Sodium Nitrate Black Powder

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Everything Black Powder

Everything Black Powder

Күн бұрын

Пікірлер: 296
@paulkonowicz1740
@paulkonowicz1740 2 жыл бұрын
Your potassium based black powder (77g:13g:10g) has a molar ratio of 0.762:1.082:0.312 of KNO3 to carbon and sulphur. When you changed to Na based black powder you didn't take into consideration that the molar mass of NaNO3 (85 g per mole) is lower than KNO3 (101.1 g mole). The result is your black powder has more oxidiser (nitrate ion) present. The new molar ratio of nitrate:carbon:sulphur is 0.906:1.082:0.312. If you want to keep the ratio of oxidiser to carbon and sulphur equivalent to that for KNO3 you need to reduce the NaNO3 to 64.8 g (0.762M x 85) while keeping carbon at 13g and sulphur at 10g. An additional consideration is that NaNO3 is hygroscopic which is why KNO3 is generally preferred to prepare black powder. NaNO3 might be inferior to KNO3 for a reason other than an excess of oxidiser or moisture content. Beavis the organic chemist.
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Thank you, I’ve had a few people mention this. I’ll have to give it a try.
@paulkonowicz1740
@paulkonowicz1740 2 жыл бұрын
@@Everythingblackpowder You mentioned that the CIA method allowed you to increase the density of your KNO3 powder, but it uses water. It is probably better to use a dry process (few drops of water) because you won't have to worry if the powder is dry. However, it might be difficult to reach the density of the CIA prepared KNO3 powder and you will need to add more NaNO3 black powder. I hope you get better results.
@francisdec1615
@francisdec1615 Жыл бұрын
I have a composition here, but it might be for blasting powder: sodium nitrate 71%, charcoal 16.5%, sulfur 12.5%. But anyway, gun powder made of sodium nitrate is a bad idea, unless you can cover every grain with wax, as they used to do with NaNO3 based blasting powder. It's very hygroscopic, while KNO3 is almost non-hygroscopic.
@Troy-nr7ku
@Troy-nr7ku Жыл бұрын
Can you translate that into English? Lol layman's terms?
@JimJohnson-y7z
@JimJohnson-y7z Жыл бұрын
Potassium Nitrate in KNO3. Sodium nitrate is NaNO3. K is potassium. Na is sodium. NO3 is nitrate. So, they are essentially the same thing, except one has sodium in the place of the other's potassium. The thing is, potassium weighs almost twice as much as sodium. So, the same weight of sodium nitrate will have a lot more nitrate in it than potassium nitrate will. So, if your black powder recipe goes by weight, your sodium nitrate powder will have a lot more nitrate in it. Too much to ignite effectively, in fact. @@Troy-nr7ku
@bonetti4
@bonetti4 10 ай бұрын
Been making explosives since childhood and opened my own explosives company, gotta say I love your work and think you are doing a great job. Keep it up!
@Everythingblackpowder
@Everythingblackpowder 10 ай бұрын
Thank you
@mattbarnett9249
@mattbarnett9249 10 ай бұрын
You're welcome. I moved on to other explosives for commerce but we still make some on occasion and it's so refreshing to watch someone who really knows the art. Watching your videos is a great way to blow out the cobwebs, it's clear you love this and are a wealth of knowledge. @@Everythingblackpowder
@putteslaintxtbks5166
@putteslaintxtbks5166 2 жыл бұрын
If the cost is low enough on sodium nitrate, it is easy to turn it into potasium nitrate if you can find ice meld made of potasium cloride (think it's usually about $10 for 40 pound bag). Just add both of the about equel wt. of each in enough boiling water to let both desolve. Remove from heat and let cool. (Can filter out any dirt, etc, befor it starts to cool.) The sodium nitrate should now be sodium cloride (table salt) and remain desolved in the water and the potasium nitrate will start forming crystals and dropping to the bottom of the container. I think most should drop out at room temp, but would cool in the fridge to get a higher yeild. Now just filter the crystals out with coffee filter or fine cloth and a light rinse to get any salt water off. Dry. Sorry so long, didn't mean to write a book.
@putteslaintxtbks5166
@putteslaintxtbks5166 2 жыл бұрын
It was years ago and best to look this up befor doing it. I could be thinking of the wrong conversion!
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Fair enough. Thank you
@Nostradamus_Order33
@Nostradamus_Order33 2 жыл бұрын
Salt substitute in grocery store has KCl
@mrsmith9079
@mrsmith9079 2 жыл бұрын
I'd be very sceptical of that. Sodium, potassium, chloride and nitrate ions are all extremely soluble in water, wouldn't be convinced that this method would reliably allow ion exchange to occur.
@putteslaintxtbks5166
@putteslaintxtbks5166 2 жыл бұрын
@@mrsmith9079Right after posting that, if I know how, I would have taken it down, as I think what I was thinking of was sodium perclorate to potassium perclorate.
@tompowers8495
@tompowers8495 Жыл бұрын
Thank you for this excellent research. I pick up a few good tips from you and the comments that result. have dabbled in the art for 60 some years........always learning........
@zebdeming
@zebdeming 2 жыл бұрын
As far as the charcoal issue, cooking it at a high temp, and for a long time, it will cook off all the volatile compounds out. When I have made my own charcoal for iron smelting, if I fully cooked it, it would be much less dense, than if I shut down early. The charcoal that I made that was shut down early was much better for making the proper atmosphere in the smelting furnace to reduce the ore properly, I could never get the fully cooked charcoal to work right. Charcoal making is whole subject in itself, and one rabbit hole that you can go down for a long time
@308dad8
@308dad8 2 жыл бұрын
The slow flash in that long barrel is probably why it gave the better velocities, burning making gas the whole time the bullet is in the barrel instead of flashing off and bullet slowing down at the end of the barrel.
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
That’s an interesting theory
@adam-k
@adam-k 10 ай бұрын
I believe smokeless powder burns slower than black powder for this reason. This is also the reason why you use smaller grain black powder in pistols than in rifles. Smaller grain burns faster which is beneficial for shorter barrels. Would be an interesting experiment to find the perfect burn rate for a given rifle. Also ideally you would use a small grain fast powder for the flash pan and slow burning larger grain for the barrel.
@DreadX10
@DreadX10 3 ай бұрын
Was thinking along those lines too. The unburned powder-dust that gets pressed against the ball might help with the gas-seal too. With a fast flash, this would be insignificant but with a slow burn it might help enough to make a difference. But in any practical use, the water that creeps into the powder will soak up so much heat that it will underperform. Rule of thumb is that you would want to reach the 'all-burned' state when the bullet is about 2/3 up the barrel (and still has 1/3 to go). This is for smokeless powder and once 'all-burned' has been reached there is only gas in the barrel behind the bullet. The rule derives from the reasoning that that last bit of created gas (at the breech) creates a mini pressure-wave that must catch up to the bullet before it reaches the muzzle in order to contribute to the velocity of the bullet. The wave will travel at the local speed of sound inside the barrel. For black powder, the equations are not so simple as there are solid particulates and they are bound to interfere in the energy transfer through the system/barrel.
@lorenray9479
@lorenray9479 2 жыл бұрын
My retort is made from standard size propane tanks the burner is holey. A small wood rack and door cut and bolt, washer guides. I made a retort chamber above with a hole bottom center to help heat the burner. I cut a circular lid, cap, top hat. They are wrapped with tank sides bent to shape and spaced for a flame guide. It took 4 tanks for parts.I made a kiln brick covering to guide flame an inch or two around the retort, burner with air venting all round base. I heat with the bark sapwood scraps I cut at 10 inches x 1+ inches for retort wood. No bark or dirt for char wood. Stacked very tight in retort chamber it heats o2 free. When torching stops, I stop feeding the burner and let it cool of its own accord. The char is sparkly with only the very slightest hint of color. No wood left. I only have to keep the artists from taking the perfect charcoal.
@rolandlee6898
@rolandlee6898 2 жыл бұрын
Being called blasting powder might explain its intended use. Like in mining and such. It may burn slower in the open but works basically the same under compression and is cheaper to make, so a significant cost cut if you need a lot of it.
@1pcfred
@1pcfred 2 жыл бұрын
This guy is ahead of the curve.
@rre9121
@rre9121 2 жыл бұрын
This stuff is awesome somewhere between experimental archeology and learning new stuff entirely. Thank you for the videos.
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Happy to help.
@dp-sr1fd
@dp-sr1fd Жыл бұрын
I read an article about Swiss Powder which said that the charcoal was made from wood that had been weathered for two years in the forest where it was gathered before being processed into charcoal. If you think about it the purity of sulphur and saltpetre is pretty much constant, the greatest variable is the charcoal. Also the very high pressure that the mix is subjected to by the rollers before being granulated may make a difference. Weight for weight the Swiss powder seems to occupy a smaller volume so has a greater density.
@HabeasJ
@HabeasJ 2 жыл бұрын
"Antique muzzleloading propellant." Yep, that warrants a subscription lol
@DreadX10
@DreadX10 3 ай бұрын
Yep, and the disappearing 'subscribe' trick helped as well!
@crohkorthreetoes3821
@crohkorthreetoes3821 2 жыл бұрын
I could be way off, but.... If I recall correctly, pushing super heated steam through the charcoal is how you make activated carbon. So.... activated carbon is gonna be pretty clean. Maybe that is the trick to clean burning charcoal....
@HoffmanReproductions
@HoffmanReproductions 2 жыл бұрын
Very interesting findings! Thanks for sharing Jake!
@averagenobody6577
@averagenobody6577 2 жыл бұрын
Just discovered your channel. It was cool to see a vid on something I'd never heard of before.
@petruse8893
@petruse8893 2 жыл бұрын
The key word is hygroscopic. If one looks at potassium/sodium nitrate formulas it is obvious that at any given weight sodium nitrate is " richer" in nitrate anions than potassium nitrate ie it will have more oxygen to supply.This being said,sodium nitrate powder is good to use while shooting in Sahara desert,completely worthless in Florida.Long time ago ,in 19th century,right before the first world war, there were promising experiments with ammonium nitrate as an oxygen donor and charcoal only.the composition lost to smokeless powder, which turned out superior to any powders based on solid ingredients
@richbattaglia5350
@richbattaglia5350 2 жыл бұрын
What information do you have on ammonium nitrate and it’s use in firearms? Also did I read your comment right, ammonium nitrate and charcoal only? This would be huge if you could cut sulfur out of the mix as it’s the most difficult material to acquire in BP production.
@hanelyp1
@hanelyp1 2 жыл бұрын
As I understand, potassium nitrate+charcoal gives good energy. Sulfur makes it easier to ignight.
@adventureswithfrodo2721
@adventureswithfrodo2721 2 жыл бұрын
I don't think you really understand what your talking about.
@dopeymark
@dopeymark 2 жыл бұрын
I'm assuming because ammonium nitrate is extremely hygroscopic as well. It used to wind up as giant clumps in the sealed bag on our farm when I was a kid.
@dwwolf4636
@dwwolf4636 2 жыл бұрын
@@dopeymark And the pressure gradient is different upon detonation. Be wary with firearms certified for BP use while using AN.
@terryqueen3233
@terryqueen3233 2 жыл бұрын
Excellent! Thanks for testing all that for a certainly appreciate it I do anyway. Have a great day and stay safe and keep your powder dry!
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Thank you
@TheErilaz
@TheErilaz 2 жыл бұрын
You can get 1900 feet per second with black powder,- but that involves the old English Black powder express rifles. As a example: The energy requirement for big game in Norway is: 1) for bullets with a weight of 138.9 to 154 grains, the estimated energy is at least 2700 joules at 100 meters E100 2) for bullets with a weight with a minimum of 154 grains, the estimate energy is minimum, 2200 joules at 100 meters. E100 Conclusion: One must have a minimum speed of 400 m/sec (at 100meters ) and a ball weight of at least 450 grains to cope with the energy requirement on big game. (2233 Joule E100 for those wondering). That is possible with: .45-120 ( 500 grains bullet, 463 m/sek 1519 ft/sec) .50-140 Sharps English cartridges: .450 Black Powder Express .461 (.450) Gibbs .500 BPE ( 440 grains bullet ,580 m/s 1902 feet/sec) .577 BP Express .500 No. 2 Express (.577/.500) 340 grains bullet 130-160 gr Fg swiss ,587 m/s 3,800 J . Scottish bottleneck: 20/577 Alexander Henry, 570 grains bullet, 1,725 ft/s (526 m/s). Speeds above 600 m/sec is extremely hard to obtain with black powder.
@keiththomas3141
@keiththomas3141 2 жыл бұрын
I wonder since the sodium nitrate burned slower it continued burning further down the barrel giving it some extra velocity at the end.
@HobbiesHobo
@HobbiesHobo 2 жыл бұрын
Interesting test Jake! I'm really liking this stuff. Learning a little bit more all the time. Hope you have this video & data all backed up somewhere just in case. Thanks , Mike.
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Thanks Mike!
@Jagdtyger2A
@Jagdtyger2A 2 жыл бұрын
Try converting your charcoal into activated charcoal or not fully carbonizing the charcoal. I heard that in the Civil War and just before smokeless powder became common, that something called "Brown Powder gave superior performance in cannons
@chemistryofquestionablequa6252
@chemistryofquestionablequa6252 2 жыл бұрын
Try drying your sodium nitrate before making the powder, and dry the powder just before glazing. Otherwise you're going to get inaccurate measurements of the nitrate, and powder that's way more damp than you want. Both will really effect performance. It would be the same with ammonium nitrate because both are really hygroscopic.
@loquat44-40
@loquat44-40 2 жыл бұрын
When i was an adolescent back in the 1950's we used to mix drug store purchased saltpeter and mixed it 50-50 with standard supermarket purchased white refined sugar, likely cane sugar. It picked up water from the atmosphere very quickly. I once did try it in an open pipe to fire a bolt. It did, but was so badly fouled that subsequence shots were not possible. I used a piece of jetex fuse for ignition.
@jeanladoire4141
@jeanladoire4141 2 жыл бұрын
I'm using sodium bp because i can't find easily potassium nitrate. If the ball isn't rammed super tight, with the low ignition speed, it sometimes puffs without actually detonating. But if you really ram the ball well, it will just pop like one hell of a baloon. With a percussion cap and a well pressed ball, you got no delay, not much smoke and quite nice power. And it's cheap and easy to find (stump removers manufacturers usually put sodium nitrate beacause it's cheaper)
@donaldcadwell3911
@donaldcadwell3911 Жыл бұрын
Look for stump remover powder in garden section of many stores.
@jeanladoire4141
@jeanladoire4141 Жыл бұрын
@@donaldcadwell3911 most of the stump removers are made with sodium nitrate, beacause it's cheaper than potassium. And that's exactly where i got my ingredient
@donaldcadwell3911
@donaldcadwell3911 Жыл бұрын
@@jeanladoire4141 Spectracide is brand we have that is Potassium nitrite.
@jeanladoire4141
@jeanladoire4141 Жыл бұрын
@@donaldcadwell3911 it doesn't exist in France sadly. But sodium nitrate work well, it was used before,but will behave like old gunpowders : you have to ram it tight for it to detonate
@donaldcadwell3911
@donaldcadwell3911 Жыл бұрын
@@jeanladoire4141 👍
@SolarSeeker45
@SolarSeeker45 2 жыл бұрын
If you want a super clean burning black powder use lampblack instead of charcoal.
@chopsddy3
@chopsddy3 2 жыл бұрын
Good info .👍 Could Swiss be cleaning the residual oils out of the charcoal ,at some point in the process, then re drying? Maybe hitting it with a blast of steam? It’s obviously not just the species of wood chosen for the char. There’s a freakish absence of funk on those Swiss patches. Other than an additional oxidizer, it must be the cleanliness of the charcoal. I’m thinking residual oil in the charcoal, like creosote in a chimney, is what is making the funk.
@juriehuman7127
@juriehuman7127 2 жыл бұрын
Activated Charcoal ?????????
@andrzejsobanski6752
@andrzejsobanski6752 Жыл бұрын
@@juriehuman7127 Activated charcoal makes for shitty powder, so that's not it.
@woodrowbrimm2805
@woodrowbrimm2805 Жыл бұрын
Sodium Nitrate is also called "Chilean Saltpeter"as it was found in Bat Caves in Chile and used for making Black Powder. It is more Hygroscopic than Potassium Nitrate,this means it absorbs moisture from the air more readily so it's harder to keep your powder dry .
@iskandartaib
@iskandartaib 2 жыл бұрын
One wonders how ammonium nitrate would work. Available as fertilizer. The folks in NE Thailand who make the giant PVC skyrockets (look up "rocket festival" on KZbin) use, I believe, some sort of meal powder based on ammonium nitrate and charcoal, no sulfur - it burns really slowly from what I understand. I remember making some sodium nitrate based meal powder when I was in school, we packed it into a cardboard cylinder, thinking to make a rocket, but it just burned really slowly and produced a whole lot of molten slag dripping out the bottom. One wonders what makes up fouling - part of it is probably a salt or oxide of the metal used in the oxidizer, which makes me think ammonium nitrate would make less fouling.
@senorjp21
@senorjp21 2 жыл бұрын
The molecular mass of KNO3 is 101 g/mol and NaNO3 is 85 g/mol. The 75:15:10 ratio will need to be adjusted. For equal weights of KNO3 and NaNO3, the NaNO3 will contain more oxygen.
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Yeah but it’s hard to argue with results
@Everythingblackpowder
@Everythingblackpowder 5 ай бұрын
Theoretically 😉
@pyrocircus129
@pyrocircus129 Жыл бұрын
I have used Sodium Nitrate in fireworks but not for a lift charge. Never heard about the theory of cooking your charcoal to hot but what if you get it over a certain temp you loose some volatile compounds that are present in the wood? Interesting!
@thinkingbill1304
@thinkingbill1304 2 жыл бұрын
Side note. Even though here in Ks we have gotten some rain, indoors it is bone dry. So, almost three weeks ago I took an H&R Topper 088 to a friends B-Day party. High school kids took some turns with it on clays. The load was Magtech brass, 3 1/8 dram Goex 2Fg, 1 1/8 #8. Big fun! About 30 shots. Anyway, this, that and the other I just cleaned it yesterday. No rust. It cleaned up spotless. Granted the fouling was extra hard. What I'm getting at, BP with KNO3 in dry conditions with non-corrosive priming isn't that big a deal ( it is, but it isn't....). It would be interesting to know if like amounts flashed on some steel plate of potassium nitrate vs sodium nitrate and left in the weather changed this dynamic.
@308dad8
@308dad8 2 жыл бұрын
I have personally noticed that Goex is a little smokier than pyrotechnics but a lot less corrosive. I know “it’s not corrosive it’s hygroscopic”. Fact is if I shoot 1 shot with pyrodex Ivette’s scrub the whole gun within hours. If I use BP I can go the whole weekend or week before it looos as bad as 1 day with pyrodex. That’s here in the south with high humidity. Both stink when burned so pyrodex only exists because the stores don’t need “explosives like licenses to have it.
@MattRios-jn1qx
@MattRios-jn1qx 17 күн бұрын
Excellent show. And I always wondered about using sodium
@scottmarshall6766
@scottmarshall6766 2 жыл бұрын
Seems like your rifle is fusing and that's adding to the slow ignition. Cut back on the priming charge, and tip the gun to the right just before shouldering to knock the prime away from the flash hole. It seems as though your flash hole may be a tad large as well. I shot competitively for 30 odd years, and these are a few things I picked up along the way. Apologies if you're familiar with these tricks. Swiss has been a tad more energetic and easier to ignite than Goex for many years, I've heard a lot of theories as to why, but none have been proven. Goex is more uniform, especially the 3F sporting. The best one for fouling control depends on conditions. With the high price and spotty availability of Swiss, I usually opt for the Goex. A lot of different oxidizers have been tried in black powder thru the years, but we always seem to come back to the old formula and methods. Excluding the newfangled nitro stuff, which I'm sure is just a passing fad... Interesting stuff!
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
The lock on this rifle is timed very well and always goes off fast when using any potassium nitrate based powder. The sodium nitrate flashes extremely slow in open air. I couldn’t agree more, smokeless powder is over rated
@zyklon2000
@zyklon2000 2 жыл бұрын
I switched from lead to 316 stainless steel in my mill many years ago. Much cleaner and so far no unwanted ignition
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Lead works fine for me.
@willowpine2604
@willowpine2604 2 жыл бұрын
@@Everythingblackpowder thats true and safe but as you mentioned you have issues with your performance (feets per second) in your rifle! One issue with lead ball media is that leaves traces of lead and contaminated the end product ! As for the charcoal process about cooking is: first you use paint can and paint can leave behind trace's of iron oxides in your charcoal ! Second: as i see you don't leave it until the fire completely disappeared which leaves behind uncarbonised wood and fuel properties in you wood! Third: of course the wood choice is the main and first factor BUT!! The correct time to harvest you tree is during the winter between mid January and beginnings of February because then the tree have take all the minerals and moisture down to the roots for protection from the winter ! Four: the cooking process needs to be at 550°F Fahrenheit or 285°c Celsius and completely cooking until the fire end's! I know a lot of process but swiss goex and other brands live with this job! Of course other factors effect the end result ( right corning( 1.7cc density or more) , correct ratio's , milling time, completely pure chemicals, etc) I hope i helped!
@davefellhoelter1343
@davefellhoelter1343 2 жыл бұрын
I "Wounder If" the speed may be In the Burn "type" with the longer barrel. could it be a better Push for a more complete burn rather than a bang? Did you notice a change in Sound? Sounded on the interweb more thump-ish? I did notice your flash looked and sounded FAST enough with a Nice Plume as should be. I noticed a change in sound with BP in some applications, rather than a crack more of a Boom! AND I noticed the CONSTANT speeds, so is fast better than consistent? I do KNOW in "reloading" the quest of the Holy Grail is "consistency" for ACCURICY. I'm On It too! Keep your smoke Pole SMOKING! Thanks!
@richbattaglia5350
@richbattaglia5350 2 жыл бұрын
I’m liking the new intro. With regards to the charcoal issues you may want to consider harvesting the wood during spring as the sap from the trees holds less inorganic matter which could weaken the ignition. If you’re going the distance season the wood for 18 months, but no more than 3 years. Long term play, but it should pay off. Cook times for willow charcoal ought to be 3-1/2 hours at 280 degrees Celsius. This information is provided with greater detail with Explosives their manufacture, properties, and history by Arthur Marshall 1915. I look forward to seeing your developments.
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Thank you!
@mlytle0
@mlytle0 2 жыл бұрын
NaNO3 has more oxygen by weight, so could burn the combustibles more completely. Possibly could get even higher muzzle velocity if the proportions of sulphur rand charcoal were increased slightly to take advantage of the higher oxygen provided. Union army used Chilean sourced Sodium Nitrate to make gunpowder since the KNO3 sources had previously been bat guano based from caves in the American South, and reported higher performance in cannon.
@archangel20031
@archangel20031 2 жыл бұрын
Smokeless Gun Powder burns really slow, but under pressure, it burns much faster. This slow burning black powder might also burn well under pressure.
@Godwh1sperer
@Godwh1sperer 2 жыл бұрын
If i may request to make it harder still: sulfurless 100% sodium powder.. can you make it work? In theory it should, in practice it probably takes serious powder making skill to make it work, making the video even more interesting. Given the higher energy per grain but the greater reluctance of it, it can give lower lows and set higher highs in terms of velocity.
@jokercortez607
@jokercortez607 10 ай бұрын
You make black powder look fun I've been thinking about trying it out
@Mr-Highball
@Mr-Highball 2 жыл бұрын
I still dont have a use (yet) for _"Antique muzzle loading propellant"_ but I really enjoy the detail and the quality of your videos
@kozakzenyk5511
@kozakzenyk5511 2 жыл бұрын
Just a thought: Maybe the lead in the ball mill are to blame for the stronger fouling? Since lead is quite soft and the milling may wear away some of it. Perhaps trying an alloy of lead/tin (Pb40/Sn60; Pb30/Sn70), which is much harder than lead itself may solve the problem.
@wijpke
@wijpke 2 жыл бұрын
It has more oxygen in it so you can use less of it to counterbalance its hygroscopic nature also you can coat it with dope the grains to make it less hygroscopic
@joeyhardin1288
@joeyhardin1288 2 жыл бұрын
Were antioxidizers used back then: as in cooking the charcoal in Nitrogen? But then, on what scale? God Bless and stay safe.
@wijpke
@wijpke 2 жыл бұрын
If you wash the charcoal with rain water you can reduce the fowling doping is done with nitrocellulose to make it less hygroscopic and use about 10 %less sodium nitrate to have the same oxygen balance
@michaellebert8907
@michaellebert8907 11 ай бұрын
hygroscopic also means you can rinse it from soil easily, making it readily available. There is actually a military field guide on how to extract use it just as you are.
@phyllisbrooks9149
@phyllisbrooks9149 2 жыл бұрын
Brother, have you ever tried ammonium nitrate powder? I heard that the powder of ammonium nitrate and charcoal can reach the energy of double-base gunpowder?
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
I haven’t tried it
@stephenhumphrey7586
@stephenhumphrey7586 2 жыл бұрын
Ammonium nitrate runs into same problem as NaNO3, it's much more hydroscopic
@CSGATI
@CSGATI 2 жыл бұрын
Use stoichiometry if you want it to burn clean. Slow burn, longer push.
@MuskratOutdoors
@MuskratOutdoors 2 жыл бұрын
Not bad at all. That first load sure had terrible lock time!
@ChrisGilliamOffGrid
@ChrisGilliamOffGrid 2 жыл бұрын
Imagine finding you here. 😉
@markcantemail8018
@markcantemail8018 2 жыл бұрын
Is Goex being produced again in May 2022 ? I assume that you were using Stock on Hand . I enjoyed your test and carefully showing the results . Thanx .
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Thank you! Check out Ethan’s channel @ilovemuzzleloading he’s been keeping up to date on all the news going on with Goex.
@markcantemail8018
@markcantemail8018 2 жыл бұрын
@@Everythingblackpowder Great , I took a peek at the May 6th Video . Thank you for the Reply .
@deandeann1541
@deandeann1541 2 жыл бұрын
Sodium nitrate absorbs water like crazy compared to potassium nitrate. It is likely that your NaNO3 black powder was slow because of water content - it needed dehydration.
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
It flashed slow. It didn’t make slow velocities. We stored the sodium made powder in a sealed container full of silica gel desiccant balls. We are doing an experiment now where we are placing are finished powder in a vacuum chamber with desiccant for a week to see if it has any effect on performance.
@deandeann1541
@deandeann1541 2 жыл бұрын
@@Everythingblackpowder NaNO3 neds to be dessicated before it is measured for powder - it holds so much water it can throw the proportions all off -eg if the NaNO3 is 10% water by weight then you end up making the powder with 10% too little nitrate. On top of that, the water in the powder can itself affect burn rate. Weigh the nitrate before and after dehydration (I use a food dehydrater for about 5 hrs at 150 degrees for the ingredients, not the mixed powder), you'll see how much of the nitrate was water, it can be surprising. The powder will also pick up moisture from the air unless it is sealed in storage.
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Very interesting. I hadn’t thought of dehydrating the sodium before hand. Thank you!
@Strike_Raid
@Strike_Raid Жыл бұрын
Sodium Nitrate is highly hygroscopic; you need to bake out the water and then make sure it isn't exposed to air to reabsorb water. That would be difficult, but unhydrated Sodium Nitrate is probably a better oxidizer than Potassium Nitrate.
@idontknowmyfirstname69
@idontknowmyfirstname69 10 ай бұрын
I was just starting to write the same thing good thing i went back and double checked. Someone wrote it a lot better than i started to. So I'll just do a condensed version so i can still get at ny point. I use nitrates for making nitric acid i use in precious metal refining. I prefer sodium nitrate to potassium nitrate as pound per pound you get a higher percentage of the weight made up by the nitrate anion on account of using the lighter weight sodium cation opposed to the heavier potassium cation. In this case the anion is the good stuff its use in black powder is no different. Now you also got to keep in mind that the sodium nitrate also has a bit of an affinity for water.s getting it completely dried out anhydrous is very difficult and then it will also literally suck water up out of the air the more water you got in your powder you do the math. I imagine using it for black powder it won't store very well, especially so in a more traditional type of container like a powder horn
@PackthatcameBack
@PackthatcameBack 2 жыл бұрын
I saw someone once use scraps of leather to make the carbon. Wonder how that would work in black powder?
@johnmace6355
@johnmace6355 2 жыл бұрын
You seem like the perfect person to ask this. I’m looking to have a sort of off grid formula for black powder. I’ve seen people posting about making BP without sulfur. Is that possible and would it be able to be used in a BP rifle or pistol? Any help with this would be appreciated. Keep up the cool content.
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Yes, I know it’s possible but I’ve never tried it myself.
@schinderiapraemeturus6239
@schinderiapraemeturus6239 2 жыл бұрын
recipe for Blue MZ- 50% KNO3, 25% KCLO4, 20% sodium benzoate (food preservative, find on Ebay), 5% dextrin
@nunyabidniz2868
@nunyabidniz2868 2 жыл бұрын
Sulfur decreases the ignition temperature and increases the burn rate [transfer across grain boundaries.] Don't bother making 0 sulfur BP if you're going to try to use it in a rock-lock; same reason none of the substitutes are suitable for priming the pan in a flinter. But you absolutely could use it for the main charge, it will just burn a bit slower [ie, use 3F where you'd use 2F of BP w/ sulfur, etc.]
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
I’ve got some powder made up without sulfur and hope to try it this weekend. Stay tuned!
@Don.E.63
@Don.E.63 2 жыл бұрын
Interesting test, it seems like it performed more like a slow burning smokeless rifle powder would to obtain the higher velocity, enjoyed the video.
@TUCOtheratt
@TUCOtheratt Жыл бұрын
Another great video! I bet you get a little tired of hearing so many expert opinions in the comments.😃
@Everythingblackpowder
@Everythingblackpowder Жыл бұрын
it’s all part of the show
@khester7397
@khester7397 Жыл бұрын
One things certain; he never tires of shameless sycophants nuzzling his butthole.
@davefellhoelter3299
@davefellhoelter3299 11 ай бұрын
I recently found taking the BARK off to the heart wood made "MY AMP" better faster cleaner? Just got some green sapling shoots from my Mexicola Avocado(look like egg plant! GOOD) in my char batter's box! I use the same CAN! would we consider glazing our Sodium Nitrate with Lamp Black?
@willywantoknow2563
@willywantoknow2563 5 ай бұрын
As far as your making charcoal my mind is contemplating the nutrient minerals within each plant based carbon that would give each charcoal a different effect. Why is willow dirty and balsa not as much? Based on your studies, do you have a chart made? Dirtiest - cleanest Weakest - most powerful Puting it on a graph with coefficients of mill time would be a very valuable chart.
@MrPanchoak
@MrPanchoak 2 жыл бұрын
Now THAT was very interesting Like you, I prefer flintlocks. Soo, saltpeter for my powder. But if the cleaning is better with a higher sodium/saltpeter ratio. It would still beat Pyrodex by a mile, and might even be ideal for cartridges.
@quint3ssent1a
@quint3ssent1a 2 жыл бұрын
Love how he constantly says "antique muzzleloading propellant", because saying some things out loud is very UNWISE.
@schinderiapraemeturus6239
@schinderiapraemeturus6239 2 жыл бұрын
propellant made with sodium nitrate will be very hydroscopic, eventually not fire due to moisture absorption. suggestion-get some potassium chloride water softener salt along with this NaNO3 and do a replacement reaction: NaNO3 + KCl ---NaCl + KNO3
@SW-ii5gg
@SW-ii5gg 2 жыл бұрын
I read potassium hydroxide for making your own from compost, will that also do the exchange?
@schinderiapraemeturus6239
@schinderiapraemeturus6239 2 жыл бұрын
@@SW-ii5gg no because sodium ion is more electronegative. sodium and chloride have a stronger affinity for each other-the reaction between KCL and sodium nittate is called a double replacement. KCL is cheap-snow melt and water softner. Cheers
@SW-ii5gg
@SW-ii5gg 2 жыл бұрын
@@schinderiapraemeturus6239 thanks for the explanation, cheers.
@djidh8476
@djidh8476 2 жыл бұрын
Why do i produce much residue when i make mine? i followed the exact same steps as you and same ingredients but still has a lot of residue
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
What do you mean by residue? Do you mean fouling?
@mfallen6894
@mfallen6894 2 жыл бұрын
Damn, I didn't know you could achieve those velocities with black powder, especially round ball (though I assume it sheds velocity extremely fast?) One of my favorite "plinking" loads for my Marlin 1894 (.44mag not .44-40 so .429-.431in, not a true .440 of a .44) is a 248gr flat-nose over 21.5gr of 2400. I think the last run I made averaged 1689fps over 10 shots from a 20" barrel, so I'd say that's pretty analogous. At least that WAS one of my favorite loads, in the before times when I could still find smokeless powder and primers... Getting really low on both so I might have to pick up a muzzle loader in order to be able to take a deer in the next few years! I know the cost of big bore revolver/lever gun factory ammo has doubled since 2019, $70 for a box of Fiocchi .44mag 240gr JSP's when I was getting them for $33 not even three years ago, so if this bs continues I honestly might have no other choice than to move to muzzle loaders. Got plenty of M80 ball 7.62 NATO, but I doubt that's a very good deer round, lol
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
there’s a few reasons why I get good velocities. One is that the round ball is lighter, roughly 140gr. Also the barrel length is a big contributing factor being 44 inches to your 20 inch carbine. I typically only run the best black powder I can make/obtain in this rifle and can get a little over 2000fps with a 75-80gr charge but I usually only do that for long distance shooting (Over 200 yards) I was testing some 44mag handloads last weekend and I settled on 23.5gr H110 with a 240gr JHP. they averaged 1400fps out of my Ruger Blackhawk, 7.5 barrel.
@TheErilaz
@TheErilaz 2 жыл бұрын
You can get 1900 feet per second with black powder,- but that involves the old English Black powder express rifles. As a example: The energy requirement for big game in Norway is: 1) for bullets with a weight of 138.9 to 154 grains, the estimated energy is at least 2700 joules at 100 meters E100 2) for bullets with a weight with a minimum of 154 grains, the estimate energy is minimum, 2200 joules at 100 meters. E100 Conclusion: One must have a minimum speed of 400 m/sec (at 100meters ) and a ball weight of at least 450 grains to cope with the energy requirement on big game. (2233 Joule E100 for those wondering). That is possible with: .45-120 ( 500 grains bullet, 463 m/sek 1519 ft/sec) .50-140 Sharps English cartridges: .450 Black Powder Express .461 (.450) Gibbs .500 BPE ( 440 grains bullet ,580 m/s 1902 feet/sec) .577 BP Express .500 No. 2 Express (.577/.500) 340 grains bullet 130-160 gr Fg swiss ,587 m/s 3,800 J . Scottish bottleneck: 20/577 Alexander Henry, 570 grains bullet, 1,725 ft/s (526 m/s). Speeds above 600 m/sec is extremely hard to obtain with black powder.
@Vishal.456
@Vishal.456 2 жыл бұрын
Hello sir I make my black powder out of potasium nitrate that usually done . But the problem with this It catches moisture in gun s breech .so i decide to take about 70 grains of powder and put in a thin layer of plastic paper and roll it down to barrel s breech .it works pretty good and same without any moisture problem.but sir I have question for you this method is good for accuracy or ballastics ? Thanks sir
@pa-pyro2804
@pa-pyro2804 2 жыл бұрын
It's nice in a few glitter star formula for fireworks
@FordGTmaniac
@FordGTmaniac 2 жыл бұрын
Would any of the perchlorates make good black powder? Nitronium Perchlorate in particular looks to be really damn powerful from what I've read, but I've also been told that perchlorates in general don't play well with Sulfur, as it makes them rather unstable.
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Mixed with sulfur it would be percussive and potentially unstable but It could be used with sulfur free black powder
@samellowery
@samellowery 2 жыл бұрын
Great info like always 👍
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Thank you
@OddBall1958
@OddBall1958 Жыл бұрын
Have you tested Potassium nitrate and sugar AKA rocket candy? Along with your other ingredients of course.
@gmacka6333
@gmacka6333 9 ай бұрын
Most "blasting powders" seems to burn just as slow. Its good for stuffing into a drill hole in rocks to blast them apart while chasing a quartz vein
@7come11two
@7come11two 2 жыл бұрын
The sodium nitrate powder should work fine in cartridge guns. Centerfire primers should set it off really well.
@Diogenes425
@Diogenes425 Жыл бұрын
What about using bamboo charcoal like the inventors of BP?
@loquat44-40
@loquat44-40 Жыл бұрын
When we were young as kids some of us would mix drug store purchased saltpeter with sugar 50-50 and it picked up water very quickly. I once tried make a homemade match lock and got off only one shot using conduit and a bolt for a projectile. It was too badly fouled to really fire efficiently again.
@tomsanders9491
@tomsanders9491 2 жыл бұрын
Curious if magnesium nitrate would work
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
I don’t know
@strangleholdoutdoors
@strangleholdoutdoors 8 ай бұрын
What was the normal setup for a rifleman? Horn and bag on right side or left side? Stances and procedures?
@dj1NM3
@dj1NM3 11 ай бұрын
It seems like the 100% sodium powder really requires compression/confinement and that might be why it was so slow (was that really 1/4 second between flint-strike and firing?) as priming powder?
@Everythingblackpowder
@Everythingblackpowder 11 ай бұрын
Yep
@jtcustomknives
@jtcustomknives 2 жыл бұрын
Makes me want to try the sodium powder in my cva wolf with 209 primers.
@tomhysell596
@tomhysell596 2 жыл бұрын
How does it work if you leave it in a fine state instead of kernelling it?
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
It works alright but it’s not as powerful
@HugoSixx
@HugoSixx 2 жыл бұрын
Hi, I made black powder following your advice on how to prepare it and the only thing I need to do is to compact it with a hydraulic press. The black powder I made burns at a similar rate to pyrodex. I made the granulation from 3f. Can it cause any damage to the rifle if I load it with this powder?
@loquat4440
@loquat4440 3 ай бұрын
As a teenager some of us to mix when 50-50 sodium saltpeter powder from the drug store with sugar and use a jetex fuse in piece of pinched off electrical conduit at both ends to make a bang. I tried it in a homemade cap lock and it was only effective for the first shot. After that there was too much fouling.
@andyd2960
@andyd2960 2 жыл бұрын
Have you tried making brown powder? From what you described, it sounds like Swiss powder is doing something similar.
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Not yet
@randywollin5732
@randywollin5732 Ай бұрын
I see some things that you have probably already answered for yourselves but I'm just not sure of the amount of powder you shoot with. You say with 50 grains but is that a right amount. I ask because I shoot 70 or more in my Kentucky 45 cal cap lock. Have you done a speed test that shows you the best charge or a bed sheet test or anything. I don't have a chronograph to test that. I have shot up to 120 grains just for fun but I don't plan to use more 80 in the future.
@generoll4027
@generoll4027 2 жыл бұрын
it's my understanding that Sodium Nitrate is hygroscopic and is difficult to keep dry.
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
Correct
@blok_pitaniya_460_watt
@blok_pitaniya_460_watt 11 ай бұрын
подскажите какой уголь лучше подходит для дымного пороха? какое дерево нужно?
@dougpruden9019
@dougpruden9019 2 жыл бұрын
cook your charcoal at a lower temp. Should have a brownish color to it.
@Nostradamus_Order33
@Nostradamus_Order33 2 жыл бұрын
K is more reactive than Na. At least, that’s what the periodic table of elements say?
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
It’s hard to argue with results
@Nostradamus_Order33
@Nostradamus_Order33 2 жыл бұрын
Are cool packs an easy source to obtain NaNO3?
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
I buy it from Amazon. It’s pretty cheap
@DenizKoksal.
@DenizKoksal. 2 жыл бұрын
Are there any disadvantages to using sodium nitrate instead of potassium nitrate? Or would they both do the same thing?
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
If you’re using a firearm that takes a cap, it’s pretty much the same. It doesn’t work so well in a flintlock
@DenizKoksal.
@DenizKoksal. 2 жыл бұрын
@@Everythingblackpowder Got it sir, thank you. I intended to load 410 cal cartridges...
@surfnblues729
@surfnblues729 2 жыл бұрын
Will this work in cartridges like 45-70 or 45 colt?
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
I haven’t tried it yet but I don’t see why it wouldn’t.
@deanshowers3386
@deanshowers3386 Жыл бұрын
Can you do this in cartridges and compare to your willlo black powder?
@Everythingblackpowder
@Everythingblackpowder Жыл бұрын
Good idea
@pixelpatter01
@pixelpatter01 2 жыл бұрын
You might have to change up your ratios to get the best results. Sodium Nitrate has more oxygen per part by weight than Potassium Nitrate. Sodium's Atomic Weight is 23 and Potassium's Atomic Weight is 39. The Atomic Weight of a Sodium Nitrate molecule is 85 while the Atomic Weight of a Potassium Nitrate molecule is 101. Thus using the Sodium salt you get almost 19% more oxygen for the same weight of Potassium Nitrate.
@erickdupont4503
@erickdupont4503 Жыл бұрын
Hygroscopic calcium and sodium tend to cake up and burn time lags behind something fierce
@TrashPanda71
@TrashPanda71 Жыл бұрын
What is the fastest powder one can make as easy as std BP ? Looking to replicate a BlackCat firecracker as much as possible. Id still need a ball mill.. whats the best ingredients and ratio. Ive been doing binary with premade alum powder, looking to get a ball mill and step it up to something more energetic..
@Everythingblackpowder
@Everythingblackpowder Жыл бұрын
I would use KN03 instead of sodium nitrate. I use a ratio of 77/13/10
@TrashPanda71
@TrashPanda71 Жыл бұрын
@WillardMcBain 77,13,10 is what I ended up on after reading more. But being in a high humidity area how bad is it for absorbing moisture ? I know it's not as bad as the SN but I have to deal with it constantly with the Potassium Nitrate and Aluminum based stuff.
@Everythingblackpowder
@Everythingblackpowder Жыл бұрын
@TrashPanda71 that’s all part of the show. I live in the south west so the humidity isn’t really a problem for me but the SN is much worse that KN03
@TrashPanda71
@TrashPanda71 Жыл бұрын
@WillardMcBain I've also been looking at Flash Powder, much easier and very energetic, but must be extra careful with it. 7 grams of Potassium Perchlorate and 3 grams of Black Aluminum that I've bought before for the binary ..
@Everythingblackpowder
@Everythingblackpowder Жыл бұрын
@@TrashPanda71 never made that
@1885win
@1885win 2 жыл бұрын
Perfect!
@551taylor
@551taylor Жыл бұрын
Because of the IRA, publicly available nitrates are now treated with a fire retardant and a chemical signature so that unlicensed people cannot make explosives with them. Untreated prills should only be available to the quarrying and demolition professions. As for charcoal, there are two types: normal and activated. Activated charcoal is the type used in water and respirator filters and has nano tubes in the makeup to absorb moisture… check them out for more info.
@Everythingblackpowder
@Everythingblackpowder Жыл бұрын
I don’t know what country you live in, but we don’t have that trouble around here.
@missingthe80s58
@missingthe80s58 2 жыл бұрын
My tests with Sodium based oxygen were identical save that mine was trash garden stuff. Lots of junk in it, only like 95% and the rest just whatever. It left a lot of crap behind. The witness plate tests suggested a poor performer but the chronograph and my shoulder said otherwise. Dirty but stupid fast.
@Everythingblackpowder
@Everythingblackpowder 2 жыл бұрын
It’s not worth a damn in a flintlock, it flashes to slow. I don’t care how fast the ball is moving.
@missingthe80s58
@missingthe80s58 2 жыл бұрын
@@Everythingblackpowder Agreed. Caplock only.
@jozsefienciu2325
@jozsefienciu2325 Жыл бұрын
Hi. What if you can not buy Ammonium Nitrate what can i use to replaces the Ammonium Nitrate?
@ciocanxxl
@ciocanxxl Ай бұрын
What if you use ammonium nitrate?
@kluper1157
@kluper1157 10 ай бұрын
what is the best PN to Buy? and told no Anti Cake?
@jorgeborau9151
@jorgeborau9151 Жыл бұрын
common charcoal whit potasiun nitrate like rocket fuel work well, idem whit sodium nitrate dont work.i change the charcoal.i use willow or poplar charcoal.more reactive and start work well and the rocket fly,
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