How to calculate d-spacing / interplaner spacing from XRD data - 10

Interplaner spacing also known as d-spacing is the distance between two consecutive planes. In this video, I have used Bragg's law for the calculation of d-spacing from experimental XRD data. I used OriginLab and excel software to perform this operation.
If you have any questions or problems, just write them in the comment section below.
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Music Source
Unconditionally by Broken Elegance 🎩 soundcloud.com/brokenelegance Creative Commons - Attribution 3.0 Unported - CC BY 3.0 creativecommons.org/licenses/b... Music promoted by Audio Library kzbin.info/www/bejne/l2KxkGSvab6WfdE

[@RahulKumar-wx6jz]

Your all videos are much appreciated. Please keep the work up. Thanks.

[@ssewasingh]

Thanks for informative tutorial, i am new to the research kindly guide me what can be done if peak fitting is not perfect??

[@srivallikatepalli8234]

Thanks a lot for providing me software and helping me in my XRD data

[@abhishekgaurav4794]

Hi Nawaz, the video has soothing music with calm explanatory movements. Today first time I got this to watch, Its of immensely valuable for me. Query: d-spacing I calculated, its different for different planes, thus do we need to report its average value in manuscript. else please help me which d-spacing value we need to consider. Eagerly awaiting for your response.

[@srivallikatepalli8234]

Deep gratitude for helping me a lot

[@shriraamasokumar3887]

Thank you very much, this helped me a lot!

[@nanoworld6122]

Glad it helped!

[@goyenkaneelam]

What if peaks are not fitted well?

[@adithpola863]

Hello, the is video is very helpful, I followed the same, it is showing me that "Fit did not converge - mutual dependency exists between parameters. You may have overparameterized the fitting function. Fixing one of them may eliminate this problem". how to resolve

[@Nova_501]

How is it known the diffraction order is 1? Is it not different for different peaks?

[@keerthanapadma8742]

I thank you for your eminent work. I would like to clarify a few. How to find the corresponding plane hkl value for these calculated d spacing? For example, if I have d spacing as 2.3 A, whether it corresponds to plane 001?

[@WYS246]

Haha, I am also looking for an answer to this question. It seems that the interplanar spacing related to the Miller index is different from here, but I don’t know how they are related. For example, I want to know the crystal structure of a crystal (020) belonging to the monoclinic system. Do I calculate the distance between faces by d=nl/2sin(Theta)? Or is it calculated by dhkl=1/sinβ2*(h2/a2+l2/c2+2hlcosβ/ac+k2*sinβ/b2)?

[@harshitasrivastava5431]

Why its showing "Fit did not converge. Maximum iteration setting of 400 was reached" in my peaks? How can I correct It?

[@sebooz4949]

I have another version of the Origin Program I could not follow your steps, I dont have the same menu on the program, if I send my x-uy data cold you calculate the d-space for me? of teta? highly appreciated

[@phantomserhat]

hello thank you very much for your effort. You are doing appreciable job. I would like to ask that the d spacing values corresponding each peak you found are different so for such an analysis what would be the number for d spacing at last? I mean will we get the average value or not ? I am looking forward to hearing from you

[@nanoworld6122]

check your email

[@SAHACOMMUNICATIONS]

Same question for me also sir. Pls reply

[@sehrishnawaz8366]

Hi..if u got your answer, please tell me how we get the single exact value? by average?

[@Muradsahar]

I am getting some negative values for d-spacing, is that allowed?

[@shrikant7812]

sir, how we get values of wavelength & order of diffraction? , which value we will use?

[@antonioculebro8038]

Muchas gracias, eres el mejor

[@livingnature7445]

Hi, nice video I have got a overview about how to calculate d space value... I have small doubt.. How to convert d space value in nanometer.

[@TheSmithing321]

Just divide your d-spacing value in Angstrons by 10. The relationship is 1 nm = 10 Â

[@AndinosMAKER]

Obrigado por este video. Estou trabalhando com difração de raios X. Atuando exatamente nesta área de distancia inter planar.

[@nanoworld6122]

This video might be helpful for you.

[@tasifranks7859]

Thank you for your excellent video. As there is a d-spacing value for each peak, and they are different from each other. So when reporting the d-spacing value we should mention the corresponding peak. Is this right? If not, how can we determine the exact d-spacing value? Many thanks.

[@niushash7928]

Thanks for your amazing videos. I have a question for you, my highscore software doe not work "search peak", so I cant continue the next steps, is there any setting for software to active ''search peak''?

[@nanoworld6122]

It should, What version you are using?

[@duhasaadi350]

keep on doing this video

[@victorruiz4331]

Thank you so much

[@oilandfatsknowledgehub]

What to do if fit did not coverage?

[@nanoworld6122]

then fit each peach individually (one by one)

[@marwahmappiasse9330]

Thank u sir

[@aminasworld4567]

thank youuuuu

[@iqrasardar7750]

Good

[@bhupendersingh1402]

Thank you sir

[@nanoworld6122]

Welcome