USP General Chapter 41 || Repeatability || Accuracy || Smallest Net weight ||
Пікірлер: 47
@gooselukas1317 Жыл бұрын
This was just what I needed to fill the gap in my knowledge. Thanks a lot!
@PharmaPill Жыл бұрын
Glad it helped!
@sydneysantiago974Ай бұрын
Thank you!!
@vijayparmar5455 Жыл бұрын
Superb so good like this video 💯👍🙏🙏
@PharmaPill Жыл бұрын
Thank you! Cheers!
@MIDCkamgar14 күн бұрын
1:19 good
@lekang8179 Жыл бұрын
thank you for summarizing this information!!
@PharmaPill Жыл бұрын
Glad it was helpful!
@rabiierraji30366 ай бұрын
...... 😅@@PharmaPill😮😮😮😮😮😮
@surendrababuchallagundla92492 жыл бұрын
Please do one video on reviewed oos guideline
@ramakrishnaguttula79412 жыл бұрын
Good information sir 👍
@PharmaPill2 жыл бұрын
Thanks Ramakrishna G
@rajuahmmed5882 Жыл бұрын
❤❤❤❤
@muralibond1373 Жыл бұрын
For rough top pan balance for monthly verification is only accuracy enough or we need to perform repeatability also..
@PharmaPill Жыл бұрын
As per European pharmacopeia Repeatability and Sensitivity. As per USP All 5 parameters required.
@bestisyettocome2645 Жыл бұрын
Sir what is the difference between smallest net weight and minimum operating weight ??
@sanjays1344 Жыл бұрын
Thank you informative
@PharmaPill Жыл бұрын
Glad it was helpful!
@shahid_palguni1 Жыл бұрын
Thank you for this video
@PharmaPill Жыл бұрын
glad it was helpful
@ajitjadhav607 Жыл бұрын
Sir, For accuracy test only weight shall be use for calibration or all weights shall be use for calibration?
@PharmaPill Жыл бұрын
Only one test weight is taken for accuracy test. Generally between 5 to 100 % of balance capacity weight is taken.
@ajitjadhav607 Жыл бұрын
Sir as per accuracy formula, if observed weight will get higher value than certified value then calculation results get in minus value, how we can write final results (limit is NMT 0.10 %)
@ajitjadhav6077 ай бұрын
Hello sir, Hope you are doing well. Let me know that a statement given in accuracy parameter that ' the test weight's max. Permissible error (mpe), or alternatively it's calibration uncertainty shall be NMT one third of applied test limit of the accuracy limit. Plz explain .
@solution24x50 Жыл бұрын
Hi Sir Please make video on Dissolution performance verification using USP Prednisone tablet..I have gone through certificate but not able to understand
@vijaybirhade9424 Жыл бұрын
Why we are selecting 5 gm weight for repeatability test on analytical Balance? Plz tell me about this sir.🙏
@PharmaPill Жыл бұрын
Just check is it 5% of your balance capacity? If answer is yes then you have selected this weight based on the European Pharmacopeia. As per EP to carry out Repeatability test, weight should be in lower end and should not more than 5% of balance capacity.
@santhoshvarma9339 Жыл бұрын
Sir as per the formula if I perform, the answer is always 0.10 For suppose (2xsdx100)/2000xsd=0.10 Am right or wrong
@ajitjadhav6072 жыл бұрын
Is d value & least count is same ?
@PharmaPill2 жыл бұрын
Yes both are same
@ajitjadhav6072 жыл бұрын
Sir, if i perform repeatability parameter as per monthly calibration then there may be possibility of changes in SD every time. In this case how we can find out smallest net weight of balance ?
@PharmaPill2 жыл бұрын
Smallest net weight need to change based on your monthly Repeatability test calibration. But ideally you will see there will not be much change in smallest net weight because most of the time your SD will be less that 0.41 d
@ajitjadhav6072 жыл бұрын
Ok sir. i have a 5 digit semi micro balance with range of 1 mg to 200 gm. As per USP chapter we can calculate smallest net weight by using formula 2000 x 0.41d i.e. 2000 x 0.41 x 0.00001 = 8.2 mg. Then can i weight below 8.2 mg for any HPLC analysis. Most of the times we have very less quantity of CRS or Impurity standard so In this case, can we weight below 8.2 mg for HPLC or other analysis preparation?
@PharmaPill2 жыл бұрын
@@ajitjadhav607 excellent Question. Don’t use for weighing below 8.2 mg. You should use ultra micro balance or micro balance.
@bestisyettocome2645 Жыл бұрын
@@PharmaPill sir it means ye 8.2 least count hai How to calculate least count of weighing balance. Plz explain
@bestisyettocome2645 Жыл бұрын
@@PharmaPill sir it means ye least count h ??
@rameshmanda3877 Жыл бұрын
Sir. Why 2000 we are using .. why not use for 1000 could you please explain to us
@dashsubhasish56672 ай бұрын
What is certificate value
@manojmodi414 Жыл бұрын
Thank you very much sir
@PharmaPill Жыл бұрын
Most welcome
@bhuvip9204 Жыл бұрын
How to find minimum load of balance?
@PharmaPill Жыл бұрын
2000xSD is the formula
@bhuvip9204 Жыл бұрын
Ok but my question is to find SD u have to do repeatability. So while performing repeatability how many gm weight should I use? If i have 220gm balance..than how will I know what weight should i use for repeatability to get SD. Please do reply. Thanks
@ajitjadhav6072 жыл бұрын
Please explaine, In repeatability there is one note that is 'The test weight must be within the balances capacity, but the weight need not be calibrated.'
@PharmaPill2 жыл бұрын
Test weight must be within in operating range not balance capacity…
@ajitjadhav6077 ай бұрын
Hello sir, Hope you are doing well. Sir let me explain below; Repeatability formula = 2000 x SD / Smallest net weight Repeatability= 2000 x SD x 100 / smallest net weight Which one is correct and how ?