XRD Analysis for Phase Determination using X'Pert HighScore Plus

In this tutorial, phase determination using X'Pert HighScore Plus software has been demonstrated.
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Instructor: Manoj Kumar
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[@ysharshit277]

Wonderful video on how to do XRD analysis. Very helpful for our research. Thank you. Keep it up

[@sunvish28]

Explained XRD in a very easy way. Thank You Sir.

[@SMSTechEdu]

Thanks :)

[@techanddesignnikhil]

It’s really a well explained video in limited and less confusing words . Thanks

[@SMSTechEdu]

Thank You very much

[@sumitsharma9187]

Guys!! You elucidate X-Ray Diffraction analysis clearly and It seems easy to understand. Hope You will continue to upload this type of video which makes the metallurgical characterization analysis become easier. All the best.

[@SMSTechEdu]

Thank you so much for encouraging words!! Surely we will work on your suggestions.

[@yoddha24]

Do not subtract the background as the area under the curve for peaks (having information about structure, atom type etc.) is destroyed. Instead just use the button "Accept"

[@asfandyarimtiaz7322]

Beautifully composed! Please do more videos on strain calculations and rietveld refinement

[@asfandyarimtiaz7322]

Actually, when I determine background, the noise gets increased in the spectrum. How to address that issue?

[@dantegervasoni]

Thanks mate, you literally saved my life...

[@rayappashrinivasmahale2438]

Thank you for Informative video...Sir how to calculate volume fractions from XRD data?

[@anamikasahu5440]

Can u please share the link of video in which u described how to calculate the percentage of different phases in which they are present in sample?

[@rahmarahma9644]

Very nice video ! Please do more videos on strain calculations and rietveld refinement

[@djaidifatiha4875]

i need it too please if you have some informations about this method help me

[@radhikachada7422]

Could you please provide software link.it would be great help for me.Tnq

[@victorpedott5856]

Thanks for your explantion Manoj Kumar. Could you share the database that you used to identify your peaks?

[@sipundash]

Is 47 is good match or should it be higher? What about other peaks in reference pattern?

[@jamalkhatib7610]

Thank you for explain. Pleas , I got x data as a text file. How can I get it into the program? Can you help me ?

[@ulfaatmuskaan4489]

Detailed video. Very informative and to the point👍.

[@hectordavidagudeloarias7484]

Why not were the checked parameters of fit goodness before the phase analysis (search and match)?

[@liaquataziz8724]

how to calculate texture coefficient by using x'pert high score software?

[@sunandobanerjee7665]

sir whenever i am subtracting the background using bending factor of around 5 or 6, roughness of the data is increasing too much, how to avoid that ???

[@protonplusacademy1839]

Sir I have made the composite of copper and zinc using plant extract.....2theta intense peak comes at 29.....sir I can't be analyzed the 29 peak.......sir plz help me......how to analyze this 29 intense peak

[@raju8184]

Thanks a lot for your video...apt explanation saved my day

[@aneeqazahra4660]

Sir i didn't get the references files with score

[@rehanabibi3171]

through this software how we can find out the particles size by shrrer equation as given in tools of this software? plz reply i want to calculate particle size but i dont how how to d?

[@muhammadim1575]

thank you so much for making such a helpful video

[@aswinia1568]

Can you provide the link to download the software please sir

[@longlove2899]

Thank you very much sir, can u please share the database u r using for xrd analysis.?

[@lizardop71]

I have one doubt , xrd report i have word fomet , the formet not supported in xpert highscore how to fix

[@SMSTechEdu]

.raw or .xrdml format is needed.

[@خواطر-ص3ن]

Hi how are you broo i have a problem i have a forma (.ASC) file i want to convert to (.RAW) format please can you help me with that.

[@muhammadim1575]

can we label peaks in this software

[@hosseinnaghizadeh3065]

Thank you very much, It was a great tutorial video.

[@muhammadim1575]

please make a video on using scherrer calculator in xpert high score software

[@ahmedaltejany8187]

Thank you for the video ... I am looking for a way to download x'pert high score but i couldn't find any link .. please send the link for me if you have it i really need it. Thanx...

[@amarishkumarshukla3214]

Gr8, its a excellent work, were waiting from long time. Please upload some videos related to, how we analyse "High entropy alloys, Powder sample. I am waiting for that.

[@SMSTechEdu]

Sure sir, We will definitely come up with more such videos.

[@esokkiyaa929]

Thank you. it is useful. how to take experimental and matched x and y values for plotting ?

[@SMSTechEdu]

Save the xpert highscore file in ASCII format. From there you can get they x and y values.

[@geologist1005]

So Calcium Silicide is the second phase...Correct?

[@usmanchem08]

Hello. Can you pls give the download link? My university systems have 2006 version which does not link to any database and therefore I am unable to perform the pattern search

[@pinalrana]

Can you please explain how we can find stress and strain using software

[@kodaiimman]

how to calculate the crystallite size from this software make the video its helpful for researcher

[@djaidifatiha4875]

I need it too by williamson hall method please

[@yashrajkanaskar2452]

Very helpful video sir, Thank you !

[@SMSTechEdu]

Most welcome!

[@faheemwani1996]

sir how to calculate lattice parameter of composite film Polyvinyl Achohol (PVA)-LaFeO3 with different concentrations

[@JarnailSingh-fz8dl]

Thanks for providing such useful information

[@maamarouraghi6678]

Can you send me the link to install High score plus software and database. Thank you

[@mairaliaqat8143]

i have XRD data file saved in "ESG format" how can i open esg file in xpert high score

[@realityofhuman4649]

Hi sir, I try to open an xrd file but I could not do that that's why I want to know which data could be open with X'Pert HighScore thank you

[@yogendrachouksey6643]

copy the xrd counts and intensity values in a word document. save the file with extension .ASC like nina.ASC , right klick on the file, select open with xpert high score I hope this helps

[@realityofhuman4649]

yogendra chouksey thank you sir i will try it

[@djouernestserge4244]

Thanks for this good video. But to understand it very well, please can i have the sofware or the link to download it online.

[@ankursarswat]

You will hardly find it online unless someone provide you personally.

[@अमितकुमारमिश्र-ग8झ]

could you please share any video on Rietveld Analysis..Thanks.

[@ShagertHourbour]

what if we don't know anything about the material, how should we deal with that analyze menu

[@AishwaryaPatil-pc3uo]

you should have to know atleast elements.

[@ricardovelazquezhernandez7587]

If you still have the softwaae, I would like have the link for dowload it, please

[@khalidhasan7241]

Could you please make a video of reitveld refinement by high score?

[@zumbiorion]

Thank you very much for your willingness!

[@SMSTechEdu]

You are most welcome Sir. Have a great day.

[@smitapandey2249]

Nice video really helpful.

[@sumantamajhi8117]

Sir when I uplod the xrd data then it shows file format not supported

[@anshu6008]

file format must be .xrmdl

[@lizardop71]

The file be word format same problem to me

[@lizardop71]

​@@anshu6008how to change fomat

[@lizardop71]

​@@anshu6008i have word format

[@SMSTechEdu]

.raw or .xrdml format is needed.

[@bhagyashree649]

very well explained

[@SMSTechEdu]

Thanks Bhagya for your encouraging comment :)

[@universalmoralstories]

Thanks, very much helpful

[@aliakremi631]

how to convert XRD excel or txt file data to xrdml file?

[@ikramlabtaini8199]

PowDDL Converter

[@valenciacarrasquillapaolat311]

How do I synchronize the database to the program?

[@leonngao5462]

www.crystallography.net/cod/archives/2016/PANalytical/COD_2016_ConvHS4x.zip I downloaded database of Highcore X'pert by link

[@andreyilin9877]

Paola, you should pay attention to what version of the HighScore do you have in order to determine which database should you use. Here you would find open Crystallography Database in which you have to look for a database suitable to your program version. If you have 4.0+ version you may use the database from July 2016, but for a previous 3.0.5 (also known as 3.0e) you will have to use the database from October 2014. In each release you will find a ReadMe file with further details. Regards.

[@mustaphamatrouf3579]

please could you share the Xpert high score software and database files, please ^^

[@debakshikashyap9892]

Where to done labelling?

[@estherrubavathi6072]

how to get phase percentage for multiphases

[@sawairakhan9974]

My COD cards showing Phase(T9) problem

[@pradeepkumarrout5269]

May you please send me the software.

[@akashgayakwad8983]

If I have text file of XRD data, so this software will support or not?? please answer anyone??

[@Manojkumar926]

No, it should be converted to compatible format.

[@joaocalandrini2330]

do u have the program?

[@SMSTechEdu]

No Sir.

[@Manojkumar926]

Can you please upload a tutorial on ritvelt analysis?

[@sunandobanerjee7665]

It's important..should upload

[@faheemwani1996]

sir please show me magnetocapacitance vs frequency data analysis

[@lokeshkumartripathi3817]

Sir make video about amount of phases present in sample

[@SMSTechEdu]

Thanks for your query. Video on this topic oming soon.

[@Manojkumar926]

That requires a different software. Hope they upload that tutorial too.

[@gyanvardhan8580]

👍

[@arko3822]

thanks a lot Sir

[@ppamonha]

Thank you!

[@kaswar9234]

Thank you very mach

[@joyrosarian7249]

thank you

[@bharathimeti7753]

kindly let me know if u can send me JCPDS CARD NO. for my material.i need it at the earliest

[@derrouicheafifa3491]

nice

[@palomajackson600]

where is the link to download x'pert high score plus?

[@ankursarswat]

You will hardly find it online unless someone provide you personally.

[@Sxmeerr]

It says no candidate fount

[@faheemwani1996]

sir please send me the link of this software

[@anandbharti7735]

👍

[@sestaisilimism8902]

Thank you

[@SMSTechEdu]

You're welcome