-That white gold in your 14k portion is Rh plated. -You could use the Au electroplated material to inquart. The Au is plated on brass, which is Ni and then Au electroplated. Just assume that all the electroplated weight is 'inquart.' You'd be adding in the same Cu and Zn that's part of your Au filled material. -That junk metal is 'brass' or 'Zn diecast', that is zincate immersion (Na2ZnO3) coated, Cu flashed, Cu plated, Ni flashed, then Au flashed. Zn is just as useful to inquart as Cu or Ag. It all comes out when you do your HNO3 boils. -The material at the bottom of your melt dish is likely stainless steel. -I'm surprised at how little slag you have floating on top. That'd be your Zn or maybe Pb oxides. Looks like they might have been rinsed out into the drain when you spatter cast your melt into the cooling water tank. -The activity series isn't going to predict reactivity with acid. If anything, the reaction you got would be from the amount of Cu and Zn in the inquarted gold. Whatever Zn you add to your process will pas all the way through to your final Fe waste stream and be discharged in any liquid supernate. -Jeez. I didn't even consider Sn. -That white sediment on the bottom of the beaker, after the HCl boil, is your PbSO4. -Double, triple or even quadruple up on your filter paper for the Buchner funnel. In the old days, we'd use an asbestos fiber filter mat. I'd think you could use an activated carbon layer on top of the filter papers to help you get your clear solution. Of course, you'd need to add the carbon to your filter paper stash for later metal recovery. Yes, the filtration step will be slow, but less sensitive to high pressure vacuum. That IS nice Au! Long road to well done!
@thegoodlookinorange1986 Жыл бұрын
Mr. Foote. Thank you for the lesson of the day. You answered my ?’s and I’m sure some of SREETIPS’ as well. Keep posting here please. I’ll be watching for my next lesson sir. 😊
@aa1.5 Жыл бұрын
49:17 "It's getting late. I'm tired. This is when mistakes happen." This quote should be noted as it is knownledge to live by. Not only pertaining to gold refining but just in general. Stay safe everyone!
@DonnyHooterHoot Жыл бұрын
You stay safe! I'll LIVE! Thank you!
@datbeast767 Жыл бұрын
Yup. Always quit if you get tired.
@hansweichselbaum2534 Жыл бұрын
@@datbeast767 Nothing much would get done if I stop after getting tired. In my case, I get most productive when it's bedtime.
@kofeebeanz Жыл бұрын
Interesting to see how different this went in comparison to using silver. another great vid!
@mjay4700 Жыл бұрын
There is nothing... and I mean NOTHING.. like the feeling of PURE GOLD.. in the palm of your hand. Always love hearing you say that. Beautiful gold bar and great pour lines. Thanks for uploading.
@PopeyeFPV Жыл бұрын
Nice recovery Sreetips!....and the bar looked very uniform. A++++
@charleswise5570 Жыл бұрын
If for nothing else, this was very interesting. To see a different inquartation with something different than silver. Thanks for the hard work.
@betadoctor Жыл бұрын
80 Minutes of goodness on a Saturday morning. Thank you good Sir.
@larryevans7669 Жыл бұрын
Beautifully done. Stepping into something new, having it act in a very unexpected way, and you made the great save. Thanks for sharing. Steady wins the race.
@huseinabdul1 Жыл бұрын
Thank yoy sir again. This was very informative as initially I was like wow that’s really smart. Until I saw the results now I know not worth the hassle. Thank you.
@stevemoore445 Жыл бұрын
Twenty years of oil field machining with many late nights on a big lathe because everyone is waiting on ya! I’m surprised I’m not dead. Thanks for sharing and I did learn something.
@sreetips Жыл бұрын
I did twenty years in the Navy. I remember waiting on the MR (machinery repairman) to cut new wearing rings for one of the fresh water pumps on the distilling plant. We had no water to take showers while underway until he got them rings cut. Them the whole ship was waiting on us to reassemble the pump and get the evaps back up and running so they could wash up. But that’s ok, I work better under pressure.
@lazerwolfdiecast Жыл бұрын
It would be cool to see a video explaining the cost to profit ratio. Like how much you spend on chemicals, electricity, and metals compared to the value of the finished product.
@anthonyrstrawbridge Жыл бұрын
I believe it is negative. The scrap metal cost is fixed at scrap value. The refining costs are expensive. If you add up the two costs it is a big loss. Also, a percentage of the scrap material is lost during refining. The gold value in dollars per weight is the same regardless of purity. I don't think the cost in dollars is his mission. The silver from karat scrap is very profitable IMHO. 👍 The costs of equipment repairs, replacements, and upgrades and now replacements again, has been significant.
@Heymrk Жыл бұрын
@@anthonyrstrawbridge Diamonds have no resale value. None.
@garymyers6638 Жыл бұрын
He’s not doing it for profit. It’s a hobby so profit isn’t the primary mover.
@anthonyrstrawbridge Жыл бұрын
@@Heymrk 👍👍👍♥️✌️
@kalicom2937 Жыл бұрын
@@anthonyrstrawbridge And don't forget the KZbin revenue.
@Antonowskyfly Жыл бұрын
You are welcome! Tremendous video of a tremendous effort with a tremendous result that I watched in tre instalments and which I give tre tumbs up--->👍👍👍
@ryanhenderson4395 Жыл бұрын
Great video, it’s fun to watch you try new things…always learning! Maybe due to the increased reactivity of the base metal less is required.
@okiedirtdiggersadventures481 Жыл бұрын
Great video. It’s a lot more work this way. The gold bar is beautiful. Awesome job.
@jamisontaylor878 Жыл бұрын
Excellent video once again thank you 😊 the struggle is real with the filtering process!!! I play with Escrap only because my feed stock is basically Free !!! The amount of time refining this material is insane but fun
@mikesnipes316 Жыл бұрын
I love the chemistry of every one of your refineries. I read, liked all your comments. I agree with everything you mentioned. Keep up the good work & keep putting out this content. I've learned a lot from you. Thank you!
@alexanderleif21 Жыл бұрын
Thank you for doing this video. I love it when people put themselves in situations that they're new at.
@daviddpg Жыл бұрын
That trick with dissolving the gold off the inside of the beaker was pretty cool.
@andrewh3141 Жыл бұрын
Appreciate the video! I know it’s kind of a taboo subject on KZbin but I’m really interested in the financials behind buying scrap gold / finding the chemicals for the best prices / selling the refined gold for profit etc. Thanks again!
@dawnjennings4864 Жыл бұрын
OMG! I am so excited to watch this just because it's an hour and 20 minutes! Can't wait!
@ousley421 Жыл бұрын
All these videos and still my favorite part is the melt table. Thanks Sreetips
@VendettaProspecting Жыл бұрын
Man I fell asleep last night at 1:04:09 !! Finishing now! Man this reminds me of inquiring with too much copper!! Nasty mess lol so much extra work
@VendettaProspecting Жыл бұрын
A lot less loss than anticipated
@beauhodges7957 Жыл бұрын
I think this video perfectly illustrates the difference between how things work in theory and how they work in reality. I thought using gf scrap was a great idea, but I never would have thought you had the troubles with it that you did. Great video.
@sreetips Жыл бұрын
I was anticipating the gold falling apart. It just didn’t happen as quickly as I was expecting.
@kenb8773 Жыл бұрын
Although this didn't all go to plan, it was a great thing to watch, to see you think on you feet, and get a great result is a testament to you sir!
@Kushrenadat Жыл бұрын
I have watched so many of these videos now and I still find it fascinating. I am sure some time in the past person or group figured out how to do this in antiquity. That knowledge was lost and that is how the rumor of alchemy turning lead int gold came about.
@smijas Жыл бұрын
Even in these difficult situations,...you produced an excellent yield and excellent content. Must be difficult to concentrate on the video-content side, while working on a stubborn process.
@catch22frubert Жыл бұрын
I love to see the honest results of experiments like this. The bulk of the brass is copper, which should be no problem when inquarting, but that 15% zinc and the lead tin soldier really changed everything. Awesome video Sreetips. Its cool to see you experimenting and showing why its better to stick with a sterling silver inquartation when possible. If not, use pure copper or pure silver.
@Welshman2008 Жыл бұрын
Fascinating video as always I thought the splatter board idea was quite ingenious in its simplicity.
@disgruntledtoons Жыл бұрын
Your most perfect bar yet, and at today's spot price just a bit over $7300. And it seems that the high-purity gold precipitate tends to clump together (so that less of it gets poured off with the waste solution) than the low-purity stuff earlier.
@mickg6480 Жыл бұрын
'Atta boy. That's more like the result we're used to. And the pour lines on that little bar are amongst the nicest I've seen from you lately.
@guygordon2780 Жыл бұрын
Not only is the Zinc more reactive, but as it is removed early, it's absence will leave channels through the remaining mostly copper alloy. Those channels will add a lot of surface area, thus speeding up the remainder of the extraction. You might find yourself using this more often, to save time. Lets hope it doesn't add any problems. Of course, you could also inquart using a mixture of sterling silver and gold filled scrap.
@DFPercush Жыл бұрын
Might be worth experimenting to see at what percent of zinc does the gold start to fall apart and form suspensions.
@BronzeAgePuritan Жыл бұрын
Using silver feeds the silver cell.
@lazyman114 Жыл бұрын
I think he spent maybe up to 10 hours extra to recover 6 extra grams from the gold filled scrap. Combined with the extra headache, I think it's not worth using this method.
@guygordon2780 Жыл бұрын
@@lazyman114 Trying something new always takes more time. Doesn't mean it's not worth trying. Best way to learn something new. The problem Steetips ran into is not inherent to this method. It's a problem whenever the inquarted gold is much less than 25%. At 25% you get a gold sponge.
@JamesSkellington-xj8nn Жыл бұрын
I love to sit and watch your videos I learn so very much . Even though I don't do experiment such as yours . It's always good learn something new from a learn Ed person such as you .
@darkunicorn1208 Жыл бұрын
Now this is gold content. Love the experimentation vids.
@vinnycordeiro Жыл бұрын
Considering that a lot of colloidal gold went to your temporary waste container while cleaning the precipitated gold, the yield was really good. I believe it was so close to the theoretical yield because of the extra from the gold filled material, about 5 to 6 grams. Anyway, that's a messy alternative to be used when you have no silver/copper readily available, but it is surely not ideal.
@daftwulli6145 Жыл бұрын
well sure it is messier, BUT on the other hand you do 2 refinings in one, scrap and carat, so it seems like it does save work, and quite a bit
@DonnyHooterHoot Жыл бұрын
I got a kick out of the aqua regia cleaning up that nasty looking glass! Great video!
@fredrichardson9761 Жыл бұрын
Excellent video! Really proves the point that your silver enquartation approach works really well compared to using gold filled scrap. Still, in spite of the extra work you produced another stunning bar with a very good yield. Well done! 👍
@boardmandave Жыл бұрын
Your process is wonderful to watch and your voice is extremely soothing thank you for another excellent video
@jasonperlmutter7849 Жыл бұрын
You've gotten way safer with your technique in these videos. Love this and really enjoy the content you make. Awesome content!
@nicholasgreen2012 Жыл бұрын
Thank you streetips. The audio quality is almost perfect.
@burriedhistory Жыл бұрын
Thanks for showing us that experiment.
@patpawlowski7635 Жыл бұрын
Really good idea, getting even more efficient with the process for gold filled material. I love seeing a new process or idea
@71723 Жыл бұрын
I think he kinda had to with this round. He said during one of his recent platinum videos that Mrs. Sreetips wasnt happy with him getting behind due to the platinum stuff.
@JamesSkellington-xj8nn Жыл бұрын
Very Beautiful bar I love how it has a fingerprint look on it . Keep up your terrific videos . 👍👍👏👏
@ArielleViking Жыл бұрын
Very interesting to see you use the gold filled scrap this time and very interesting to hear the facts of "gold plated", I will never buy this now after learning this from you. Nice that the yield was close, I wonder how much gold is in the stockpot? Awesome video. 👍
@kwinterburn Жыл бұрын
Don't know whether this might be useful but I used to have to extract settled sediments from the liquids, the problem was you couldn't Syphon off all of the liquid, so I got a wine bottle with a plastic screw top, cut off the bottom with a tile saw, then you could fill with the liquid and leave it, the sediments settled on the plastic cap right in the neck, so you could Syphon off almost all the liquid without disturbing the sediment, it's also how the painters extract pigment from water based paint out of brushes, it just flows out of the brush and falls to the bottom without circulation,
@tonyquark493 Жыл бұрын
Wow at the final dissolve in aqua regia, it seems the solution was so saturated with dissolved gold I think that's why it was having trouble dissolving more until you added more Hcl! You can tell when that auric chloride is that dark the yield is going to be crazy! Amazing video, and it was a dirty procedure, but as usual, you turned it into a win!
@pittypatterputzzler5311 Жыл бұрын
This gentleman sound's like a Airplane Captain I feel save to fly with. I am watching this for 3 days, it is really interesting. Thank you. Good bless America and it's service to the world.
@sreetips Жыл бұрын
Thank you!
@pittypatterputzzler5311 Жыл бұрын
Don't thank me, please I didn't do anything. But this videos are Legendary.
@pittypatterputzzler5311 Жыл бұрын
kzbin.info/www/bejne/a6uTqIh3adZkr6M this person has all the hacks on KZbin.
@roberthayward9299 Жыл бұрын
Great work as usual Sreetips. The zinc and copper will use a little more nitric acid than the silver would have because these metals both have a valence of 2 rather than the valence of 1 for silver. Interestingly, under some controlled reaction conditions, zinc will form nitrous oxide "laughing gas" instead of the brown nitrogen dioxide that usually forms.
@sreetips Жыл бұрын
I noticed some white foam during the nitric boils.
@gratshor Жыл бұрын
36:39 You no need to waste hydrochloric acid for silver test. Use for it medium to high saturated solution of sodium chloride (cooking salt times cheaper than muriatic acid). And salt will not rise acidity of solution, but gives same precipitation result as acid. 36:50 That green cloud is copper dichloride (CuCl2) and possibly zinc tetrachlorocuprate (Zn[CuCl4]), both salts quite unstable(especially second) in nitric acid or it's salts solutions 43:44 Nasty ortostannic acid (or fine tin oxide, from G.F. material) clogging filters in minutes or go though it if not fine enough. Using filter "sandwich" will help alittle. Filter Sandwich from top to bottom: rude filter (cotton pad), semifine filter/filters(quick and/or medium flow class) and fine filter (slow flow class a.k.a. "blue tape"). To prevent forming tin oxide add citric acid as inhibitor (about 24 gram per 100 ml HNO3) and avoid to heat solution above 50°C. 53:46 forgot stannous chloride test
@apveening Жыл бұрын
About that silver test, I'd say it is inconclusive, led chloride will also precipitate. The way to distinguish led and silver is to take a bit of that precipitate, (try to) dissolve it in ammonia and add some potassium iodide. Led chloride won't dissolve in ammonia and silver iodide will give a nice, bright yellow precipitate.
@sreetips Жыл бұрын
Or, just add a piece of copper. Silver will cement out, the lead won’t.
@sreetips Жыл бұрын
I didn’t do stannous at a couple spots. I’m so used to not do it then I forget while shooting the video.
@apveening Жыл бұрын
@@sreetips Works ... in a non-acidic solution.
@gratshor Жыл бұрын
@@apveening Lead chloride precipitate only in concentrated solutions, in diluted solution it's redissolves. Solubility difference between lead and silver chlorides is significant: for PbCl2 is about 1gram per 100ml (at 25°C), and for AgCl is about 20micrograms per 100ml (or 0.2gram per tonne)
@bikinglikebecker Жыл бұрын
is home refining profitable? aside from when you purchase for demonstration purposes & overpay... Also I was thinking Instead of just doing a straight nitric to pull out the base metals only, you could do it another way without having to inquart. Why not do aqua regia to put all metals in solution then precipitate/filter & do nitric pulls when it is a dried powder? I think it would do it better with fewer nitric boil pour offs... I could be wrong, I have as yet to do my first refine with all this e-waste from computers I found that I couldn't just rebuild & give away... Surprised that some of these old processors can go for quite a bit of cash... same as the ram & other hardware... almost like it was when it was cutting edge technology... lol..
@sreetips Жыл бұрын
You could put the karat gold directly into aqua regia without inquarting with silver. But two major problems would arise. 1) it makes a very dirty solution that looks like used motor oil. 2) any of the gold that contains much silver would passivate. The HCl in the AR would react with the silver and form a tough layer of silver chloride that would shield the gold from the acid. To remedy it must be removed before the gold will go into solution. Both problems are completely eliminated by inquarting with silver (or clean copper) and parting with hot dilute nitric boils BEFORE going to aqua regia. Plus, I refine silver and the first step is to dissolve it in hot dilute nitric acid. So why not use it to inquart? Like refining both metals at the same time.
@waynewalsh2008 Жыл бұрын
I watched this for too long…… can’t take my eyes off of it 😊
@SaltyMeatHook Жыл бұрын
From the pimple to a mighty dimple bar! Very nice!
@gregdobrick3410 Жыл бұрын
As always, great video,beautiful bar.
@ICU2B4UDO Жыл бұрын
That bar of Au is worth $8K!! Nice job Mstr. Ch.
@CreamPolo Жыл бұрын
Your Videos have soul cleansing quality.
@chrish1585 Жыл бұрын
I see the benefits of using the gold filled material for inquarting. I wonder what the cost benefit is compared to silver. A higher gold yeald, but not much silver to recover. Still fun to watch.
@sreetips Жыл бұрын
I refine silver also. The 1st step is to dissolve it in hot dilute nitric. So I missed an opportunity to get some more silver dissolved. I have much sterling that needs to be dissolved. But I’ve also got a bunch that needs to be melted, granulized, and run through my silver cell. I’m way behind on everything.
@carlosalmeida4415 Жыл бұрын
Love watching you work sreetips. I never miss a video.
@TroubledOnePaydirt Жыл бұрын
I really enjoy these longer videos like this. I prefer a long video to multiple shorter ones I think. I’m guessing you won’t be enquarting with gold fill again anytime soon… ouch… still, pulled it off. Challenge complete. Lol… 👍💪💪
@Sanzus2 Жыл бұрын
Ended up with a good looking bar! First drop the liquid was the same color skin turns when wearing gold filled jewelry! Have you thought about going to a greater gold percentage with the alloy to see if it prevents it from going colloidal?
@sreetips Жыл бұрын
Didn’t think of it for this run. But it’s not a bad idea.
@Sanzus2 Жыл бұрын
@@sreetips the other thought would be to re-melt after the first couple of nitric acid baths when you are no longer getting a reaction and most of the zinc is gone. You would be left with mostly copper and some silver and it might keep it from breaking down into colloidal.
@Lancelot.666 Жыл бұрын
Another stunning looking bar of gold, well done Sir..🙂👍
@cypridiot Жыл бұрын
Me and my wife recently discovered your channel and we have been bingewatching your content. It has a very strong ASMR video feel to it. Now we got talking about your accent and im thinking Boston, the wife is saying Vermont. How wrong are we?? Absolutely enjoying the video's!
@sreetips Жыл бұрын
Iowa
@cypridiot Жыл бұрын
@@sreetips oh lord.... haha tnx for your reply. Love what you are doing
@spamaccount6460 Жыл бұрын
So glad to see a happy ending on this. It sounded like it wasn't going too well and I was afraid of what the actual yield was going to be, but in the end, it's a gorgeous bar and very little (temporary) loss of gold!
@sreetips Жыл бұрын
That’s exactly how I was feeling
@anthonyrstrawbridge Жыл бұрын
Today I am increasingly aggravated by my state legislative branch. Again, they have reached into my pocket and helped themselves to take money which does not belong to them. I am distraught to the very wickedness of their hands and I am resolved to halt this ongoing molestation of my very person. FU legislation!
@sreetips Жыл бұрын
Most people are clueless about how their finances are being plundered.
@rdk162 Жыл бұрын
MAKE AMERICA GREAT AGAIN!!! LOVE YOUR VIDEOS!
@jerryellis835 Жыл бұрын
Considering the amount lost in waste that was a excellent total. Way more than I thought. No stannous testing, was it not really necessary on this one or was it cause you knew some would stay suspended ? 1 other question I always wanted to ask, would it be worth getting a digital karat reader? I know a lot of pieces not plumb would always be either under or over karat stamp. Would that interfere in inquarting ?
@sreetips Жыл бұрын
There’s a “Goldie locks” range for inquarting. Too much silver and the gold will crumble to a powder making separation of the silver difficult to pour off. Too little silver and the nitric may not be able to penetrate.
@ghosttwo2 Жыл бұрын
When you get the purple gold nanoparticles in suspension, I wonder if adding a small amount of SMB would act as a surfactant, and cause them to condense? I know that it can make particles of many atoms when it reacts with chloroauric, but I wonder if it can have the same effect on particles in suspension. Next time you get some 'purple gold' it might be worth putting some in your spot wells and trying different remedies like copperous, or even lye. If you can find an additive that efficiently condenses colloidal gold, it might open up other refining options.
@bfd1565 Жыл бұрын
I enjoyed the longer video. This was a fun one to watch. I knew in the end. You were going to produce an amazing looking bar of pure .999 gold. I'm looking forward in you tackling the gold refining waste. This gold filled experiment throw a lot if junk into it im guessing. Fun stuff Sreetips.
@sreetips Жыл бұрын
I’m might jump right on the waste and get that gold out of there.
@PaulBrown-uj5le Жыл бұрын
@@sreetips I was thinking about that.
@alistairclark681410 ай бұрын
That's a good looking pour sir! Cheers from Canada! 🇨🇦👍
@CLP_II10 ай бұрын
Hooyah Shipmate!!! I love your videos. You do great work. I have an idea, could you put your fume hood over a regular glass topped stove? Then you would have four burners at the ready and you wouldn’t need to keep replacing the single burner so often. Thank you.
@CLP_II9 ай бұрын
Also a self cleaning oven gets like up to like 900 degrees. That might help instead of using your outside oven/ kiln. I hope not to be nosy, but after seeing your videos from years ago it seems like you are constantly trying to improve your processes. I’m mostly thinking of how I’m gonna make my refining work center. You motivate me!! If you can do it I can too.
@sreetips9 ай бұрын
That’s not a bad idea except, the stone wouldn’t hold up to exposure to the acid fumes.
@JossWaddy Жыл бұрын
Been doing my revision. (You've got me doing my balanced equations again!!) Seems to me that the white clouding solid making that first filtering a nightmare was almost certainly Lead sulphate. Anyone agree? Sree mentioned that lead solder was likely present in the Gold Filled material. Honestly, this channel is reigniting my love of chemistry all over again! If I'm ever at a pub quiz, I'm definitely going to know what Muriatic Acid is more properly known as!! Thanks again for all your effort.
@sreetips Жыл бұрын
Tin and nitric form metastannic acid, or tin paste. It will clog a filter like trying to pull Elmer’s glue through a filter paper.
@JossWaddy Жыл бұрын
@@sreetips and this is why I should not be trusted to get out the chemistry set!! thank you!
@1911darkstar Жыл бұрын
Beautiful bar! Super interesting process this time. It looked like you were loosing quite a bit when the gold was in that finely divided state during the pouring off process. It’s really interesting the different states the gold goes through during the process. Any ideas for future inquarting, i.e different metals or just going to stick with sterling?
@sreetips Жыл бұрын
I have more sterling that needs to be dissolved so I’ll probably use that.
@John-dp3ln Жыл бұрын
Beautiful recovery from what looked like a colossal mess.
@Hawk013 Жыл бұрын
THis is the kind of thing they need to be teaching in chemistry classes, way more interesting to watch and see actual results.
@arch1107 Жыл бұрын
tbh i think they try to teach this, ot least my teacher did, but i was too young to get it
@sreetips Жыл бұрын
I took a chemistry class in high school 50 years ago and got a “D” and never took another.
@arnedalbakk6315 Жыл бұрын
Hello Mrs and Mr sreetips. I love the way you take us thrue wats happen. Ten tumbs up from me😊. I coment before i have see the whole clip, becouse i now you i now you make it🌹. Have a nice weekend, and my god bless you more, and more. Thank you both of you. Arne
@Joe.Rogan. Жыл бұрын
Seems like no matter how you process GF scrap it's a pain the ass. If there was only a way to figure out how to streamline the extra time it takes it would be a great way to use up all that GF scrap you got stashed away.
@josephrupsis4623 Жыл бұрын
would be nice if he tried again at some point. Was hoping it would streamline the GF process. Maybe he needs to add less GF and more karat due to the zinc?
@sreetips Жыл бұрын
Trying to process both at the same time usually defaults, time wise, to the slower of the two processes. Seems like.
@stephensepe7113 Жыл бұрын
Just a late observation here- but using the GF scrap, you don’t take into account the karat gold content from the GF stuff into your calculations- curious if your 6kt inquartation goal is still met.
@sreetips Жыл бұрын
The fact that the gold crumbled to a powder instead of staying solid chunks is an indication that there was actually too much non-gold metals present in the alloy.
@apveening Жыл бұрын
That test for silver with HCl in the small beaker was inconclusive, led will give the exact same reaction.
@shaneyearby4438 Жыл бұрын
Great video and it seems like a real pain to process it this way. But at least it turned out a beautiful bar. Seemed to break the gold down a lot more than silver.
@matthewsemenuk8953 Жыл бұрын
My idea for a cool bit of video, or video in itself, is showing how the lead in solution reacts to the sulphuric acid by adding a bit of lead or solder to what would be a gold refining process Obviously it would only be a proof of concept video and not actually include the use of gold in solution, but maybe some weighed out (gram or two) before and after lead/solder to a silver or copper solution? Just a thought. Thank you for the awesome videos.
@sreetips Жыл бұрын
Coming up, good suggestion.
@matthewsemenuk8953 Жыл бұрын
@@sreetips Cool :D
@NikolaHoward Жыл бұрын
I think the expression is "Can you do it? Well, yes. Should you do it? Heck no!" Interesting reactions there. Would be interested to know what dropped out of the Blue Nitric residues - would guess a whole heap of copper!
@sreetips Жыл бұрын
Correct
@CuttinEJ Жыл бұрын
I’d have to say you did a great job considering how nasty the solution looked prior to the first filtration. I think I’d have to agree with your conclusion too. Only reason to inquart with gf is if you were desperate and really couldn’t get your hands on some silver or copper.
@daviddavis4005 Жыл бұрын
Gooood evening from central Florida! Hope everyone has a great night!
@arnedalbakk6315 Жыл бұрын
Same to you😊
@sreetips Жыл бұрын
Goooood evening!
@barnes29510 Жыл бұрын
I've been watching/learning from you on recycling the gold from computer boards, etc. I purchased a solution that's 33.2% chloric acid to release the gold. (Living in a small town I can't find nitrate acid). But is 33.2 strong enough for what I'm doing? And is it ok to leave the parts soaking overnight? Thanks!
@sreetips Жыл бұрын
I don’t have any experience chloric acid. I’ve used hydrochloric acid and 3% hydrogen peroxide (acid/peroxide aka A/P) to release gold foils from computer scrap fiber board. Hydrochloric acid from ace hardware. Hydrogen peroxide from the grocery store.
@barnes29510 Жыл бұрын
@@sreetips I'm sorry I meant hydrochloric acid. It's a solution for cement etching. So hydrochloric and hydrogen peroxide would be a 1:1 ratio for the boards. Sorry for asking so much. I'm a total noob with chemistry
@davidangell66935 ай бұрын
Do u buy from a store or have you ever made your own distilled water? I recently have been making my own distilled water and it had been going well then out of nowhere I added some water to a solution that had some silver and sure enough It turned into silver chloride just out of the blue. So I'm gonna have to go back to store bought until I can figure out what happened. Thanks for making the videos. Especially this one. I had gotten this same sort of thing happen to me.
@sreetips5 ай бұрын
I use about twenty or twenty five gallons of distilled water per month. So I just get more be at the grocery store.
@jphillips4371 Жыл бұрын
Over an hour sree refining video on a Friday night 😎😎.
@arnedalbakk6315 Жыл бұрын
😊🇺🇲
@mikeconnery4652 Жыл бұрын
Another great video and a beautiful gold bar.
@Fambamm-ib6pw Жыл бұрын
Amazing video thanks for sharing as always.. How is your silver cell doing, we miss it lol
@sreetips Жыл бұрын
I’ll get some footage of it in my next video.
@floydsallee2041 Жыл бұрын
Awesome video love it. I would like to see you refine gold-plated material I think that would be cool to see starting weight vs refined weight, just a suggestion. Thanks again
@NOFX0890 Жыл бұрын
Search for his vids on sulphuric acid stripping cell.
@buggsy5 Жыл бұрын
He has a video where he does exactly that, if I recall correctly.
@NOFX0890 Жыл бұрын
@@buggsy5 certainly. Then not long after, he sold all his gold plated scrap. Telling..... Is the juice worth the squeeze.
@buggsy5 Жыл бұрын
@@NOFX0890 Gold plated scrap is not worth refining, probably even with a stripping cell. It might be profitable for a big refinery that could treat it as a secondary recovered material. Heap leaching might also be worthwhile if you have a few tons of the scrap - but that process is really nasty.
@guygordon2780 Жыл бұрын
Wow. Did not expect that much difference (powder instead of a sponge.) Looks like you could cut back on the amount of base metal when it contains zinc. I don't think you made a mistake trying this. You just need to tweak the process a bit, and it could well work out better than using just sterling silver.
@josephrupsis4623 Жыл бұрын
I agree, though he uses sterling to refine both the gold and the silver. I figured it'd be easier to refine the GF than it would be to increase the karat yield. Would be nice if he tried again at some point.
@sreetips Жыл бұрын
Gold filled takes several days to get it done. I can refine gold to high purity in ten or twelve hours. Combining the two processes into one, like in this video, seems that it defaults to to longer of the two processes, time wise.
@sreetips Жыл бұрын
I may try it again with a smaller quantity of karat scrap and reduce the amount of gold filled I add.
@guygordon2780 Жыл бұрын
@@sreetips The basic idea was sound. But yeah, it was a large amount for a trial run.
@troynixon9467 Жыл бұрын
Awesome video as always , was quite the adventure !!
@dannomight19804 ай бұрын
Would it be beneficial to add an inline whatman filter when siphoning the liquid out around the 31min mark or just in general? Might be a way to save some time and gold in situations like this video? Heck I may just order some for my future endeavors 🤔 Most men can always use new tools or equipment right?
@sreetips4 ай бұрын
Right!
@ericshuping3651 Жыл бұрын
For the purpose of inquartation, how do you know how much gold-filled material to use? Or do the constants you use for sterling silver still apply?
@sreetips Жыл бұрын
Should still apply.
@dabigdawg145 Жыл бұрын
I've been learning so much. I might try my hand at metals recovery.
@dynorat12 Жыл бұрын
if you use a stainless screen that's touching the water you can get a finer beads of inquarted medals
@chrisvanderburg5568 Жыл бұрын
Would it be more efficient to remelt the black gold powder and inquart with silver so you can refine in a normal fashion instead of pouring off small amounts of suspended gold powder each and every time you drain off a rinse?
@sreetips Жыл бұрын
I’ve done that when I added too much silver and the gold crumbled to a powder. Remelt, inquart with silver and proceed as usual.
@GalutiaFamilyChannel3 ай бұрын
Thank you for the demonstrations of the process of “Aqua Regia”.
@sreetips3 ай бұрын
Glad to do it.
@JustJeff62 Жыл бұрын
Absolutely excellent video Sir Sreetips!💯This is exactly how we learn brother! A huge THANK YOU!!! You did a incredible job cleaning up that solution! Bravo!!! Is there a difference between Stump-out and Food grade SMB?
@sreetips Жыл бұрын
Thank you. No difference.
@josephnoonan82 Жыл бұрын
finally, a very long videos like the old days!
@ZoonCrypticon Жыл бұрын
@7:00 here the stories, the memories, the tears and the smiles, the efforts and struggles of a multitude of humans is molten down into oblivion...
@sreetips Жыл бұрын
This has been happening since ancient times. Biblical.
@RossSeverns8 ай бұрын
This is my favorite show.
@I_am_BiG_Al Жыл бұрын
I've literally been binge watching now for like 3 days and that's the first time you've worn a mask lol