melting PALLADIUM BLACK

Converting yellow palladium salt (Palladosammine Chloride (NH3)2PdCl2) ) to palladium black and melting it into a button.
#owltech #palladium #preciousmetals
Music: / awc6f

[@lukekingi2210]

Beautiful piece mate 👌

[@OwlTech333]

Glad you like it!

[@lukekingi2210]

@OwlTech333 of course, it's so hard to get nice Pd sometimes but I will have to try the borax to stop oxidation as it's cooling trick I just learned from this video. Thanks

[@Andrxox]

Отличная работа!

[@OwlTech333]

Спасибо!

[@asjordan4071]

سؤال لو سمحت … هل يذوب ملح البلاديوم بالماء فقط ؟ و هل اذا كان يذوب فطريقة تحويله الى معدن هي نفس الطريقة في هذا الفيديو ؟

[@OwlTech333]

يمكنك تحويل ملح البلاديوم إلى معدن بطريقة تسمى التكليس، لكني أفضل التحويل الكيميائي باستخدام حمض الفورميك.

[@asjordan4071]

@@OwlTech333 شكراً للرد …. لكن اسمح لي بالتوضيح اكثر من بعد اذنك … قمت بإضافة ماء ساخن إلى إحدى العينات الترابية و بعد الفلترة وجدت أن الماء قد انصبغ باللون الأصفر .. فقمت بتبخير الماء و وجدت اني قد تحصلت على ملح اعتقد انه ملح البلاديوم . سؤالي الان هل فعلاً من الممكن ان يذوب ملح معدن البلاديوم بالماء فقط بهذه الطريقة ؟؟؟ و هل اذا كلست هذا الملح بعد تبخير الماء عنه يكون قابل للصهر ؟

[@mdmuqeem9531]

Hey can we do this procedure with dmg yellow salt ? Please reply

[@OwlTech333]

yes

[@escrapchannel]

Fantastic quality of the refining and melt! 🌟🌟🌟🌟🌟👍

[@OwlTech333]

Thank you!

[@sxfvvgcd4829]

سلام عليكم اخي العزيز اذا كان يوجد في الماء الملكي رصاص كيف التخلص منهو

[@OwlTech333]

H2SO4

[@sxfvvgcd4829]

@@OwlTech333 اخي العزيز ألم افهم

[@WilXliFY]

Do you prefer NaOH vs NH3? And which Salt reduces quicker with Alkaline/formic acid, Yellow or Red Brick? I had some delayed issues yesterday reducing ~30 grams of red salt with HN3/Formic Acid. Seemed either not enough heat at first or my NH3/formic solution was to diluted.

[@OwlTech333]

Hi! Prefer NaOH, never reduced the red salt before so I don't know. As for you issues, heating to at least 85C is a must.

[@hamguer3653]

Good job you prof thanks for video

[@OwlTech333]

Thanks for watching!

[@sxfvvgcd4829]

فيديو رائع

[@DenisAlvarenga-es5bn]

Black paladio l thinkso l gotte sir,

[@NOFX0890]

Very nice button! I couldnt see the weight... ill guess maybe a little high, around 11g. Great vid OwlTech.

[@benlee4940]

9.48g

[@NOFX0890]

@@benlee4940 thanks.

[@OwlTech333]

9.48g Thank you!

[@lubomirmitkov7677]

Това е завотско рафиниране така се рафинира в целият свят точно така го правя и аз

[@OwlTech333]

Bravo!

[@lubomirmitkov7677]

След амоняка го въстанивявам с солна при пеха 2

[@ИванИванов-ш2т9р]

И накуя ты его плавил?? Не проще ДОРЕ получить отправить на завод за 5 % на афинаж?? Куда отработку деешь?? Соседям по даче сливаешь))

[@OwlTech333]

нет, не проще

[@ИванИванов-ш2т9р]

@@OwlTech333 Лицензия есть на драги?

[@naserait9479]

شكرا لك استفدنا منك ❤❤❤

[@بیفی-خ3ص]

👏👏

[@UrirhfUduruf]

سلام عليكم عندي بلاديوم اصفر كيف تحويله الئ بلاديوم هل ضيف عليه نتريك ام ماذا ارجو الرد

[@OwlTech333]

With formic acid

[@حسامالسعودي-س1ذ]

لو سمحت يافنان الفيديو نازل من غير ترجمة من فضلك اعد صياغة الفيديو بالترجمة

[@ProspectorTripp]

Beautiful dude! Score 👍 Peace Prospector Tripp

[@OwlTech333]

Thanks 👍

[@aliosmankucukpacalar]

Hi.What are the ratios of formic acid and sodium hydroxide?

[@OwlTech333]

No specific ratio used, just after adding the formic, add the NaOH on small increments, waiting to react between additions until all yellow salt turns black, then continue boiling for 5-10 minutes and it’s done. You don’t need much reagents - for this reduction I used roughly 50ml formic and 10-15g NaOH

[@goldnandobrowm5877]

Top você realmente mostra como se faz, parabéns 👏👏👏👏

[@DragMetall]

Здоров дружище! Красота!

[@OwlTech333]

Спасибо большое!

[@radiocomponent]

Привет, красивая палладиевая чернь получилась.

[@Mr.Intellectual]

👍

[@OwlTech333]

Привет! Спасибо!

[@SURFEAMORETERNO]

Hi Mr owl, good? The yellow salt is come from? Please.

[@OwlTech333]

MLCCS

[@ghostprotocol5876]

Nice.. Pd is very unique.. sometimes , i feel that palladium metal is alive😅 they expand sometimes. Like a metal sponge

[@ajingolk7716]

😑 why did speed up the video when melting! How much didt tooked?

[@OwlTech333]

5min

[@ajingolk7716]

@@OwlTech333 i melted palladium in less than one minute with arc but the carbon electrodes are a mess. Now i have rhodium 🤞

[@حسينالجنرال-ش3ج]

Hello, greetings to you for the wonderful effort, sir. I have a group of platinum mixed with sand, which is chloride. How do I start working on it?

[@АлексАлекс-ч5ы]

Озвучка повний пізд**. Дякую за відео

[@АлександрГаношилкин-ы6ы]

Здравствуйте! Отлично! Скажите, какую музыку используете в ролике?

[@OwlTech333]

Спасибо! Музыка моя: on.soundcloud.com/awc6F

[@zismistrator]

iridium please...

[@احمدالظاهر-ع3ظ]

مرحبا اخي فيديو رائع اخي هل ينطبق الامر على البلاتين كذلك بعد ترسيب ب كلوريد المونيوم التحويله الى اكسيد جاهز الصهر لك شكر وتقدير ❤

[@OwlTech333]

Ok

[@alllove1754]

How much would you sell that little button for? Have you given thought to opening a store or do you have one already?

[@OwlTech333]

This one was sold the same day it was made. Unfortunately it went for 20% below spot price

[@alllove1754]

@@OwlTech333 aww! HTe it when it gets away from us for cheaper than value! I remember when palladium was 10% what platinum was. It was like copper or maybe silver. Now platinum is palladium's junior league metal, like silver is gold's... anyways. Just curious.

[@hamguer3653]

Professionnel thanks for vidéo

[@ImanGoldRecovery]

thanks for goood video patron 🌹🌹🌹🌹👍

[@OwlTech333]

Thank you for watching!

[@alexhsabro2028]

Залипательное видео, приятно видеть как работает маэстро.

[@OwlTech333]

Спасибо за просмотр!

[@chieunguyen1586]

Rất hay! Cảm ơn bạn!

[@gomanatala8558]

جميل جدا جدا روعه تسلم استاذ العزيز بلتوفيق أنشاء آلله تحياتي يا من مصر

[@OwlTech333]

Thank you!

[@stelioschatzikyrgios9444]

Hello, very good job! I am converting the yellow salt using HCL and zinc, have you ever tried it?

[@OwlTech333]

Yes

[@Mr.Intellectual]

16 👍👍👍👍👍👍👍👍👍👍👍👍👍👍👍👍

[@OwlTech333]

Спасибо!

[@Rei.dos.metaies]

Qual foi o processo para obter o sal amarelo de paládio

[@OwlTech333]

There’s a video

[@ilmarzeiger729]

Very good videos,thank You Owl Tehc.👍🤗👍

[@OwlTech333]

Glad you like them!

[@yuryandy861]

Отличная работа👍 раньше плавил без буры или я ошибаюсь?

[@OwlTech333]

Спасибо! Тоже с буры плавил

[@nfyrav]

@@OwlTech333 Я палладий плавлю с содой Na2CO3

[@jamisontaylor878]

Very cool glad to see you back😊

[@OwlTech333]

More to come!

[@navrangstudio8273]

Sir how are you I have ground many stones and dissolved them in Aqua Regia (stones with stannous chlorid test show Platinum group metals) after urea adding SMB and some Iron sulphide ten grams dust was received around I once again made Aqua Regia to make pure gold, half of the dust did not dissolve, I do not understand what metal it could be.

[@مجیدفنایی-ب9ع]

ما برای کار کردن به چه صورت بفهمیم که فلز ما رادیوم هست ممنون میشم

[@DenisAlvarenga-es5bn]

Sir after is black color

[@OwlTech333]

What do you mean?

[@DenisAlvarenga-es5bn]

@@OwlTech333 sir when you finish litle be more late paladio is lite be more dark

[@diegohenrique3388]

Hello, good evening, my name is Diego, I'm from Brazil. do you have email so i can send some questions ?? for example: I have an ammoniacal solution containing palladium .... I added hcl and yellow pd salt precipitated .... IF I TAKE THAT YELLOW SALT AND ADD FORMIC ACID AND THEN GO PUT IN SODIUM HYDROXIDE, WILL IT BE BLACK LIKE THIS ?? .....I WORK WITH RHODIUM, PALLADIUM, GOLD AND SILVER ....IT WILL BE A PLEASURE TO EXCHANGE INFORMATION. HUGS

[@OwlTech333]

Yes it should be exactly as this

[@Mr.Intellectual]

[@abdulsattar70909]

So beautiful video I like it❤❤❤