Silver Cell Anode Filters Part 4

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sreetips

sreetips

Күн бұрын

Пікірлер: 216
@rogerclaiborne6815
@rogerclaiborne6815 Жыл бұрын
He's not kidding about the dangers of those fumes. Doesn't take much. Wish I would have stayed away from messing with this stuff years ago. Outside where the wind constantly changes directions doesn't cut it, got to have a good fume hood set up like he does.
@rom65536
@rom65536 Жыл бұрын
They don't call it "Brown Death" for nothing. I hope you didn't get too much of it.
@Alsacien
@Alsacien Жыл бұрын
Excellent advice. Nitrogen dioxide is heavier than air, so it has a tendency to stick around if it isn't aspirated away by a good fume hood. Were you able to smell it sometimes? Could you expand a bit on your current symptoms, please?
@sreetips
@sreetips Жыл бұрын
Outside is just too dangerous. Even if approached upwind of the reaction, the wind forms eddy currents that pull the fumes right into your face. Even if you hold your breath, turn and walk ten paces, the fumes are still in your hair, clothes, eyes and skin. When you do breath you can still smell them. And if you can smell them then that means you’ve exposed your lungs. Doing these reactions without a fume hood is too dangerous.
@sreetips
@sreetips Жыл бұрын
When I first started, I didn’t have a fume hood. I did it in my back yard. I immediately noticed muscle cramps in my legs out of nowhere. My lungs do produce mucus at an abnormal rate. I’m sure that in the end, my exposure during my time with no fume hood, has caused irreversible damage.
@rogerclaiborne6815
@rogerclaiborne6815 Жыл бұрын
I got COPD and it may have contributed to some of that. I'm a construction worker and was exposed to a lot of dust as well. May be partially why I have some chronic sinus issues. I stay away from doctors as much as I can so don't know it for a fact. Just a suspicion. @@Alsacien
@derekforeal7049
@derekforeal7049 Жыл бұрын
Watching that yellow flash to black gets me every time
@AshChildOfGod
@AshChildOfGod Жыл бұрын
It was so instant that it caught me off guard😂 super cool
@JamesSkellington-xj8nn
@JamesSkellington-xj8nn Жыл бұрын
I absolutely agree 100 % seeing that change over is so amazing.😮😮😮
@Alsacien
@Alsacien Жыл бұрын
14 grams of gold is insane. Congrats! When I replied to the guy who wrote that it was foolish to go after what was left in the filters a few weeks ago, my prediction was that you'd end up with a bead of gold, a bead of platinum group metals, a few ounces of silver and satisfied viewers who learned something, but by "bead" I meant maybe 3 grams! It would be amazing to know how many kilograms of silver crystals came out of the silver cell to obtain 14 grams of gold from the impurities, but I suppose that this might be proprietary information. ;-) Looking at the mess you had to deal with in the first third of the video, I didn't expect it to end on such a high note! Thanks for yet another fascinating series!
@sreetips
@sreetips Жыл бұрын
Boiling nitric puts traces of gold in solution. Then it follows the silver into the anode basket.
@Alsacien
@Alsacien Жыл бұрын
@@sreetips That was my theory too. That those traces would accumulate into a total of 14g of gold is a testament to how much impure silver shot went through the silver cell! I hope that you kept enough information to be able to calculate a yield (how many grams of gold per kilogram of pure silver crystals), even if you choose to keep it private.
@matthewdroz5613
@matthewdroz5613 Жыл бұрын
Very clever and wonderful process to watch from start to finish. I have learnt so much from your videos. Thank you sir.
@Timechunks
@Timechunks Жыл бұрын
Once again persistence, patience and skill pay off, good to watch and a very cool way to make a dollar. Thank you.
@Antonowskyfly
@Antonowskyfly Жыл бұрын
You’re welcome! Definitely a marathon. I had to check the elapsed time, at what felt like the 1hr mark, to find that I was only 20min in. A rare case of time NOT flying by when having fun. An enthralling performance, both video edit-wise and refining result-wise. Thank you Sir!
@jamescball55
@jamescball55 Жыл бұрын
I have done chemistry research my whole career (retired now). Your video is an outstanding example of research when the unexpected happens - which, ironically, happens all the time. You show a very methodical and reasoned approach to problem solving. I love it. Wish I was back in the lab. Keep it up!! On another note I am going to make a silver cell with glass instead of a SS bowl. I love watching crystals grow. I have watched all your silver cell videos with facination.
@RyanEglitis
@RyanEglitis Жыл бұрын
Don't you need a metal bowl to run a current through to grow the crystals?
@jamescball55
@jamescball55 Жыл бұрын
My plan is to use a SS strip about 4 in wide the length of the glass vase as the other electrode.
@sreetips
@sreetips Жыл бұрын
Yes
@RyanEglitis
@RyanEglitis Жыл бұрын
@@dunravin But then all the growth is from that cathode instead of the entire bowl surface.
@RyanEglitis
@RyanEglitis Жыл бұрын
@@dunravin A glass cover would give similar visibility, without the warping effect of a bowl bottom.
@stevenjones916
@stevenjones916 Жыл бұрын
Patience of a saint but what a reward for your endeavour.
@b.c.9358
@b.c.9358 Жыл бұрын
Extremely interesting series. I've been having a strange new series of health issues and your videos are very calming, even when disaster strikes.
@iceman2184
@iceman2184 Жыл бұрын
SCIENCE! It was good to see you set aside the PGM mess and go for the gold. Circle back now that you're on a roll. You got this Kevin
@Dean_F
@Dean_F Жыл бұрын
Your videos are always a highlight to my day when they come on. The filter baasket series, while im sure its a huge pain, is just so much fun to watch. You are truly a master of your craft. On another note i refer everyone interested in refining to your KZbin. Not that you need the added support but you're still the goto for knowledge and never giving up. A youtuber named bigstacked melts down non ferrous metals mostly but he has a pile of silver contacts and sounds like he was ready to try something with them. So naturally ive been teying to get him to watxh you. Keep up the great work. I hope you love what you do because your viewers sure do.
@sreetips
@sreetips Жыл бұрын
Big Stack is awesome. Thanks for your support.
@someguy-k2h
@someguy-k2h Жыл бұрын
I'm impressed you got through the whole thing and wound up with 14g of gold. I bow to you, sir. You are what persistence looks like. Now you need to get the palladium and platinum that is left in your solutions. That's the really tricky part
@sreetips
@sreetips Жыл бұрын
I’m dreading it
@Joe.Rogan.
@Joe.Rogan. Жыл бұрын
It's so interesting to see how metals follow each other. That gold came from silver shot that was basically almost pure silver to begin with. By using a silver cell to extract only the silver from the silver shot and capture a the miniscule amounts of other metals in a vacuum filter bag then refine that down into its individual elements is amazing. This would be considered magic in the olden days.
@sreetips
@sreetips Жыл бұрын
I think the gold came from the nitric boils I do on inquarted gold. Hot nitric will put traces of gold in solution. Then it follows the silver into the anode basket of the silver cell.
@Joe.Rogan.
@Joe.Rogan. Жыл бұрын
@@sreetips Yeah that makes sense. 14g of gold just seems nuts to me.
@gunnystew7404
@gunnystew7404 Жыл бұрын
Well come back Mr. Sreetips!!! Welcome back, looking forward to the full length videos. ❤
@DavidDavis-Central_FL
@DavidDavis-Central_FL Жыл бұрын
Gooood evening from central Florida! Hope everyone has a great night! Been waiting for this video!
@sreetips
@sreetips Жыл бұрын
Goooood evening!
@yourex-zq2sh
@yourex-zq2sh Жыл бұрын
Hell yeah! Another upload by the king! Cheers!
@rogerclaiborne6815
@rogerclaiborne6815 Жыл бұрын
Who knew silver scraps had so much palladium, platinum, and gold impurities in it.
@apveening
@apveening Жыл бұрын
The answer very clearly is sreetips ;)
@sreetips
@sreetips Жыл бұрын
I believe that the gold came from nitric boils of inquarted gold. Boiling nitric puts traces of gold in solution. Then it follows the silver.
@tf3688
@tf3688 Жыл бұрын
I admire your persistence along with your knowledge. I'm glad to see it was well worth it!
@TroubledOnePaydirt
@TroubledOnePaydirt Жыл бұрын
That color change around 18:25ish when he drops those ice cubes in, was wild! 🤯
@davidmccleary5540
@davidmccleary5540 Жыл бұрын
Why I love this channel, if at first you don't succeed....good times
@bfd1565
@bfd1565 Жыл бұрын
Fascinating. Absolutely fascinating Sreetips.
@erikferland6602
@erikferland6602 Жыл бұрын
I love the color of the gold in solution. It’s close to my favorite color.
@sreetips
@sreetips Жыл бұрын
Notice that it’s darker orange when hot. As it cools it turns more toward yellow.
@BrokenTWelder
@BrokenTWelder Жыл бұрын
Another awesome to watch refining. Great job Senior Chief
@skinnywheelz
@skinnywheelz Жыл бұрын
I wonder if there is more gold in the solids remaining in the filter? Great video, Thanks for sharing!
@sreetips
@sreetips Жыл бұрын
I’m thinking the same thing. Maybe a little. I’ll give a good boil in AR in part 5 and we’ll see.
@ChrisCVW
@ChrisCVW Жыл бұрын
Really speaks to how important reprocessing all your “waste” is. How many attempts to capture that gold had it evaded before you finally got it in that ingot?
@sreetips
@sreetips Жыл бұрын
The gold probably came from nitric boils of inquarted gold.
@kwinterburn
@kwinterburn Жыл бұрын
Thinking about the difficulty separating the solids, I used to use pressure not a vacuum , started with a big syringe and a weight , it developed into a stainless funnel made from a piece of pipe with a threaded pipe fitting either end , the top had a airline connector , the bottom had a stainless mesh filter and a reducer stuck the vacuum on one end an 180 psi on the other and left it to it , bit of welding needed to get the filter supported properly , but it lasted for years , was used for extracting solids from transformer oil but the same process works for any material , there was a Russian idea years ago of using a open cell foam as the filter but you compressed the foam to get the filter size you wanted , then released the compression the foam sprang out and you could wash out the solid from the now very open filter ,
@TheBubagrunt
@TheBubagrunt Жыл бұрын
What a pain in the arse! This is interesting series in dealing with wastes and extracting extra value. I’m sure you’re frustrated but having fun as well. Thank you for sharing😊
@johnmccormick650
@johnmccormick650 Жыл бұрын
I thought maybe a nice gold button, not half an ounce! These videos never cease to amaze me.
@sreetips
@sreetips Жыл бұрын
I don’t ever remember getting that much gold from the anode filters.
@PiezPiedPy
@PiezPiedPy Жыл бұрын
Just goes to show how much gold is carried across with the silver from the nitic washes, totally surprised me.
@nikolajwinther5955
@nikolajwinther5955 Жыл бұрын
That's a surprisingly good explanation. I would say sreetips would be hard pressed to get that much gold, even if he processed gold plated silver only. And he never does. So where did it come from? The nicteic washes! Great that the gold is recovered.
@sreetips
@sreetips Жыл бұрын
The gold probably came from nitric boils of the inquarted gold.
@nikolajwinther5955
@nikolajwinther5955 Жыл бұрын
@@sreetips yes, you have sometimes confirmed gold in solution from nitric boils only. How much gold did you come across last time you did a anode-filter series?
@sreetips
@sreetips Жыл бұрын
Can’t remember, I’d have to look. But this one seems the highest amount recovered from these filters.
@newtronix
@newtronix Жыл бұрын
Excellent! Well worth the processes!
@floydsallee2041
@floydsallee2041 Жыл бұрын
Man you are so good at this it boggles the mind
@seymourpro6097
@seymourpro6097 Жыл бұрын
Some mixtures will filter through a thick bed of filter pulp. Get some filter paper or kitchen paper and add a lot of water then blend it with a blender or similar (buy your own!) then, on top of a filter circle fill the buchner funnel and let it drip to near dryness. You should have a half inch thick disc of filter paper which will retain much more in it's thickness than a single filter circle can. (My last lab of work bought the bits of filter paper that the circle had been cut from, for just this purpose -we used a lot of it.)
@sreetips
@sreetips Жыл бұрын
This was like trying to filter Elmers Glue.
@OG_Wakanobi
@OG_Wakanobi Жыл бұрын
I'd be curious to see what your personal stash looks like!
@jamisontaylor878
@jamisontaylor878 Жыл бұрын
Excellent video thank you great job😊
@ChrisHopkinsBass
@ChrisHopkinsBass Жыл бұрын
Kinda reminds me of the episode of Blackadder where Lord Percy creates a nugget of pure Green!
@davidestabrook5367
@davidestabrook5367 Жыл бұрын
That's chemistry, you think you know what's going to happen, then you find out, that you don't know what's happening. It's frustrating at first, but you experiment to figure it out, and gain knowledge and experience, and are left with a feeling of satisfaction and self-confidence, on top of the pile of gunky filters. There's nothing else like it. I had one problem where no matter how much sodium carbonate I added, the pH didn't rise. And that's what started my learning about buffers, and so I started making buffer solutions, to get the pH where I wanted it.
@ottolehikoinen6193
@ottolehikoinen6193 Жыл бұрын
The DMG polymerized loosely due Pd ions? Try to change the pH of the sticky stuff with some lime?
@bigdaddympd
@bigdaddympd Жыл бұрын
Have you looked into refining PGM into pure constituents? How do they do it in industrial refining?
@sreetips
@sreetips Жыл бұрын
If I get enough PGMs then I’ll try a refining.
@davidgardiner3386
@davidgardiner3386 Жыл бұрын
hey mr sreetips i asked you a question about your waste couple of weeks ago and i looked into it and i started a course on chem waste management and got a job in waste water management so heres hoping .
@sreetips
@sreetips Жыл бұрын
Congratulations
@jeepin4on4
@jeepin4on4 Жыл бұрын
Thanks for this lesson. Silver cell anode filters and you recovered Gold. Question is, where did the gold come from? Most of your silver is from sterling silver ware that I see or watch. Should I buy every sterling set I find and go through the process of refining gold silver and trace amount of palladium? I never get platinum or rhodium ( too impatient i guess).
@Alsacien
@Alsacien Жыл бұрын
It must be coming from two sources. 1) Impurities in the silver objects he dissolves directly into hot nitric acid. 2) Minuscule amounts of gold that go into solution with the hot nitric acid baths when Sreetips works on refining gold. Then the gold from these two sources cements out of the solution onto pieces of copper along with the silver and ends up as impurities in the silver shot that is used to feed the silver cell.
@jeepin4on4
@jeepin4on4 Жыл бұрын
I did not know that gold will cement out on copper, thanks.
@apveening
@apveening Жыл бұрын
@@jeepin4on4 Check the reactivity tables, everything above (or below, depending on direction) copper will cement out on copper. That includes, but is not limited to silver, gold and all PGMs. Copper in its turn (together with the aforementioned group) will cement out on iron, which again will cement out on zinc (if you wish to recover iron).
@sreetips
@sreetips Жыл бұрын
Silver is a carrier of gold and platinum group metals. Hot nitric boils will put traces of gold in solution. Then, it follows the silver.
@lylestavast7652
@lylestavast7652 Жыл бұрын
as many tmes as you mentioned you didn't know what you had there, and it turned out a nice inglette of gold, I think this certifies you as an Alchemist !
@Rob337_aka_CancelProof
@Rob337_aka_CancelProof Жыл бұрын
3:06 Thank you for doing that in time-lapse but I'm curious why you chose to pipette instead of decanting? I obviously missed something but I'm unsure as to win and with multiple videos preceding this one I was hoping you could just help me out with that
@sreetips
@sreetips Жыл бұрын
I didn’t want to disturb the settled solids
@shaneyearby4438
@shaneyearby4438 Жыл бұрын
Very nice recovery and a nice bar to boot. 👏
@Kanalmarket
@Kanalmarket Жыл бұрын
Approximately how many kilograms of silver were purified to get that much gold and side products? Thanks for your videos and answer.
@sreetips
@sreetips Жыл бұрын
About 25 pounds
@RyanEglitis
@RyanEglitis Жыл бұрын
Bit messy, but good you have a way forward. I always wonder why you don't run the non-smb gold dropping method for mixed PGMs (like this and the stock pots), since it's supposed to be more gold selective.
@Rob337_aka_CancelProof
@Rob337_aka_CancelProof Жыл бұрын
4:30 I recently saw a buchner filter funnel (I think that's what it's called) that was easily the size of a dinner plate and likely had at least ten times the surface area you are working with currently that might be worth investing in if you're going to do this more in the future
@kimberlynolz5725
@kimberlynolz5725 Жыл бұрын
Oh he has one I believe it's a 10 or 12 in Buckner funnel
@seymourpro6097
@seymourpro6097 Жыл бұрын
Have you seen the price of big labware?
@davidestabrook5367
@davidestabrook5367 Жыл бұрын
Instead of using big filters, the best technique is to learn how to make diatomaceous earth (D.E.) filtercakes. You add 1 teaspoon D.E. to a 60 mL plastic pot, then add 25 mL water (or solvent your filtering, like ethanol). Then swirl it around to make a slurry. You pour this onto a filter paper, and shake the Buchner to help it settle, then let it gravity filter until the water runs through. You then slowly add vacuum to pack it hard. Then refilter what runs through, until the water runs clear. D.E. filtercakes filter to submicron efficiency, at a reasonably fast drip rate. They can filter stuff that blocks paper filters instantly. You'll need to experiment to find out how much to use for your filter size, but a 2-5 mm D.E. filtercake layer is adequate. And you can scratch the D.E. with a glass rod, to expose fresh surface, when the filtration rate drops too low.
@sreetips
@sreetips Жыл бұрын
I’ll check it out. Thank you.
@sreetips
@sreetips Жыл бұрын
Fossilized remains of diatoms.
@pozeetronz
@pozeetronz Жыл бұрын
a magnificent ingot and a good job, Mr. Chemist.have you tried restoring gold with Sodium Nitrite?
@sreetips
@sreetips Жыл бұрын
I have not
@buggsy5
@buggsy5 Жыл бұрын
I am surprised that so much gold followed the silver from your nitric acid digestions. In the inquartations, there are bound to be near molecular gold particles completely surrounded by your silver/copper used for inquartation and is too fine to be caught by your relatively coarse filters. As you stated, those minute particles would follow the silver.
@ArielleViking
@ArielleViking Жыл бұрын
Beautiful half oz gold bar from that black mud, love it. 👍
@josephnoonan82
@josephnoonan82 Жыл бұрын
great video!
@whatthefunction9140
@whatthefunction9140 Жыл бұрын
I lost track of where the gold came from. How did that much gold get in the silver shot?
@ctvxl
@ctvxl Жыл бұрын
Most of the silver was used for gold refining. He in-quarts the gold with silver, then extracts the silver with nitric acid. While gold is not very reactive with hot nitric acid, some very small trace amounts do get dissolved in it.
@apveening
@apveening Жыл бұрын
@@ctvxl And that ends up with the silver in the cement, which ends up as silver shot in the silver cells. And so the gold (and PGMs) end up in the silver cell slime.
@sreetips
@sreetips Жыл бұрын
Hot nitric boils put traces of gold in solution.
@BigWeenieC
@BigWeenieC Жыл бұрын
I’m sure you’ve answered this in the past, but where do you source your chemicals for refining gold? I.e. Hydrochloric, Nitric and sulfuric acid… I’m sure it gets expensive!!
@sreetips
@sreetips Жыл бұрын
Mostly from the hardware store. Nitric from dudadiesel.com
@eddieg5466
@eddieg5466 Жыл бұрын
Good morning, a couple of years back I saved one of your videos "How to recover gold from trimmed fingers using household chemicals without heating it " Today I was trying to get back to it, but I couldn't find it, not even straight from your channel. Can you please send me a link so I can rewatch it again !! Thank you in advance !! Big fan of the channel by the way !!.😊✌
@sreetips
@sreetips Жыл бұрын
That must have been the salt and vinegar recovery.
@eddieg5466
@eddieg5466 Жыл бұрын
@@sreetips I saw it already, and it is not ..😪 I have some notes from that video, and you started with 500g of trimmed fingers on a 4000 ml beaker, then you explained how to get the HCI from Ace hardware store, hydrogen peroxide from any drug store, regular household bleach, also using 20 mule team borax and stump out by bonide from Ace hardware. I actually had the process written down, but I wanted to check the video again to make sure I'm doing it right...but I can find it on KZbin..😓
@sreetips
@sreetips Жыл бұрын
@eddieg5466 “computer circuit card gold recover hardware store chemicals pt1” and there’s a pt2. Is that it?
@eddieg5466
@eddieg5466 Жыл бұрын
@@sreetips I got it !!🥳 Looking at the last suggestion you send me, the one that I was looking for popped up.."how to recover gold from computer scrap with household chemicals " Thank you for the help my friend. Have a wonderful weekend !! Best regards !!..✌💖
@ruffanuff
@ruffanuff Жыл бұрын
14 grams is outstanding, sure you never used to get anything like that previous?! Great all your hard work paid off.💪
@sreetips
@sreetips Жыл бұрын
I don’t remember getting that much gold from these silver cell slimes.
@josephcormier5974
@josephcormier5974 Жыл бұрын
It's a great thing to redo the slime look at what you just got 14 grams of beautiful gold thank you for sharing this with us six stars sir
@ctstone8322
@ctstone8322 Жыл бұрын
I'm starting up my first refining project and right now the hardest part is finding scrap gold. It's rough in Michigan
@sreetips
@sreetips Жыл бұрын
It’s out there. You’ve got to know when, where and what to look for. Get up early and be there first or else all the metals will be long gone.
@ctstone8322
@ctstone8322 Жыл бұрын
@sreetips Big Thanks Sreetips! Also I've watched alot of your videos and I was wondering 🤔 could you possibly do a video about inquarting karat gold with silver crystals from the silver cell, or is that somthing out of the possibilities?
@jwrappuhn71
@jwrappuhn71 Жыл бұрын
Excellent.
@prestontucker6171
@prestontucker6171 Жыл бұрын
So is this amount of gold typical as "contamination" in your cement silver? I've got to think that it's coming from waste that ends up in your stock pot from other gold refining processes, right? Or is there really this much gold to be found in the sterling silver you process with your silver cells?
@sreetips
@sreetips Жыл бұрын
When I boil inquarted gold in nitric, the boiling nitric does put traces of gold in solution. These traces get poured off into my silver jar. Then they follow the silver into my silver cell anode filter. Gold is insoluble in the anode filter. It gets trapped in the filter. And that, I believe, is where all that gold comes from.
@MickNailZ
@MickNailZ Жыл бұрын
14 kg silver and about 14g of gold is about .1% gold. Do you think some of that gold comes from your melt table “dust”? It would be interesting if you processed your melt table sweeps, or atleast half of them
@sreetips
@sreetips Жыл бұрын
Some of the gold dissolves in the hot nitric boils. It get poured off into the silver jar. Then cemented on copper along with the silver. The cement silver (with traces of gold in it) gets melted into shot and run through the silver cell. The gold is insoluble do it stays in the anode filter with the slimes.
@MickNailZ
@MickNailZ Жыл бұрын
@@sreetips I do find that some gold in nitric acid boils. I use zinc to collect, since zinc doesn’t dissolve in nitric readily. But it wouldn’t be as fun to not have gold in the slimes. Makes it worth it. The PGMs are good for a video, bad for time management
@sreetips
@sreetips Жыл бұрын
Nitric won’t dissolve zinc. I didn’t know that.
@bobross5580
@bobross5580 Жыл бұрын
Amazing!
@HE-pu3nt
@HE-pu3nt Жыл бұрын
The guy at your local hardware store must think you REALLY hate tree's.😁.
@ericmcc75
@ericmcc75 Жыл бұрын
I am completely curious about what the financial profit is with the amount of acids, filter papers, an other consumables. I know you do a great job minimizing the wastes. I am not asking about specifics, but percentage profit would quell my curiosity.
@ericmcc75
@ericmcc75 Жыл бұрын
@Sreetips_Contact023 since you opened your account 12 minutes ago, I suspect this is a solid scam. Reporting.
@sreetips
@sreetips Жыл бұрын
My profit is not in paper dollars. It’s in pure gold. I’d have to sell the gold to realize a profit in dollars. And I ain’t selling any of my gold. My goal is to convert as much paper into gold as fast as I can. While it’s still dirt cheap.
@ericmcc75
@ericmcc75 Жыл бұрын
@sreetips wise move. I appreciate your videos. So essentially, you are converting paper credits to metal ounces. With this conversion, are you seeing profit at the current exchange (again, considering input costs)?
@D_A86
@D_A86 Жыл бұрын
2:26 I don't know why but this cracked me up 😅😅
@NOFX0890
@NOFX0890 Жыл бұрын
Nice!
@frantiseklaluch6605
@frantiseklaluch6605 Жыл бұрын
Wow, I have 10 g of gold from electronic scrap, you have 14 from anode slime... BTW, your furnace has some mark on the top now... I am not the only one with marked furnace... 🙂 What could be those last "insoluble" solids?
@apveening
@apveening Жыл бұрын
I expect there to be some (most definitely not much) iridium and osmium, which will in trace amounts follow other PGMs, but are by and large insoluble even in aqua regia. For the remainder, I don't have the foggiest.
@PetraKann
@PetraKann Жыл бұрын
Gold ions are positive - why are they accumulating at the anode which is also positive?
@sreetips
@sreetips Жыл бұрын
Nitric boils put gold in solution. Then it follows the silver into the anode basket. But the gold doesn’t dissolve. It gets trapped in the anode filter as slimes.
@MrTexaninNC
@MrTexaninNC Жыл бұрын
I think that Walmart brand distilled water has chlorine in it. All of my silver nitric acid boils that I’ve used that water in has white crystals that formed. Is that silver chloride or something else?
@sreetips
@sreetips Жыл бұрын
Who knows what compounds lurk in the solutions of refiners?
@scotthultin7769
@scotthultin7769 Жыл бұрын
192👍's up sreetips thank you for sharing 😊
@adrianstanton2652
@adrianstanton2652 Жыл бұрын
A question Would using hot distilled water be better at rinsing solids?
@sreetips
@sreetips Жыл бұрын
Yes
@jbmaximus6910
@jbmaximus6910 Жыл бұрын
What is DMG? IM sorry I just dont know?
@ottolehikoinen6193
@ottolehikoinen6193 Жыл бұрын
en.m.wikipedia.org/wiki/Dimethylglyoxime forms loose coordination compounds with select metal ions having an electron structure with specific properties
@ChrisHopkinsBass
@ChrisHopkinsBass Жыл бұрын
There’s Gold in them thar solutions!
@MADDLADO1
@MADDLADO1 Жыл бұрын
Nice job, but someone might have to buy you a new lab shirt for Christmas, lol
@sreetips
@sreetips Жыл бұрын
I’m going to offer it for sales on my eBay site.
@MADDLADO1
@MADDLADO1 Жыл бұрын
@@sreetips That's hilarious, 🤣😂
@joshkelly3743
@joshkelly3743 Жыл бұрын
This is an art form
@sergeantcraphead
@sergeantcraphead Жыл бұрын
Hello from Colorado Mr sreetips!
@sreetips
@sreetips Жыл бұрын
Hello!
@gfhrtshergheghegewgewgew1730
@gfhrtshergheghegewgewgew1730 Жыл бұрын
huh? how was that much gold in your silver shot to be left behind in the silver cell anode filters? so basically the silver that cements out of the silver nitrate (that comes from the gold refining where you nitric boil out the silver in the enquarted gold) isn't entirely silver and somehow gold is coming out in the silver nitrate solution and cementing out onto the copper with the silver as well as the other less reactive metals aka PGMs?
@sreetips
@sreetips Жыл бұрын
That’s correct. Boiling nitric will put gold in solution during the nitric boils of the inquarted gold. The gold then follows the silver into the silver cell and gets trapped in the silver cell anode filter.
@perrypoling3860
@perrypoling3860 Жыл бұрын
Sreetips, with all the distilled water you use, have you thought about making your own ? Love you science, adventure taking and dry humor. Thank you for inspiring my new hobby. 7:33
@Heymrk
@Heymrk Жыл бұрын
He's discussed it before and while he would like to have a water distiller, his setup just doesn't accommodate.
@letsdragthecave2017
@letsdragthecave2017 Жыл бұрын
I'm guessing that distilled water is probably cheaper to buy than to make
@perrypoling3860
@perrypoling3860 Жыл бұрын
Thank you for the replies. I did not look to hard before I asked. I have one that was my reasoning.
@sreetips
@sreetips Жыл бұрын
I use about twenty gallons per month. It is easier for me to buy it at the grocery store.
@zero-waste
@zero-waste Жыл бұрын
@@letsdragthecave2017. I use huge quantities of distilled water every month. All is homemade at no cost, by utilization of the waste heat from my four pyrolysis units and my metal melting furnace.
@johnM-Jr
@johnM-Jr Жыл бұрын
Hi Sreetips,, i was looking on eebay... saw an ad for 45+ Pounds Old PC Motherboards Gold Metals Recovery Scrap Lot Recycle. if you had to take a wild guess, about how much gold would you get from a lot like that?
@deanfulford69
@deanfulford69 Жыл бұрын
At least 75$
@matthewf1979
@matthewf1979 Жыл бұрын
Sreetips has quite a few gold finger/pc scrap videos. Don’t waste your time if you’re looking to get a payday out of it. As a hobby or for the experience, go for it. It’s a lot of work.
@sreetips
@sreetips Жыл бұрын
I’m not sure. But I’d hate to have to face a mountain of low-yielding computer scrap.
@jamesd4013
@jamesd4013 Жыл бұрын
Wow. Nice
@JoelHirtle
@JoelHirtle Жыл бұрын
What happens with the sandy looking material that you removed the gold from?
@rom65536
@rom65536 Жыл бұрын
he'll likely do another aqua regia extraction on it just to make sure he got all the good stuff.
@sreetips
@sreetips Жыл бұрын
I’ll boil it in some more AR in part 5
@mrtank1967
@mrtank1967 Жыл бұрын
So worth keeping those what look to be garbage filters. Nicely done.
@garymyers6638
@garymyers6638 Жыл бұрын
Do you have a person you can ask when things go wrong?
@sreetips
@sreetips Жыл бұрын
Not really. Most refiners are reluctant to give up their refining secrets. Especially to someone who they know will share it with the masses on KZbin. All I have is my experience and common sense to rely on. In many cases, when it looks like I’m making a bold move, it’s really just taking the next logical step based on my experience.
@nelsonosbornne4531
@nelsonosbornne4531 Жыл бұрын
When will melt the palladium and silver? The is a 5 th part?
@sreetips
@sreetips Жыл бұрын
Soon, pt5 is coming.
@nelsonosbornne4531
@nelsonosbornne4531 Жыл бұрын
@@sreetips excellent!
@youssefzouine8191
@youssefzouine8191 Жыл бұрын
Please don't delay the next part too much 😂
@EchoJulez
@EchoJulez Жыл бұрын
Dang! Caught the video drop!
@Sanzus2
@Sanzus2 Жыл бұрын
Nice! That green jello though?
@sreetips
@sreetips Жыл бұрын
I’ll find a way to get around it
@Mephisto707
@Mephisto707 Жыл бұрын
Will you melt the platinum/paladium at some point?
@sreetips
@sreetips Жыл бұрын
Yes, if I get enough of it to process.
@derekforeal7049
@derekforeal7049 Жыл бұрын
Wow lotta small transfers
@shaneyork300
@shaneyork300 Жыл бұрын
I don't think I ever seen a color change happen so quickly
@RollingRoadEFI
@RollingRoadEFI Жыл бұрын
The PGM precipitate looks like ramen noodle seasoning.
@ICU2B4UDO
@ICU2B4UDO Жыл бұрын
About $975.00 Mstr. Ch. Not a bad haul at all...
@nwliving
@nwliving 9 ай бұрын
Second time thru. Love it
@silentmuffin5804
@silentmuffin5804 Жыл бұрын
Could a little bit more gold be in the sand stuff it would be cool if you could show us you got all the gold
@sreetips
@sreetips Жыл бұрын
Possibly, I’ll give it another boil in AR in part 5 and we’ll see.
@slimpickins09er87
@slimpickins09er87 Жыл бұрын
Did you just create gold out of silver, palladium and dmg. I could swear you already got the gold out of solution.
@sreetips
@sreetips Жыл бұрын
Nitric boils put traces of gold in solution. Then it follows the silver.
@TroubledOnePaydirt
@TroubledOnePaydirt Жыл бұрын
Yeah I think I see why he mostly refines gold. My god this stuff was messy. He seems completely fed up with this green sludge. 😩
@sreetips
@sreetips Жыл бұрын
It’s as if the metals are laughing at me, right out of the beaker!
@GuruEthereal
@GuruEthereal Жыл бұрын
💛💛💛🤙✌🖖🖖 STREETIPS
@dynorat12
@dynorat12 Жыл бұрын
great little bar
@ANCIENTASTRONAUT411
@ANCIENTASTRONAUT411 Жыл бұрын
We love screetips
@miltondamiao6540
@miltondamiao6540 Жыл бұрын
Super top.
@jasonpavlik4904
@jasonpavlik4904 Жыл бұрын
$850 today's price
@gregfridholm2136
@gregfridholm2136 Жыл бұрын
What is DMG?
@sreetips
@sreetips Жыл бұрын
Dimethylglyoxime
Silver Cell Anode Filters Part 5
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