Split vs. Splitless Injection

  Рет қаралды 132,983

Restek Corporation

Restek Corporation

Күн бұрын

Пікірлер: 33
@bobbysumarso5965
@bobbysumarso5965 4 жыл бұрын
nice, rarely i got information i need with these kind of videos but this one is actually pretty good
@blackyme2889
@blackyme2889 4 жыл бұрын
i wish they taught us like this in pharmacy ,,, thank you man you helped me alot
@RestekCorp
@RestekCorp 4 жыл бұрын
You are most welcome!
@اشرفمصطفىكاملفعص
@اشرفمصطفىكاملفعص 3 жыл бұрын
You're the bestest in explanations
@okyoros
@okyoros 10 ай бұрын
Thank you for such wonderful explanation.
@sknagulmeera9633
@sknagulmeera9633 4 жыл бұрын
RESTEK is a Backbone to us
@RestekCorp
@RestekCorp 4 жыл бұрын
Thank you!
@giuseppezedde4553
@giuseppezedde4553 3 жыл бұрын
Your videos are a masterpiece! They are truly perfect, I congratulate you. I would be really grateful if you made a video describing all the steps of a gas chromatographic analysis. Thank you very much!
@RestekCorp
@RestekCorp 3 жыл бұрын
We'll have some more videos coming very soon looking at some details of both split and splitless injection.
@giuseppezedde4553
@giuseppezedde4553 3 жыл бұрын
@@RestekCorp Thank you very much! 👍
@xI777Ix
@xI777Ix 3 жыл бұрын
Restek are beasts when it comes to GC.
@sknagulmeera9633
@sknagulmeera9633 4 жыл бұрын
Thank you for putting knowledge increasing video
@RestekCorp
@RestekCorp 4 жыл бұрын
Our pleasure!
@aartigupta2390
@aartigupta2390 3 жыл бұрын
Great Explanation 💯💯
@jabutosu
@jabutosu 2 жыл бұрын
Very useful
@ramonverduzco3522
@ramonverduzco3522 2 жыл бұрын
In the diagrams of the inlet it appears that the column protrudes more into the liner for splitless injections versus split injection. Is this correct or am I taking too much from the diagrams? Thanks!
@RestekCorp
@RestekCorp 2 жыл бұрын
Column installation distance should not change between split and splitless.
@aartigupta2390
@aartigupta2390 3 жыл бұрын
In splitless type, why was the vent opened after sometime?
@RestekCorp
@RestekCorp 3 жыл бұрын
In splitless, the vent is opened to purge any remaining material from the inlet. Accordingly, it is important to set the time for when that happens correctly. You should allow time, based on flow rate and liner volume, for 1.5 to 2 liner volumes to pass through the inlet, then open the split vent to purge any remaining material.
@aartigupta2390
@aartigupta2390 3 жыл бұрын
@@RestekCorp Alright understood. Thanks alot💯
@halamboha50
@halamboha50 4 жыл бұрын
If you could make videos for other injection methods Thanks
@RestekCorp
@RestekCorp 4 жыл бұрын
We've some more videos on optimizing split and splitless that are in development. Any particular injection methods you are interested in?
@halamboha50
@halamboha50 4 жыл бұрын
@@RestekCorp Thanks for your quick response and I appreciate it. A lot of sample introduction methods in GC can be used such as: 1- Thermal desorption (single vs multi/ two stage) 2- Solid-phase microextraction (SPME)/ Headspace 3- Purge and Trap 4- Cold On-Column Injection 5- Programmable Temperature Vaporizing (PTV) Injection 6- Gas Sampling Valve These are some other sample introduction methods other than split/split injection method. Thanks
@RestekCorp
@RestekCorp 4 жыл бұрын
We have several videos in development for SPME right now, and most of the rest of your list are already on our idea list, but we will add the others. Thank you!
@willynmbithi5270
@willynmbithi5270 4 жыл бұрын
great one,i rememer Dr Shikanga,elaborating the same
@gazitec
@gazitec 4 жыл бұрын
best video ever
@thilpanneerpanneer2327
@thilpanneerpanneer2327 Жыл бұрын
How to calculate split rato based on column and split flow.
@RestekCorp
@RestekCorp Жыл бұрын
It is generally expressed as a ratio of split flow : column flow, so if you have 100 mL/min of split vent flow and 1 mL/min of column flow, you have a split ratio of 100:1.
@ИльназФахрутдинов-р6н
@ИльназФахрутдинов-р6н Жыл бұрын
@@RestekCorp problema hello, after replacing the burner, the chromatograph does not start, output 580000, and cannot be set on fire, can you tell me what the problem might be
@thilpanneerpanneer2327
@thilpanneerpanneer2327 Жыл бұрын
Nice explanation sir
@rajeshunique151
@rajeshunique151 4 жыл бұрын
thanks for the video
@Meraki.chemsci
@Meraki.chemsci 2 жыл бұрын
Excellent
@adosar7261
@adosar7261 4 жыл бұрын
How gas flow is in volume/time? How can we measure gas volume when it flows?
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