very much sir for this informative video...

[@nanoworld6122]

Most welcome

[@pny8598]

Can u please send me the xrd data for practice to plot multiple graph in origin

[@dungdao6594]

You can measured your samples and do it.

[@thetthetswe3004]

@NanoWorld, now I can calculate % crystallinity easily coz of ur good instruction. But I would like to ask about which method is it based on? coz I need to write this calculation in Materials and Method section. May I know any reference to cite in paper. Thanks to again.

[@nanoworld6122]

You may cite this article as a reference, doi.org/10.1088/2053-1591/ab0aaf

[@momonudin7059]

how to measure the baseline?

[@civilengineeringknowledgeb2955]

what about the value of amorphous?

[@hafiqaidil2067]

Thank you sir for this tutorial

[@AravindhanR-ix2zr]

thank you so much it is very much useful

[@nanoworld6122]

Enjoy...

[@abdulmanan5823]

What are the units of area?

[@aysarauteniyazova3925]

Thank you very much!!!

[@ZafarAli-pm4dz]

Excellent work

[@victorruiz4331]

can you plz make video on how to determine rate constant of dye degradation on origin from lnC/Co vs time please please

[@nanoworld6122]

i'll try.

[@victorruiz4331]

I will be eternally grateful to you

[@garrytalaroc]

Perfect for lazy readers like me. Thank you!

[@nanoworld6122]

😛

[@RAM-xr5ve]

Very useful video

[@masome-x8e]

Thanks ever so much🙏

[@زينالعابدينماجد-د2ب]

thank you very much

[@AnkitaSingh-un3sj]

I am not able to find peak analyser in my originpro. Please help.

[@nanoworld6122]

Okay, How can I help you?

[@maryamliaqat4471]

At 3:45 minute, i cant select my peak. Kindly reply me, i sent a message on FB. Thanks

[@chandanmahata5241]

double click

[@dr.kassahungashu]

Thanks

[@nadianatasya6724]

Helo, I’m having trouble with my graph. It has too many highest peak compare to the peak in your video. May I get your email so I can further discuss my problem with you? The data also reach up to 2000 in excel. I really need help since this is related to my fyp project. Please respond and help me :(

[@nanoworld6122]

Hello Ms. Nadia, you can contact us at, [e-mail] You can also reach us through our Facebook page. Send me your data, I'll check it.

[@sameninna9958]

@@nanoworld6122 you r very hopfull . I hope y can help me for my data XRD

[@learningofturkish7809]

Thank you so much, can i connect with you please.

[@nanoworld6122]

You can contact me through email. (Email address is available in the description of video)

[@nano-dataanalysis5033]

What is a unit of measurement. Area of ​​Crystalline Peaks؟؟؟

[@nanoworld6122]

Area unit = counts x 2theta

[@sameninna9958]

Im very interested with this

[@LucasRibeiro-bk3cx]

Obrigado!!

[@nguyenkequang]

need to buy origin pro 2018, 2020 or anything :(. i cant' use with origin pro 8 crack

[@nanoworld6122]

No need to buy, Originpro 9.5 is easily available with crack. You can download and install it.

[@RahulThakur-ou4nd]

how do you know what i want all the time😂

[@TheMissaya96]

Thank you so much. This video really helpful.