Hey Picky, I would really appreciate a precise 'recipe' to make the appropriate strength for both the Cetrimide and the Ferric Nitrate solutions. I have 110 fully gold-plated telecom PCB s so will need to make at least 10 liters of solution and then re-use it several times! Many thanks and have a great 2023!
@silviugavrila94612 жыл бұрын
can we use a lower concentration of the citrimide solution like 5% or 10% witch is found in industrial desinfectant or can the citrimide be replaced with some other inhibitor withs is more available
@RANDOMIZE-qk2vk4 ай бұрын
Thanks for sharing! You have great knowledge How many times can this solution be used before it loses the ability to dissolve tin? Do you know how to recover the tin from the solution ?
@PickyPlans4 ай бұрын
Thanks, to about 150-200 g tin per liter. Add HCl then filter lead chloride and percipitate tin using aluminum
@MrMegaMaui2 жыл бұрын
I saw an alternative compound based on ammonium nitrate sulfuric acid and urea
@bencapobianco20452 жыл бұрын
I’m a new subscriber! Love the information you provide!!!! Great job keep it up!
@PickyPlans2 жыл бұрын
Here is link to main article US patent i Don't have any claim on it, this was a demonstration only and research to test different inhibitor: patents.google.com/patent/EP0559379B1/en Make sure to SUBSCRIBE and stay updated 👇kzbin.info Leave a comment below, let me know what you're thinking 😉
@julianalcorso57032 жыл бұрын
Looks like an excellent dissolving solution. Two questions please........ 1. Can I make the Cetrimide? If so what is the recipe? I have looked online and I do not see a 15% solution. 2. approximately how much iron do I need to dissolve in how much HNO3 to make the ferric nitrate solution? (to arrive at 78%) I assume I can just adjust the volumes of the components depending on the concentrations available? for example, my HNO3 is 68% so I would only add 44.2ml, and so on. Please keep these great and informative experiments coming. WELL DONE!!
@julianalcorso57032 жыл бұрын
@@PickyPlans Outstanding! Thank you so much! I am in Australia, where are you??
@julianalcorso57032 жыл бұрын
@@PickyPlans What a beautiful country and the most friendly people! I visited many years ago........ And the food YUM YUM
@seanflannery59762 жыл бұрын
Seems like a great solution for dissolving tin I'd love to give it a try. Wondering where you can buy the cetrimide or how you can make it. Had trouble finding a answer to ether of those questions.
@hamidrezakhansari64692 жыл бұрын
Wooow It was very attractive👍🏻✌🏻
@TheRecho Жыл бұрын
Really nice and fast. However, is there an alternative to the cetrimide? I simply cant find any in Europe 😕
@PickyPlans Жыл бұрын
Try find one of these three, in pure form only 1 % would be enough for this purpose. Dodecyltrimethylammonium bromide C14: Tetradecyltrimethylammonium bromide C16: Hexadecyltrimethylammonium bromide
@jesserodgers28122 жыл бұрын
Are other ammonium quats suitable as a replacement for the cetrimide? Can you link to the source material about dissolving solder?
@charlesmayer5627 Жыл бұрын
how to recovery tin from solution brother?🙏🏻🙏🏻
@callmeadmin Жыл бұрын
Indium recovery! In modern solders, there can be indium and silver among other metals. Also some processors might contain indium. There can be quite a bit of indium in solder. Indium might become much more expensive, as it's production is only 1200t per year while silver production is around 25000t a year. There might be some indium in chemical wastes. I wonder if it is possible to recover either metallic indium or indium salts?
@quintonharvey1501 Жыл бұрын
Does the silver come off with solder and tin
@MrMegaMaui2 жыл бұрын
and then how do you make it fall?
@2001pulsar2 жыл бұрын
Why is the cetrimide orange colour? What else is in it?
@2001pulsar2 жыл бұрын
@@PickyPlans awesome. Thanks.
@kanedytham45972 жыл бұрын
please need help here in the uk the only product i can find with cetrimide in it is 3.0%concrete would that still work and also please also can you please do a video of you making ferric nitrate 78% please it would be a very big help
@kanedytham45972 жыл бұрын
@@PickyPlans thank you so much
@milangabriel2842 Жыл бұрын
I’m in same boat.did you find any solution?
@milangabriel2842 Жыл бұрын
Ii can’t buy nitric acid here…any advice?
@opposites-3699 ай бұрын
Can you DIY make some like gel flux to make lead solder fast melting on PCB? thx before 👍🏻
@royalrefining61822 жыл бұрын
Thank you for this video. Can you use electrolysis to get the tin back out of solution? Or would you eventually end up dissolving some other base metals in this process?
@royalrefining61822 жыл бұрын
@@PickyPlans thank you. I have accepted you. You can share your video links directly to the group if you like
@TonyCartel-xi8hf6 ай бұрын
Hi, can you use this solution without ferric nitrate, because is problem to make this or expensive to buy-it,,Why ferrite nitrate is needed for in the solution/ purpose of the ferric nitrate? THANKS IN ADVANCE BROTHER!
@PickyPlans6 ай бұрын
Yes you can remove it from the list. It's just used to remove the last thin layer of solder on the copper/ Solder forms alloy with copper with few micron thickness ferric nitrate removes that layer
@TonyCartel-xi8hf6 ай бұрын
Continu Your Awesome Work!
@ManMountainMetals2 жыл бұрын
Tin? I'm in!
@abdeljalilabdeljalil513520 күн бұрын
Can you explaine how to make a 15% cetrimide please
@PickyPlans20 күн бұрын
Not easy to make, try to get , polyquaternium 7 or 10 (used in making hair conditioner) it is much easier to get
@abdeljalilabdeljalil5135Ай бұрын
Do you think that i can loose some gold if i used urea based solution to grt rid of tin??
@PickyPlansАй бұрын
No , filter solution to get the gold
@abdeljalilabdeljalil513520 күн бұрын
Thank you very much@@PickyPlans
@Rei.dos.metaiesАй бұрын
Fiz aqui nítrico 3×1 está tendo resultado
@dirceudepin77552 жыл бұрын
Nice!
@kimloaiquy36412 ай бұрын
Thật là tuyệt vời ❤❤
@privateuser2463 Жыл бұрын
can you recover the silver out from out of the solder off the boards?
@Jibrannajam927 ай бұрын
If you use the HCL method, silver doesn't get dissolved in it, so it should most likely settle out to the bottom either as a fine powder or sludge
@julioperez8065 Жыл бұрын
Thanks
@khanacknowledge76045 ай бұрын
Sir, how long can I save it after making the solution? (cEtrimide base)
@PickyPlans5 ай бұрын
About 3-4 days and up to 7 days in cold place
@elnazkz2 жыл бұрын
the best vidio❤
@ssofmas84732 жыл бұрын
Hi we use just dilute HCL for tin and solder removal and use heat for acclamation reaction , this way you show is new and good info but I think too much expensive is it right? And we use 3 time diluted HCL for solder and Tin removal.Did you math how much your solution? And how many times can we use?
@Jibrannajam927 ай бұрын
Which boards did you use to depopulate? And how many times do you actually reuse your HCL solution for the same?
@julianalcorso57032 жыл бұрын
So sorry but I have one more question............ Would the Urea based solution have worked quicker if it were heated up or even boiled?
@julianalcorso57032 жыл бұрын
@@PickyPlans Thanks so much for your prompt reply! I will do a trial just warming it up to say about 80C while I source the Cetrimide. Keep up your great work!
@zero-waste2 жыл бұрын
@@julianalcorso5703. Most backyard refiners, at least those without any greater chemical knowledge, will benefit from doing things the old fashioned way. Remember KISS (Keep It Super Simple). Some processes may take a little longer, but they're simple and the chemicals are cheap. A two step process, first very diluted HCL and then diluted HNO3 will do the job. Electrowinning or carbon reduction will recover the metals. Full leaching process is described in my comment (3 parts) here: kzbin.info/www/bejne/i6bKoKV5mL14j9k .
@julianalcorso57032 жыл бұрын
@@zero-waste Thanks for the advice! I am a winemaker and therefore have studied and understand organic chemistry but this Ewaste recovery is fairly new to me. I agree with KISS!!! All I am trying to do is remove the remaining solder from several Kg of high-grade telecom pins. as well as the remaining solder from the boards (120Kg). I tried HCL but must have had it way too concentrated (1:1) What strength would you recommend? Once again thanks so much for your help!! BTW I am in Australia, You?
@zero-waste2 жыл бұрын
@@julianalcorso5703. You really should separate fully gold plated pins from those with only partial gold plating, and process them in two batches. Tin behaves odd in many ways. One of them is: If tin solder have been in direct contact with gold plated pins a phenomenon called metal diffusion have occurred. It's best illustrated if you use a cheap soldering iron with a copper tip. The tip becomes inevitably shorter and shorter as the tin solder absorbs a tiny part of the copper tip every time you use it. Therefore, the dissolved solder from fully gold plated pins do contain gold! Metal diffusion is the reason that a two step process is needed for complete removal of solder on Printed Circuit Boards. Many backyard refiners struggle with the last remaining solder on PCBs, i.e. the components will not fall off. A small part of the solder is encapsulated in the diffusion layer of tin/copper. HCl cannot dissolve copper, but HNO3 can. Read my three part comment for tin removal process here: kzbin.info/www/bejne/i6bKoKV5mL14j9k . Try it and leave a comment if you find it can be either simplified, or improved. After tin removal the electronic components can be sorted for further processing. The bare boards are processed for Bromine extraction, and pyrolyzed yielding raw fuel oil. Finally the copper is separated out. What remains is solely glass fibers, which have so little value that it's just given away for free to a glass recycler. I process any kind of low/med./high grade Printed Circuit Boards. Currently at least 3 tons in stock, but it's way too cold for chemical processes in the winter here; awaiting summer time. During many years I've traveled to many countries visiting numerous small and large recyclers/refiners, but still haven't been in Australia; it's pretty far from Denmark, actually half the way around the globe. However, as an avid sportfisher a trip to The Great Barrier Reef for big black marlin is tempting. If I decide to go to Australia it could indeed be very nice to pass by, and enjoy a glass of delicious Australian Full Bodied red wine while discussing e-waste recycling and recovery processes.
@julianalcorso57032 жыл бұрын
@@zero-waste Once again your link takes me to Omegageek64. A guy in Florida ????
@ba-uy7ft10 ай бұрын
bonjour. attention au condensateurs dans l acide ou chaleur ,risque explosion .bonne chance
@PickyPlans10 ай бұрын
🙏
@asosalam46522 ай бұрын
❤
@sherifaly1017 Жыл бұрын
رائع 👍🏾👍🏾
@Recycling-ey1yc Жыл бұрын
👍
@ChimeraChemLab10 күн бұрын
Чем опасен нитрат мочевины?
@PickyPlans10 күн бұрын
потому что это взрывчатый материал
@ChimeraChemLab10 күн бұрын
@PickyPlans Абсолютно нечувствительный ко всем видам воздействия, даже если выделить его из раствора