In this video I demonstrate how to make nitric acid for gold and silver refining.
Пікірлер: 440
@otilium7503 Жыл бұрын
The golden color is so gorgeous!
@spencergraves9893 жыл бұрын
Thankful for you and your videos. I appreciate your precision and how this video describes the whole process with the upmost detail.
@philipbender9563 жыл бұрын
Thanks, I am happy you enjoyed the video 🤗😀
@prinz10ga4 жыл бұрын
Fascinating and very informative. Would love to observe first hand.
@larrylaird91 Жыл бұрын
Thanks for the chemistry class and it's exactly what I am looking for fuming red nitric acid, I need it to make mucury fulminate which is very dangerous but if stored in water it is safe as long as you don't drop it.
@ethicalhacker88875 жыл бұрын
Thank you from Pakistan
@gamingshortschannel11093 жыл бұрын
Absolutely awesome information. I am happy I stumbled across a bright mind like you. Keep up the good videos. Can't stop watching them.
@philipbender9563 жыл бұрын
Thank you, I am happy you enjoyed the video 🤗😀
@S730SD4 жыл бұрын
In the same instance, I'd have added boiling water to the crude nitrate after putting it in the beaker; just enough to dissolve them. Might speed up recrystallizing & with less H20 to get rid of. :)
@josephpecoul65323 жыл бұрын
Im a Casual Observer and im on board thanks for the video.
@philipbender9563 жыл бұрын
Thanks, I am happy you enjoyed the video 🤗😀
@paulscottpadgett19963 жыл бұрын
Much Respect 💪
@ourodolixo-e5 жыл бұрын
Very good 👏👏👏👏 Nice👍
@n.pisamoovung18223 жыл бұрын
I'll have to give this a try. Thank you so much for the explain
@philipbender9563 жыл бұрын
Thanks, I am happy you enjoyed the video 🤗😀
@sreetips5 жыл бұрын
Nice work, I'll have to give this a try. Thank you.
@tchouwie5 жыл бұрын
sreetips I came here because I usually follow you. I just wanted to reply so both of you know. You can make Nitric acid for free. If you take wood ashes as a source of potassium and your morning pee for the source of Nitric. You mix the two and boil that, the vapor that will come out as it boil will be Nitric acid. Just letting you know in case both of you didn't know.
@sreetips5 жыл бұрын
That would make a very interesting video.
@johnblair81465 жыл бұрын
Sreetips, the beginning of this video reminds me of your videos about precipitating gold from chloroauric acid solutions only backwards. :-)
@AbuBakr.Abdullah4 жыл бұрын
@@tchouwie wow did u try that yet?
@craigmohammed86804 жыл бұрын
88888980ijhyu9
@NOFX08902 жыл бұрын
Another great video Philip. Thanks for the info and thanks to the people in the comments for the extra tips. Id add something, not very technical, but a thrift store stainless potato masher might help with breaking up the Potassium Nitrate crystals. Love your Audio track man. Dont ever change your style.
@philipbender9562 жыл бұрын
Thanks, I am happy you enjoyed the video 🤗 😀
@anahoae5 жыл бұрын
You can make it from thin air and electricity as well Nice vid thank you
@okay86323 жыл бұрын
not so easy though
@ismetbiljali97004 жыл бұрын
Very nice Man thanks
@jacksonvillereclaimedwood67093 жыл бұрын
Great video dude!
@philipbender9563 жыл бұрын
Thanks, I am happy you enjoyed the video. 🤗😀
@camsmagnetadventures40303 жыл бұрын
Thanks keep up the video man now I can refine some silver
@philipbender9563 жыл бұрын
Thank you. I am happy you enjoyed the video 🤗😀
@JK-zl7vv Жыл бұрын
Very helpful brother 😎👍
@mr.planter4943 жыл бұрын
You're a great teacher.
@philipbender9563 жыл бұрын
Thanks, be sure to treat other chemistry channels as a class. You will learn more from many 🤓
@mr.planter4943 жыл бұрын
Dude I love your videos
@philipbender9563 жыл бұрын
😌😅🤗😎
@najeebullahamjad82244 жыл бұрын
Nice posting
@johnnyx534 жыл бұрын
Good video! Practical- esp when seeing the price of nitric online and the ultra-high expense of hazard shipping! You’re like paying double for it
@thehatedones51534 жыл бұрын
Distill battery acid, it’s cheaper and you can find it locally
@chemistryofquestionablequa62526 ай бұрын
@@thehatedones5153that’s sulfuric acid, not nitric
@shintokatana172 жыл бұрын
Very nice, thank you for sharing
@philipbender9562 жыл бұрын
Thanks, I am happy you enjoyed the video 🤗 😀
@gwsmith764 жыл бұрын
You should filter the potassium nitrate solution boil it until salt begins to form on a metal spoon or knife when it’s removed from the super concentrated liquid. The place in fridge for 4 hours, repeat process. Your yield will double if not triple, take less time and ultimately produce more nitric acid.
@amrendramishra5457 ай бұрын
Congratulations 😊
@Berghiker2 жыл бұрын
When potassium nitrate dissolves in water, it is an endothermic reaction as the temperature drops.
@gantz4u4 жыл бұрын
Provided you have all of the glass laying around. Cost break down for ingredients looks to be US dollar $17 to $23 here. Vs. $50 to $62 for roughly the same amount of purchased nitric(if they will even sell it to you) at these quantities, no clue how the cost break down works for 55 gallon orders but I'm somewhat doubtful the savings with this scale there. Mileage may vary on those ingredient prices.
@tomspeed20002 жыл бұрын
Is nice video, at the end I recommend to be use dark glass container instead transparent glass because HNO3, specifically at high concentrations forms will decomposing by the lights..
@philipbender9562 жыл бұрын
Thanks, I am happy you enjoyed the video 🤗 😀
@nurcahyani9802 жыл бұрын
Yes tangkyou mastter impormasi nya yes
@philipbender9562 жыл бұрын
Thanks, I am happy you enjoyed the video 🤗 😀
@legaia_28044 жыл бұрын
Would any basic distillation kit work for this, or should I buy a certain kind? Sorry for my ignorance
@jhyland874 жыл бұрын
Damn... Those crystals are too pretty to break! You should see how big of a single crystal you can grow.
@Billionaire2.0492 Жыл бұрын
can we use sodium nitrate instead of pottasium
@jadenephrite3 жыл бұрын
Regarding 2:03, adding potassium nitrate into water produces an endothermic reaction which is the cooling effect. On the other hand, if it had been an exothermic reaction, this would have produced a heating effect.
@philipbender9563 жыл бұрын
Yes I misspoke during the narration.
@rene.martinez57144 жыл бұрын
Thanks bro fr
@moci42 Жыл бұрын
I have no desire to make nitric acid, but the chemistry of it is most interesting.
@mdsajidnoman97164 жыл бұрын
Nice
@StevenSchoolAlchemy3 жыл бұрын
Great job!
@peterlamont6475 жыл бұрын
Hey, and when you're done making nitric acid, you can make some corned beef with all that salt peter...couple tea spoons to a brisket, brine for a couple weeks in the fridge.
@peterlamont6475 жыл бұрын
Although the stuff I have is pink...potassium nitrate is white. So I wonder if it is just a mixture of salts I have...
@philipbender9565 жыл бұрын
@@peterlamont647 the pink stuff maybe an anti-caking agent.
@peterlamont6475 жыл бұрын
@@philipbender956 I'm thinking they put pink dye in it so that you don't mistake it for regular salt. In many recipes & cook books it is referred to even as pink salt. It also tells you when the meat is corned(its the only way I can tell) when it turns pink. This is also what gives salami, pepperoni, corned beef, bacon, ham, pastrami etc. their respective pinkish color. I had always assumed that salt peter was pink as a chemical as a result...I definitely learned a lot from this video!
@hmax15914 жыл бұрын
O.K. thank you for the chemistry class. very interesting. I doubt it I would be refining gold or silver from computer parts, I have seen your other video and seems quite a lot of work for such a small amount of gold. . But it is interesting. I mix potassium nitrate and sugar to make great smoke bombs.
@chancebutler64722 жыл бұрын
tyvm
@philipbender9562 жыл бұрын
Enjoy 😁😊
@thebobsquadmob4 жыл бұрын
I have the honor of being #1000. I am not a chemist by any stretch but I would say this is a great instructional video. I was actually looking for instructions on turning the non-metallic lead in a lead-acid battery back to metal. Robert Murray Smith did one a few years ago but I think he removed it because too many people were on him about the safety of handling lead. I see quite a few guys doing battery revival videos and the not metallic lead seems to go to an undisclosed location.
@fivel9764 жыл бұрын
i have found that if you filter of your water from the first batch and use it in a second batch you get a much better yeald first batch i got 2 pounds from the 3 pounds i stared with the second batch using the water from the first batch i got 3 lbs 2 oz of crystls
@johnrpickett17943 жыл бұрын
Hello - The video worked great. Was able to follow, adjust for my size equipment and the results were spot on ... The 1st time. I do have a follow on question for my 2nd and 3rd batch I did months later. Upon completion I did not have any Potassium Sulfate left over in the boiling flask. Why and what was the catalyst for this occurring? Hope you see this new question on an older comment. I enjoy the videos!
@philipbender9563 жыл бұрын
It sounds like you used an excess of sulfuric acid.
@johnrpickett17943 жыл бұрын
Thanks. Will pay more attention.
@johnrpickett17942 жыл бұрын
Saw my error. Potassium nitrate measured in grams. Sulfuric acid measured in ml. Next batch went perfect. Thanks again!
@zmarekk3 жыл бұрын
Great job :) like is ok.
@philipbender9563 жыл бұрын
Thanks, I am happy you enjoyed the video🤗😀
@user-je2yg3om8n Жыл бұрын
Thank you for this description. Please how can I use sulphuric acid deluted 32% ?
@philipbender956 Жыл бұрын
I am not sure if you can. 🤔 I am happy you enjoyed the video.
@imsidetracted4 жыл бұрын
i used to use stump remover for my candy rocket engines then i discovered amazon when I wanted to add powdered aluminum darned if they dont sell it, and potassium nitrate! cheaper also!
@philipbender9564 жыл бұрын
Yes, I purchase all my potassium nitrate from amazon.
@billywalker86315 жыл бұрын
Can you link to a place to get all the glassware you use in your distillation setup? Or a list of pieces? Thanks
@GainsGoblin5 жыл бұрын
Probably better that you learn about it on your own. Playing with acids without any knowledge about basic chemistry isn't very safe especially if you plan to play around with nitrogen compounds. I can ship you a distillation lab I did recently. The principle is the same as what is described here and the apparatus used to distill is similar.
@longimanusisurus1323 жыл бұрын
Simply beautifull. Could you tell me how much quantity you get of nítrico acid using that 800 of PN, and 600 of Sulfúric ac?
@philipbender9563 жыл бұрын
About 500 mil
@rkb67833 ай бұрын
WOW... THAT WAS EXPENSIVE !
@michschep76015 жыл бұрын
Filter the hot solution before cooling to remove anti-caking agents...... and its endothermic reaction when mixing nitrate and water.....
@abdullraufkhn40522 жыл бұрын
Good very nice vedio.
@philipbender9562 жыл бұрын
Thanks, I am happy you enjoyed the video 🤗 😀
@abdullraufkhn40522 жыл бұрын
@@philipbender956 Thank u very much Sir.
@gauravsrivastava94772 жыл бұрын
phillip I love your work , its amazing to watch you doing all this , I also want to do this , can you name sources where I can buy these chemicals , equipments and the scraps for the experiment . Love from India. ❤️❤️
@philipbender9562 жыл бұрын
Thanks, I am happy you enjoyed the video 🤗 😀 Try searching "gold fingers" on eBay. You can also find all the equipment and chemicals there.
@philipbender9562 жыл бұрын
Amazon is also good they have the best price on potassium nitrate. Pyrotechnic grade.😀
@somsackvongsa7077 Жыл бұрын
@@philipbender956 edward scizor hand.
@homealchemy3 жыл бұрын
What is the name brand for the sulfuric acid drain opener? It’s looks so clear!
@philipbender9563 жыл бұрын
Rooto Professional drain cleaner. I get it from my local hardware store. It's not always clear sometimes they just forget to put the dye and inhibitor in it. The reaction will still work fine if you have coloured sulfuric acid drain cleaner. Once you start the reaction the heat and acid will destroy any impurities in the mix. The solution will go clear very quickly. I hope that was helpful. I am happy you enjoyed the video
@valtercisco3 жыл бұрын
Is it possible to use the bottom of a stainless steel distiller to heat the mixture and the rest of the process in glass tubes?
@philipbender9563 жыл бұрын
Yes just make sure it's high-quality non-magnetic stainless steel.
@keithmorrison61763 жыл бұрын
to make the crystals do you put in the freezer or just in the regular part of the fridge.
@philipbender9563 жыл бұрын
To make crystals you need to chill the solution but not freeze it. I would advise you place in the refrigerator not the freezer.
@KD0CAC3 жыл бұрын
A few couple questions , I heard that high purity nitric acid will decompose - how to stop that ? Use of brown glass for storage ? Thanks
@philipbender9563 жыл бұрын
Yes, use Brown glass for long-term storage. Then keep in a cool dark place away from UV light.
@ivsongold3223 жыл бұрын
👍👍
@philipbender9563 жыл бұрын
😆🤗
@robertkorfanta90872 жыл бұрын
Hi. Thanks for all the videos. Can you use a nitric acid substitute instead of the stump out
@ahmedmahdi1849 Жыл бұрын
You can get potssium nitrate from a fertilizer bag containing the salt
@jhyland874 жыл бұрын
Question - On one of the videos on NileBlue (NileRed's second channel about random lab stuff and cleanups), he states that RFNA should be stored in a bottle only at like 50% of the volume, since the nitric acid fumes can build up the pressure and cause it to fail. Additionally, he said that he vents his bottle often, sometimes daily, to ensure pressure isn't built up. Do you do the same thing for RFNA storage?
@philipbender9564 жыл бұрын
I don't know about any of that stuff 😯 But just for good measure I did just check a glass bottle of concentrated nitric acid. That I made myself two years ago......... There was no pressure in the bottle. Everything looks good 🤔 Maybe Nile blue was speaking of some sort of peroxide compound. I know that can get explosive as it degrades with age.
@jhyland874 жыл бұрын
@@philipbender956 nope, it was RFNA. go to 1:30 in this video: kzbin.info/www/bejne/iYPNaHqmgZiFm9E
@front27605 жыл бұрын
Hi nice vid.Brings me back to when i was taking chemistry in school.I wondered though if it might not easier to pick up potassium nitrate from a butcher supply that sells spices and such.Might be a little easier i think.
@philipbender9565 жыл бұрын
I agree it would be easier. I have searched around. Extracting potassium nitrate from Spectracide stump remover is cheaper then just buying potassium nitrate. From 6 pounds of Spectracide stump remover you will get 5 pounds of potassium nitrate at a cost of $44.00. Every other source I have found is more expensive and has a shipping cost. With this method it cost about $55.00 per liter of %95+ nitric acid.
@front27605 жыл бұрын
Ya i forgot about shipping.I have around 1200 gm of sterling that i melted down so i now i need some nitric acid for the next step.Hence me watching these videos.
@philipbender9565 жыл бұрын
@@front2760 it takes about 800 mil of the nitric acid that I make to dissolve 1000 grams of sterling silver. I will be publishing a video demonstrating such in about a week.
@mahdiarghafarian40315 жыл бұрын
Did you work with RDX and PETN or plastic explosives ?
@philipbender9565 жыл бұрын
I have not worked with any explosives. I am more of a hobby chemist.
@kl.et.earth.com..1896 Жыл бұрын
I would have liked to create some nitric acid to purify my collected bit of gold that I have so far electrolytically refined with sulfuric acid, This video & other methods I have examined seem unpleasant & hazardous by the very nature of the subject of such strong chemistry, Though I don't really like the idea of evaporating a small amount of lead I think cupellation is by far a more acceptable approach to my fussiness really. Very interesting video thanks.
@MrKenny91513 жыл бұрын
This is a photo of a .9999 silver coin with something called a MilkSpot. Milk spots are believed to be caused by the cleaning process the Mint. The cleaning process involves some kind of detergent (not sure the type) but when some of this detergent is unintentionally left on and then baked in during the annealing process you get Milk spots. So that's why looking for the strongest acid or base that silver isn't affected by so as not to damage the coin itself and remove the milk spots.
@philipbender9563 жыл бұрын
Try using electrolysis to clean your silver coin. All tarnish will be removed instantly with electricity.
@BullProspecting5 жыл бұрын
Or if you could make a video on how to make a rudimentary Distillery that would be awesome. I don't know if that can be done but if so that would be super helpful. I'm trying to do gold recovery from computers and I want to get set up professionally so everything is safe. Thank you so much for making this video because it is awesome! You are the man! And I did not know that about the latex gloves thank you for sharing!
@philipbender9565 жыл бұрын
If you have very limited lab experience. You may just want to purchase your nitric acid. Making nitric acid is very dangerous especially if you have limited experience with distilling. I wouldn't make your own still if you're going to use it for acids. You can get a decent glass distilling kit for $35 on eBay. A fun and easy way to learn how to distill is to make your own ethanol. (Drinking alcohol) lt's a good way to learn and it's not nearly as dangerous as hot acids.
@bigacorns69 Жыл бұрын
@@philipbender956 in this case it may be important to distinguish the difference in ethanol, bought at a gas station and the ethanol in an alcoholic beverage.
@philipbender956 Жыл бұрын
@@bigacorns69 yes, the ethanol at the gas station. Is mixed with gasoline. I would call that denatured. The ethanol in beverages is safe to drink.
@vibeLia4 жыл бұрын
Can we used calcium nitrate directly substitution of potassium nitrate?
@philipbender9564 жыл бұрын
Yes, any nitrate salt will work.
@b.wakegijig26253 жыл бұрын
@PhilipBender say I just made Potassium Nitrate from Instant Cold Packs which was my Calcium Ammonium Nitrate then separated to only have Ammonium Nitrate which I then added Potassium from a No sodium Salt substitute. Will this work for this Nitric acid synthesis? If not what would you recommend to purify homemade ingredients? Such as the ones that later yield such a fine chemical like Nitric Acid.
@philipbender9563 жыл бұрын
Yes, go on Amazon and purchase pure potassium nitrate crystals. You can get them laboratory and pyrotechnic grade. Much cheaper than making yourself.
@chanheosican6636 Жыл бұрын
I plan to do this with calcium nitrate and 31% hydrochloric acid in reflux at 60 deg C.
@goldenscrab3 жыл бұрын
can i use NPK fertilizer instead of the potassium nitrates? its a fertilizer that contains nitrogen phosphorus and potassium, but about 60% if that is potassium
@philipbender9563 жыл бұрын
You would need to extract the potassium nitrate 1st
@goldenscrab3 жыл бұрын
@@philipbender956 using the same method you did at the begining of your video or there is another method for that?
@jayhanson2224 Жыл бұрын
I appreciate the video, but I some questions. What is typically the time it takes you to do the distillation process? How do you figure out the purity of your nitric acid? Could you maintain a 290 - 300 degree temp and extend your distillation time and produce more nrtic?
@GoldenAura323 ай бұрын
You could measure the density. Also once the boiling point passes whatever temperature you target you will no longer distill anything.
@imranammo Жыл бұрын
Hi Excellent video Is this caustic soda
@kgchrome4 жыл бұрын
two quick questions... 1. are you removing the fore run and lower boiling temp distillate that comes over before you hit 135C, or are you keeping everything that comes over above a certain temperature? if not, wouldn't that result in a lower percentage final product? 2. putting the thermocouple in the glass thermometer well only gives you the temperature of the air in the well, not the vapour temperature. an alternative would be a thermometer adapter with a PTFE seal, and a PTFE coated thermocouple probe, or a regular glass thermometer. thanks for the video.
@philipbender9564 жыл бұрын
I collected the entire run into one bottle. I started with fairly dry high-purity ingredients. The resulting nitric acid is over 95%. It will instantly ignite lab gloves. You will only make water down acid if you add water at the beginning of the reaction 😉
@philipbender9564 жыл бұрын
I wish I had a nicer thermal couple 🤓 I'm just grateful that I'm not stuck using the alcohol thermometer that came with the set 😳
@williamrussellmorley5 жыл бұрын
it was claimed saltpeter was added to our food in navy bootcamp 45 years ago ...
@antigen44 жыл бұрын
William Russell yes it was supposed to curb masturbation
@michaelsinaloense64494 жыл бұрын
Nothing short of amputation will stop an 18 yr old from doing the deed. Lol.
@LakshmiLakshmi-qy9uo3 жыл бұрын
Super
@philipbender9563 жыл бұрын
Thanks, I am happy you enjoyed the video. 🤗😀
@loneparvaiz36355 жыл бұрын
Nice, Sir please tell me which chemical is used for smelting silver ore it will be your most kindness
@JimNichols3 жыл бұрын
you *smelt* silver ore with heat not chemistry.
@vibeLia5 жыл бұрын
How to make ammonium phosphate into ammonium nitrate?
@BobSmith-es5wc3 жыл бұрын
thanks morgan freeman
@thepatriotrocker80014 жыл бұрын
Is there a way to refine the stump out to get pure sodium metabisulfite to use as a precipitant? Or would it just be easier and cheaper to buy the sodium metabisulfite
@philipbender9564 жыл бұрын
It is cheaper and easier just to purchase sodium nitrate from Amazon. I was demonstrating that it was easily extracted from the spectrum brand of stump remover. Only the spectrum brand contains sodium nitrate. Do not use stump remover containing sodium metabisulfite.
@thepatriotrocker80014 жыл бұрын
@@philipbender956 okay, thanks.
@mfrost17433 жыл бұрын
Hello man. Great video! I stumbled across this & learned alot! I'm wanting to try to make my own nitric acid as I currently have a bunch( fills up an entire 12x15 room) of computer & e scrap that I'm wanting to reclaim and refine PM's. I have some questions: 1) I'm wanting to use this single distribution simple distillation using 304 SS as the distillation tube( or as we call "the worm" instead of glass.( because I have an abundance of 304) glass filter flask as my pot, & a brown glass( lab grade that I haven't ordered yet) jar for the collection pot. Do you know of any problems this will cause? 2) After I reach 315 & stop distilling, can the sulfuric & nitrate in the still be reused or reclaimed to make future nitric acid? 3) couldn't I use the nitric to reclaim the pm from the scrap instead of AP? Seems like it would be much faster & probably produce more yield as efficiency would increase? This is a start, but can I please email you for more info?
@philipbender9563 жыл бұрын
Thank you I am happy you enjoyed the video.🤗 Yes you can use a stainless steel still. Just be sure to ensure the purity of the steel by using a magnet as 304 SS should be non magnetic. Once you have reached 315゚ keep driving it till It stops producing. The remaining product will be mostly Sodium bi sulphite. Not worth your time or energy trying to scavenge any remaining acid. As far as using nitric acid instead of AP. It takes about one Litre of concentrated Nitric acid. Per pound of scrap. To separate gold foils.
@RandyManu-jk1yn2 жыл бұрын
M>Frost hallo what is the abbrevation MP and AP ?
@cadillac85972 жыл бұрын
@@RandyManu-jk1yn PM=Precious Metals AP= Acid/Peroxide (a process to refine precious metals)
@RandyManu-jk1yn2 жыл бұрын
@@cadillac8597 okei!!! Thanks 💡
@chemistryscuriosities5 жыл бұрын
It's an endothermic not exothermic reaction
@claytonmccormick6223 жыл бұрын
once there was a harty scolor who is no more for what he thought was h2o was h2s04:=) i have noticed titanium camp cups and pots how hard would it be to convert one as a distillation rig as it would last a lot longer then borosilicate glassware as it would not crack from uneven heating or brake when dropped just wondering?
@philipbender9563 жыл бұрын
Sounds like a good idea.
@MmeHyraelle3 жыл бұрын
What else can you use? Havent found any stump remover in canada.
@philipbender9563 жыл бұрын
Sodium metabi sulfide
@JoSeeFuss2 жыл бұрын
Using such a higher concentration of nitric to dissolve silver, would you recommend making two containers of 95% nitric? In a proper bottle, how long can it be stored and in what temperatures? I live in the southern nevada desert
@philipbender9562 жыл бұрын
I have bottles of nitric that are 3 years old. It may be a good idea to keep it out of direct sunlight.
@joeestes81143 жыл бұрын
This is the expensive way! I can buy potassium nitrate for 3 dollars a pound on line and that stuff is over 8. Still awesome video!
@Ta2dwitetrash3 жыл бұрын
Far supply store near me has 55 lb bags for 55 dollars. I was suprised i found it so cheap.
@YTcontentconnoisseur3 жыл бұрын
Thanks for the great info! If you do completely dry and vac seal your KNO3, should you add some distilled water to the reaction flask?
@philipbender9563 жыл бұрын
No. The less amount of water the better.
@grahampike4882 жыл бұрын
Can you put the nitrate mixture in a plastic container in the fridge with a lid on it?
@philipbender9562 жыл бұрын
Yes, happy you enjoyed the video 🤗 😀
@johnh86154 жыл бұрын
Is the orange colour a contaminant?
@philipbender9564 жыл бұрын
Yes technically the orange color is a contaminant. The orange color is mostly nitrogen dioxide with a small amount of nitrogen trioxide. Both are caused by the decomposition of nitric acid. You can remove the orange color by bubbling dry air through the nitric acid. The orange color does not interfere with any metal refining reactions.
@GodJoker5 жыл бұрын
Did you add chlorine?
@philipbender9565 жыл бұрын
No the only two ingredients use were potassium nitrate and sulfuric acid. The only thing that reminds me of chlorine is the smell of nitric acid. It has a slight chlorine odor.
@Butterflytaxidfw5 жыл бұрын
Do you have to a glass beaker to do this? Can you use a metal pan?
@philipbender9565 жыл бұрын
You can purify your potassium nitrate in any container. I used glass so you could see what was going on for the video. I normally use a stainless steel bowl to purify my potassium nitrate. As far as making and distilling nitric acid. I would definitely recommend using glass. Hot concentrated nitric and sulfuric acid are extremely corrosive.
@Butterflytaxidfw5 жыл бұрын
@@philipbender956 I do not have a distiller I certainly do not have that expensive glassware. I looked to see if I could buy nitric acid but my friend told me that it is watched because of people making bombs. I want to use it for gold recovery
@philipbender9565 жыл бұрын
@@Butterflytaxidfw you can get a glass distillation apparatus off of eBay for $30. Just look up distilling kit. Also you can purchase 70% nitric acid off of eBay. the only reason the government would think you are making bombs with nitric acid is if you also purchase other bomb-making supplies and you start watching a bunch of videos on how to build a bomb.
@Butterflytaxidfw5 жыл бұрын
@@philipbender956 Cool I will check it out, I just do not want the feds knocking on my door. Thanks
@philipbender9565 жыл бұрын
@@Butterflytaxidfw I completely understand I definitely wouldn't want to break the law either. I don't think the feds would look into you unless you were purchasing gallons of nitric acid. Then they may be more curious as to how you're disposing of it versus whether or not you're making bombs.
@hugostiglitz44522 жыл бұрын
7:20 in a sense. its used to not let it degrade the joint grease causing a leak. thats why sulfuric acid is used bc it wont degrade it.
@philipbender9562 жыл бұрын
Yes. You can also just let the system seal itself. Take your pic concentrated sulfuric acid or concentrated nitric acid. They're both pretty nasty when you touch them as you take apart the rig to clean it.
@hugostiglitz44522 жыл бұрын
@@philipbender956 really???? ive never heard of doing that. ive always been told to grease with sulfuric with highly corrosive/basic distillations.
@rookthecook86755 жыл бұрын
how much potassium nitrate was it?can i use fertillizer?
@philipbender9565 жыл бұрын
I used 800 grams of potassium nitrate in this batch. A good rule to follow is to use equal amounts of potassium nitrate and sulfuric acid. If anything you should use a excess of sulfuric acid. You can use fertilizer that contains potassium nitrate but I would recommend extracting the potassium nitrate. If you just add sulfuric acid to fertilizer that contains potassium nitrate. The sulfuric acid and the nitric acid that you produce will react with the other chemicals present in the fertilizer. That will diminish your yield.
@emilaticha7224 жыл бұрын
Hello, How many grams of KNO3 and Na2S2O5 should be added to water ?
@philipbender9564 жыл бұрын
Add enough water so that you completely dissolve the kno3. But you want the solution to be saturated so use boiling water. As far as the na2s2o5 is concerned. That is useless for making nitric acid. Save it for precipitating your gold out of aqua regia.
@Rob337_aka_CancelProof7 ай бұрын
0:50 but this is the one you want to use for dropping that gold once you get it into solution
@tipxking99443 жыл бұрын
Would it have been easier to dry the potassium nitrate chrystals in a oven with a slight heat for quicker drying process?
@philipbender9563 жыл бұрын
Yes but it is a waste of energy.
@tipxking99443 жыл бұрын
@@philipbender956 that makes sense. Why is the nitric acid dense yellow at a higher concentration instead of clear? Do it contain sulphur contaminates?
@DFPercush2 жыл бұрын
@@tipxking9944 that's the brown NO2 gas, the reason it's called red fuming nitric acid. Very toxic. Above about 70% concentration it starts doing that, because some of the nitric acid decomposes into NO2. You can also dissolve NO2 back into water to produce weaker nitric acid.
@imsidetracted4 жыл бұрын
When you make the potassium nitrate crystals do the excess additives pour off down the drain?
@philipbender9564 жыл бұрын
Yes. What is left over is mostly the cutting agent. Potassium nitrate is extremely hydroscopic. It will pull moisture out of the air. I think they add something to prevent this from happening. And a small amount of dirt. Most likely from the facility where they store the potassium nitrate and mix the cutting agent. It should be safe to pour down the drain as this product is designed to be used outside in the environment. It is stump remover.
@imsidetracted4 жыл бұрын
@@philipbender956 thanks for quick answer. I just crystalized some potassium nitrate from China and it was heavier going in than it was coming out. I think the stump remove is more pure. More expensive tho so crystallizing it is great for me.
@philipbender9564 жыл бұрын
@@imsidetracted you can purchase pyrotechnic grade potassium nitrate off of Amazon. And it's cheaper than stump remover 😎
@imsidetracted4 жыл бұрын
@@philipbender956 I did 10lbs. Weighed it then crystalized it and it lost weight.
@TT-nh7rx3 жыл бұрын
What would be the best tubing to use to connect to a vacuum pump for making nitric acid?
@philipbender9563 жыл бұрын
Vinyl seems to give the best resistance to nitric acid. I purchased mine from a store that had aquarium supplies.
@TT-nh7rx3 жыл бұрын
@@philipbender956 cool, thanks for that. Finally... what kind of air vacuum pump do you use for this?
@philipbender9563 жыл бұрын
@@TT-nh7rx I don't know, you would have to find one that was chemical resistant. You don't need to run this distillation under a vacuum. I just attached a vinyl hose to my vacuum take off adapter and put it directly into my fume hood.
@TT-nh7rx3 жыл бұрын
@@philipbender956 Thanks for your help dude 👍🏻
@JimNichols3 жыл бұрын
It doesn't "create a Peltier effect" as this effect is created by thermoelectric devices it creates an endothermic process as it reacts with copper in air. BUT the rest of the video was very good science!
@MadScientist2672 жыл бұрын
That's ok "adding KNO3 to water will cause an exothermic reaction and the solution will start to cool down"...
@giansieger86872 жыл бұрын
Mad Scientific my thought exactly. Also he said hydroscopic… And why imperial temperature? I was thinking the whole time why he‘d heat to the BP of sulfuric acid. He coulda mentioned that at some point.
@mahdiarghafarian40315 жыл бұрын
Did you titrate it which you said its 95% ? or by density ? if from density you should first remove no2 or freeze that to clear the acid
@philipbender9565 жыл бұрын
I deduced the purity from density it weighed out correctly. Also if you don't add any water and you dry your ingredients. You will always produce a very high percentage. Another trick is to add a little extra sulfuric acid to gobble up any water present.
@mahdiarghafarian40315 жыл бұрын
Yes Your acid is RFNA due the dissolved excess NO2 which forms as N2O4 in that but it has less than 2 percent water
@Salty4eva5 жыл бұрын
is this process significantly cheaper than buying Nitric Acid? Or are there other reasons for using this process?
@philipbender9565 жыл бұрын
Yes it is cheaper to make the acid. Also the acid I produce is much stronger than the store-bought. The best you can purchase online is 70% the acid I make is greater than 95%.
@firasabbis80564 жыл бұрын
You can make HNO3. From. NaNo3+Hcl ----------> HNO3+NaCl
@metamorphicmuttmetall.l.c.68485 жыл бұрын
I believe the reaction at 2:10 is endothermic not exothermic.
@philipbender9565 жыл бұрын
Yes you are correct I was thinking endothermic but I said exothermic.