Would glass boiling chips help with the foaming

thanks you very much. Yes, I absolutely learnt some new techniques

Awesome video 😊

I know the waste only has a few ml of HNO3 but you can distill it out and just leave the sulfuric acid and chromic acid behind for your glass cleaning endeavors

I believe my teachers exposed me to mercury when I was younger. They knew I was a super genius.

I need that

Couldnt i just use a regular distillation apparatus?

I'm confused. He says he's running a 4 molar scale reaction which I guess would normally include 4 moles of water, (which is 72.06ml), though his mollecular notation diagram didn't include water, and at 2:17, he says he adds "nearly 9 extra moles of water" to the reaction side to facilitate carrying the nitric over. That's 162.13ml (Is that 9 on top of the presumed original 4, or just 9 total?) All well and good right, but then at 4:30 says he's adding 200ml of water to the reaction side.. 200ml is 11.1 moles of water, not 9 moles. And if you include the roughly 7% water in the 232ml of 93% h2so4 then that brings the total water volume in solute to about 216.24ml which is 12.003 moles of h²o. So, does it matter how much water you add? It doesn't seem like it does. I guess your end distillate would just be more dilute right? But why did he say he adds 9 extra moles of water and then proceed to add 11 moles? How come nobody else has pointed this out or asked about it? Is there an ideal amount of water to add to this reaction?

This product can cause cancer and is dangerous to the environment

Butthole loosening super serum

Can this chemical break iron nail and loose its magnetic property

I wish there was an easier way to make AA. This is a bit too complicated for me. : )

Great video. Informative and educational. Along with NurdRage's video, I was able to make dioxane on first try withourt messing up. But, Doug, my man, you talk way too fast and should fine tune your presentation, polish it up. Still, I rank it right up there witrh NurdRage. And that is a compliment.

Hello, my teacher, don't be tired. Is there carbon tetrachloride or chloroform in this methylene chloride that you made? Or is there only methylene chloride?

hey doug

On adderall?

Can i use 15% sulfuric?

Doug! After washing with hno3 , is there perhaps a desiccant that I could store it next to in an old non functional vacuum chamber pot?

In Canada,drain opener is %98 concentrated sulpheric acid, no need to distill,unless you don't like green dye

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Hello! Sulfate acid foams strongly during distillation. Please suggest an effective defoamer for the distillation of sulfate acid.

Why not using sodium nitrate instead of the corresponding potassium ?

lets say if one uses all starting ingredients which are 99% pure... will the end product be safer to use relatively?

Wish this channel was still active :(

Can iron chromite work in this situation?

Can I use anhydrous sodium hypochlorite? Ive got so much of it, as i found a huge bucket at a construction site (take it easy it was outside of the site and i only liberated 8 lbs of it!) But I didnt realize that it was way too much for me as I will never use all of it. Plus im hearing anhydrous sodium hypochlorite is Explosive? Any feedback will surely be appreciated. Take care

Брат,ты крут,нравиться наблюдать за твоей работой.Побольше бы таких людей на Земле.

Can i use vinigar 5% instead of the glacial???

Cheer~~~a salt of the anion CO32−, typically by reaction with carbon dioxide.😊

Dean stark apparatus would take care of removing H2O from the dioxane!!

We still miss you, Doug. Hope you're doing alright in this busy world.

Awesome. I wish you could show some "Easy destilation, like fractional " I never got that. I'm 58 and I love to learn from you man. Cheers from Sweden

thanks for the cleanup tips, most youtubers dont include them

Nice video

could use a salt and water chlorine generator for this?

this looks useful to make acetic anhydride with.

Northwest,ON,Canada

Awesome. NorthwestONCanada

Great Video!!

NorthWest,ON,Kanada

What is the heat required for distillation?

Science is just explaining witchcraft after the fact

So I've distilled h2so4 3 times now following your setup, minus the leibig condenser and substituting a Vigreux column. I also purchased a small terracotta plant base, broke it into small chips, ground the sharp edges and used them as boiling chips. Each time I've don't this I've ended up with quite a bit of white powder in my leftover discard solute. I speculate this is silica from the portion of terracotta that has dissolved, but I'm not sure, any ideas?

You and your experiment are great! Your mind is very clear, and yield of experiment is very high!

Why is it that sodium acetate abbreviates to NaOAc, makes it seem like a formula for a sodium oxygen actinium compound.

Can a impure tin ingot be refined to pure tin through electrowinninng or electrolysis

here in poland you can buy 500ml of DCM for 4 euros

Can i use Xylene as a solvent to get out the MeSalicylate?

I love how fast you talk. Thats pleasant