Chromyl flouride?

react hydrogen and chlorine together!!

Here in Brazil they sell 1 liter 91.8% ethanol at the market, its pretty cheap, about 3usd dollars or 12 conto🇧🇷

What about the ammonia, which says is the first ingredient in the stripper I have? What is the part that makes it goopy, cellulose?

Doug you talk too damn much...........PLEASE!!!!😮

I love how every home chemist uses the same PH papers and stonylab or labasics equipment

I don’t have a vacuum, so will I still be able to complete the process?

Basically , It is carbon compound ( in olden days our elders used wood to cook by inhaling co2 . I also came with this incident no. of times ) and non_irritating .

Legend has it the product is still drying in the vacuum dessicator.

As a beginner, I loved this demo. Thanks!

So I'm actually using one right now because I had to filter a material out of water. If I remember I'll update on how well it worked

Really want to see you. So interesting.

Just curious.Why do you distract the ether? What would one use tgat for?

Dean stark trap is one of the most underrated pieces of glassware

The Dean-Stark Trap is definitely one of the most underrated lab glassware pieces

Is that high end chainsaw fuel?

Everclear 190 proof. Molecular sieves soaked for 3 days.

Just a thought re keeping the xylene vapours in and minimising loss of xylene. You could put up a crude ice-bath on top of the beaker to set up a simple reflux system. Obviously, need to make sure the bowl you put on top isn't to heavy / doesn't fit too well to avoid breaking the beaker (that Would be a disaster). Some water might then condense out of the air, but that would be easily to remove from the solution (before cooling) with dried silica gel / molecular sieve.

Needed to uh, take a rest about 4 am. I notice you didn’t say anything about sleeping. 🤔

You can pour methanol/ethanol/isopropynol into the stripper after it's mostly distilled to continue the distillation for a slightly increased yield, however there still needs to be some leftover DCM for the polymer to not crash out.

Can we use the same process for potassium acetate?

can it work for potassium acetate?

I do realize this video was made 9 years ago so perfectly understandable If you do not know. I was wondering what final yield might have been with the initial 50 sulfer

❤

sadly off the shelf MEK at the hardware store is a thing of the past.

Ever clear is what i use

Would glass boiling chips help with the foaming

thanks you very much. Yes, I absolutely learnt some new techniques

Awesome video 😊

I know the waste only has a few ml of HNO3 but you can distill it out and just leave the sulfuric acid and chromic acid behind for your glass cleaning endeavors

I believe my teachers exposed me to mercury when I was younger. They knew I was a super genius.

I need that

Couldnt i just use a regular distillation apparatus?

I'm confused. He says he's running a 4 molar scale reaction which I guess would normally include 4 moles of water, (which is 72.06ml), though his mollecular notation diagram didn't include water, and at 2:17, he says he adds "nearly 9 extra moles of water" to the reaction side to facilitate carrying the nitric over. That's 162.13ml (Is that 9 on top of the presumed original 4, or just 9 total?) All well and good right, but then at 4:30 says he's adding 200ml of water to the reaction side.. 200ml is 11.1 moles of water, not 9 moles. And if you include the roughly 7% water in the 232ml of 93% h2so4 then that brings the total water volume in solute to about 216.24ml which is 12.003 moles of h²o. So, does it matter how much water you add? It doesn't seem like it does. I guess your end distillate would just be more dilute right? But why did he say he adds 9 extra moles of water and then proceed to add 11 moles? How come nobody else has pointed this out or asked about it? Is there an ideal amount of water to add to this reaction?

This product can cause cancer and is dangerous to the environment

Butthole loosening super serum

Can this chemical break iron nail and loose its magnetic property

I wish there was an easier way to make AA. This is a bit too complicated for me. : )

Great video. Informative and educational. Along with NurdRage's video, I was able to make dioxane on first try withourt messing up. But, Doug, my man, you talk way too fast and should fine tune your presentation, polish it up. Still, I rank it right up there witrh NurdRage. And that is a compliment.

Hello, my teacher, don't be tired. Is there carbon tetrachloride or chloroform in this methylene chloride that you made? Or is there only methylene chloride?

hey doug

On adderall?

Can i use 15% sulfuric?

Doug! After washing with hno3 , is there perhaps a desiccant that I could store it next to in an old non functional vacuum chamber pot?

In Canada,drain opener is %98 concentrated sulpheric acid, no need to distill,unless you don't like green dye

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Hello! Sulfate acid foams strongly during distillation. Please suggest an effective defoamer for the distillation of sulfate acid.

Why not using sodium nitrate instead of the corresponding potassium ?

lets say if one uses all starting ingredients which are 99% pure... will the end product be safer to use relatively?