I hit the jackpot with this device - many times higher palladium content than the one declared by the manufacturer: 0.4g vs 8.5g Pd
Пікірлер: 148
@djbeacon68952 ай бұрын
Back in 1995 I headed up a project to replace Pd in MLCCs with Ni. Pd was then about $75 / t.o. Did calculations on how much the project would save the company if Pd went up to $100 and even 150 / t.o. We went ahead and completed in 2001. Saved the company 100s of millions of dollars per year.
@blacklabelonthebedrocks2 жыл бұрын
Great piece of scrap, great result! Good to see you are back, looking forward to upcoming videos. Best regards from Germany.
@OwlTech3332 жыл бұрын
Thank you very much!
@steven22122 жыл бұрын
Merry Christmas Owl! Great vid!
@OwlTech3332 жыл бұрын
Merry Christmas to you too! Thanks for watching!
@SURFEAMORETERNO2 жыл бұрын
One more time, a good job. Great video mr. Owl.
@julianalcorso57032 жыл бұрын
Oh, and I should have added that there has never been any doubt about your refining skills!
@chosen1one9302 жыл бұрын
Always good to see new videos from you
@OwlTech3332 жыл бұрын
Glad to hear it! More to come!
@colonialcharlie87022 жыл бұрын
Thanks for the labelled pics! There's great variety in those vintage boards, hopefully there's as good pd in the ones i find here. 😀
@OwlTech3332 жыл бұрын
I hope so too!
@julianalcorso57032 жыл бұрын
Hey Owl, I haveonly just caught up with this vid. Your editing skills have improved dramatically!! Well done you!
@OwlTech3332 жыл бұрын
Thanks!
@escrapchannel2 жыл бұрын
When I watch your videos I feel like in medieval alchemistry lab! Beautifully explained are all processes! 🌟 🌟 🌟 🌟 🌟 👍
@FollowMe2aMillion2 жыл бұрын
Great video, hope all is well. We missed you!
@NOFX08902 жыл бұрын
Pro recovery Owl tech, with what you had available. Thanks for the vid, a pleasure to watch. From Aus
@cabulingue2 жыл бұрын
all Ure videos are great. and the material you recover is also very good stuff. wish you good health always
@OwlTech3332 жыл бұрын
Thanks for the kind words
@davidgold5312 жыл бұрын
It is a long time we havent see you!! Thanks make many videos please!!! Good new format
@OwlTech3332 жыл бұрын
Thanks, will do!
@royalrefining61822 жыл бұрын
Nice work as always
@OwlTech3332 жыл бұрын
Thank you! Cheers!
@dr.a0063 ай бұрын
Awesome! Those old things made back when Au, Pd, Ag, Pt were somewhat cheap.
@OwlTech3333 ай бұрын
Yes
@ilmarzeiger7292 жыл бұрын
Very good videos! Thank You Owl Te ch!👍🤩👍
@OwlTech3332 жыл бұрын
Thank you too!
@ManMountainMetals2 жыл бұрын
Vintage electronics tremble when this man walks by.....😉👍
@tawnihaynie10652 жыл бұрын
Welcome back my friend. Great video. Please take care and stay safe. 🙂🙂🙂😇😇😇❤❤❤❣❣❣👍👍👍
@SocratePrimusSapiens2 жыл бұрын
That's a great catch ! And, i may say, it's a game we love : Finding treasure where others see nothing. always a pleasure to see your vids ! Regard.
@OwlTech3332 жыл бұрын
Thanks! Always pleasure reading your comments!
@fazluddinmalik42712 жыл бұрын
thanks a lot for support
@user-le3ps2vc7e2 жыл бұрын
Nice to see you again 👍
@OwlTech3332 жыл бұрын
You too
@nyangotomoses65442 жыл бұрын
Thank u for ur good lesson ,iam watching u here in kenya ,keep on buddy
@andywhite822 жыл бұрын
Great video. Couple of thoughts to get a higher purity button. After converting Ag with HCl to AgCl and filtering, what about adding a few ml of 98% sulfuric acid to precipitate any remaining Pb. Have you thought about using Zn to precipitate the PGMs instead of formic acid? I've found changing the Ph of acidic solutions to be too time consuming. Looking forward to your next video.
@OwlTech3332 жыл бұрын
I only started using sulphuric acid recently, didn't have it back then when the video was taken.
@carlogarcia67922 жыл бұрын
well done mate! great vodeo. thank you!
@OwlTech3332 жыл бұрын
Glad you liked it!
@farisfaris52822 жыл бұрын
Can you make videos on how to recover indium and gallium? They are scrap metals, but there are no videos on how to recover them and their price is acceptable, especially for people from developing countries
@dirceudepin77552 жыл бұрын
excelente,muito bom amigo,from Brasil!
@vincentrousseau81942 жыл бұрын
Na2co3, formic acid + naoh don t drop thé copper in the same time ? Or did you leave all thé copper with cuppelation ? Thank you , good vidéo like
@hasantokgoz30692 жыл бұрын
Allah razı olsun sağol kardeşim
@ivsongold3222 жыл бұрын
Very good 👏🏾👏🏾👍🏾
@OwlTech3332 жыл бұрын
Thank you! Cheers!
@mahmmud9802 жыл бұрын
Welcome tech good job
@frantiseklaluch66052 жыл бұрын
Great video, just question, why donť you precipitate lead with sulfuric acid and filter to remove lead? It is used when purifying gold, is it different with PGMs? There was quite a lot of lead on XRF analysis... Just curious...
@OwlTech3332 жыл бұрын
I didn't use H2SO4 back then, instead I used sulphamic acid , but didn't have any. It was a recovery process anyway that't why i didn't bother melting in a dirty crucible.
@frantiseklaluch66052 жыл бұрын
@@OwlTech333 OK, so get all the precisious metals, clean later (or sell as is...), legit... As I have heard, purification does not increase the price so much or not at all...
@hasantokgoz30692 жыл бұрын
Sağol kardeşim teşekkürler Allah razı olsun senden çok çok çok teşeķürlér diliyorum size Aslan kardeşim
@saint27573 Жыл бұрын
what kind of metal analyzer machine do you have ? Where did you purchase it ?
@mike99deanmike762 жыл бұрын
Only the best! What XRF do you use?
@OwlTech3332 жыл бұрын
Olympus
@gold999gang2 жыл бұрын
Nice video 🦉
@OwlTech3332 жыл бұрын
Thank you 🤗
@Amac-uz9hm2 жыл бұрын
What is the silver cement are where do you get it great to watch 👍
@OwlTech3332 жыл бұрын
kzbin.info/www/bejne/oIPKmaCbr8Zpgc0
@tinsoffish18102 жыл бұрын
Very nice💪
@OwlTech3332 жыл бұрын
Thanks ✌
@varlov55232 жыл бұрын
Сова как всегда на высоте. Спасибо за видосик и инфу.
@OwlTech3332 жыл бұрын
Спасибо за просмотр
@varlov55232 жыл бұрын
@@OwlTech333 нет проблем привет из эстонии таллинн.
@dizzious2 жыл бұрын
I noticed you didn't grind them to powder this time. Does all mlcc ceramic dissolve in pb/ag alloy?
@OwlTech3332 жыл бұрын
The video was shot a couple of years ago, only edited and uploaded now at that time I didn't grind the ceramics Wich resulted in longer processing time.
@jamisontaylor8782 жыл бұрын
Excellent video we're you guys bin
@AnggaSaputra-gj5xc2 жыл бұрын
how long does the process take when you add sodium carbonate+formic acid and naoh to get a black powder?
@OwlTech3332 жыл бұрын
10-15min
@chosen1one9302 жыл бұрын
What are the rectangle red boxes? They look like trimpot resistors but bigger
@OwlTech3332 жыл бұрын
yes they are
@asdepicas24 Жыл бұрын
Que tipo de aparatos llevan esos condensadores?
@quintonharvey1501 Жыл бұрын
Where did they come out of
@leventesomogyi6222 жыл бұрын
Hello OwlTech, I can see after the first "burning out" you always use high temperature smelting. I'd like to avoid this and was wondering if a "wet process" e.g. by dissolving the burnt capacitors in nitric acid or nitric acid / hydrochloric acid mixture could be used as well. Basically dissolve everything then selectively precipitate what you are not interested in then the PGMs. I would like to use the PGMs as catalysts hence not interested in producing a nice Pd/Pt ingot or medalion in the end. :-) It seems you have quite an extensive knowledge about these things, maybe you know a few things about the wet process as well. By the way, I'm curious why those old ex-Soviet capacitors contain so much PGMs? Thanks!
@ilmulogamdantehnikpelogama9569 Жыл бұрын
when giving caustic soda what while it is heated, sir
@user-zw4nu3mo5p2 жыл бұрын
Супер теперь пересмотрю разочков 5-шесть
@TrinityGoldRecovery2 жыл бұрын
to melting palladium which kind of crucible you use?
@OwlTech3332 жыл бұрын
Alumina crucible
@bazonis1gp2 жыл бұрын
👍👍
@spfein2 жыл бұрын
All that alchemy looks fun until the math starts lol
@whatwill18122 жыл бұрын
After long time
@OwlTech3332 жыл бұрын
better late than never ;)
@romanpankin54122 жыл бұрын
Лайк как всегда! А сколько золота в нем вышло в итоге?
@matthewcurry35652 жыл бұрын
I'm just curious on "dropping" metals from solution using SMB, and other's like you use. What exactly is dropping the metals? Is it just reducing the PH of the acid, or is there a real reaction going on to create the metallic forms thus "dropping" them from solution? If it really is just reducing PH wouldn't you be able to use like baking soda, or even water? Been a little confused on the chemistry of the formation of the aqueous solutions back into their metallics.
@OwlTech3332 жыл бұрын
For a metal to be in solution means that it has donated electron or electrons becoming a positively charged ion. In order to get it out of solution, or to "drop" it, the ion neeads to accept electron or electrons. SMB, and other precipitants give the electrons to the metallic ion so it becomes atom and drops out of solution.... The way I see it
@matthewcurry35652 жыл бұрын
@@OwlTech333 okay okay, so you need to dump in a negatively, or a reactively (-) charged substance to drop it out if I'm understanding that correctly. So in SMB it is the bisulfate (-) that actually does the work, and the sodium which is (+) doesn't do much. Thanks for the very insightful reply, and wanted to say I thoroughly enjoy your "outback hands on" style setup there. Especially using concrete as a cupel for example. So cheap, yet seems highly effective. Great stuff, and thanks again! (Let me know if I have that twisted, or backwards. Lol)
@OwlTech3332 жыл бұрын
In a nutshell yes!
@matthewcurry35652 жыл бұрын
@@OwlTech333 NICE! Glad I can comprehend these things now haha. Glad to hear that. Thanks again, and keep up the great work!
@matthewcurry35652 жыл бұрын
@@OwlTech333 So what I am reading is sodium carbonate should do the trick. It is also -2 valency just like SMB really. Unsure if the charge is the only factor, but it seems from our description that it works. Why would people use anything else with the prices I wonder?
@user-oj8ve2pt2x11 ай бұрын
رائع جدن وممتاز مقطع جميل كيف يمكن تحضير حمض الفورميك الترسيب
Does this apply with old American electronics old school stereos or the old projector tv
@OwlTech3332 жыл бұрын
Don't think so
@ilmulogamdantehnikpelogama9569 Жыл бұрын
In this video it is not shown when it is time to give a formic acit sir
@fherdian1002 жыл бұрын
How are u my friend ...
@thegolddrop76682 жыл бұрын
I can only get 67.5 percent nitric acid is this normal and what are you using to test the button what xrf analyzer is that
@user-bw6mo7cc1b11 ай бұрын
مرحبا عمل رائع جدن هل يمكن صهر المكثفات مع الرصاص الوحده فقط بدون فضه ومن ثم تبخير الرصاص بل البوتقه الاسمنتيه والحصول على البلاديوم تستحق تقدير والمتابعه والاحترام
@OwlTech33311 ай бұрын
Yes you can melt them even without lead, but you’ll need very high temperatures
@RizwanKhan-bi1ki2 жыл бұрын
How to wash silver chloride completely free from PGM. I tried but can't satisfy.
@OwlTech3332 жыл бұрын
try with dilute HCl
@Avci__ Жыл бұрын
Sir, I extracted palladium of a very high caliber, but I was not able to melt it. Do you have a suggestion for me in the process of smelting?
@alexhsabro20282 жыл бұрын
Хотелось-бы посмотреть на иностранную технику с подобным содержанием.
@muriaticacid70042 жыл бұрын
Thumbs UP
@SashaRybachok2 жыл бұрын
👍
@yuryandy8612 жыл бұрын
Спасибо за ролик, отличная работа 👍 и с возвращением, отдельное огромное спасибо за русские субтитры, мой англиский далеко от совершенства 😁 Будь здрав!
@OwlTech3332 жыл бұрын
Спосибо за просмотр!
@yuryandy8612 жыл бұрын
@@OwlTech333 написал в контакте, если не против есть моменты которые хотелось бы обсудить
@habeebnawab4212 жыл бұрын
Can u help show how to separate pd & pt
@OwlTech3332 жыл бұрын
Ok
@sxfvvgcd4829 Жыл бұрын
فيديو رائع ماء المواد التي رسبت البلاديوم او ماء المواد التي حايدت النتريك
@muhammadshahzad3602 жыл бұрын
website name where you find contain detail of frequency comparator
First sodium hydroxide or sodium carbonate I'm confuse. Please write subtitle so everyone can understand easily. 😉
@OwlTech333 Жыл бұрын
@6:23 NaOH - sodium hydroxide, @10:59 whatever base you have handy Na2CO3 milder reaction - slower, NaOH vigorous reaction - faster
@rohitlkv Жыл бұрын
@@OwlTech333 nice bro and one more question when u added formic acid. Thanks 😁
@mouhametmana30512 жыл бұрын
bienfait
@tawnihaynie10652 жыл бұрын
🙂🙂🙂😊😊😊
@AaaBbb-xn8bk2 жыл бұрын
А при купиляции в щолочи...потери палладия? NaOH-растворяет при сплавлении палладий
@OwlTech3332 жыл бұрын
Нет
@sheilaboothroyd4293 Жыл бұрын
We watch all that and then he never says how much precious metals are worth at the end??? What your doing is ace but I'd like to know how much money you've made, that's the whole point of what your doing?l.🛡️🧐
@OwlTech333 Жыл бұрын
you can make the calculation yourself 9.9g Pd times the spot price today it is $56.8 per gram which ads to $562
@user-sd1ur4bn2r6 ай бұрын
Даже не удевлен)) Щас подобные ковыряю Добро народов СССР не экономили на производстве
@user-ed5wv7fb3y2 жыл бұрын
Здравствуйте! Купаж ето хорошо 👍 но я предпочитаю кислоты!) ЛАЙК вам ✌️