Synthesis of Ferric Pyrophosphate Nanoparticles

[@purushottammaurya2825]

Namaste sir one question This ferric pyrophosphate powder contain what percent of iron?

[@aparna6707]

Thanks sir but how can iron oxide or ferric pyrophosphate dispersed in water beacuse the process of nanoparticles is that precipitation and kept sometime than iron oxide or ferric pyrophosphate settle down. Is any nanoparticles is dispersed in water.

[@purushottammaurya2825]

Sir ethylene glycol food grade nhi h Yeh toh avoid karna chahiye Koi or option batao sir

[@aparna6707]

Sir can you plz make a video on whey protein/biopolymers stabilzed ferric pyrophosphate

[@aparna6707]

Sir give me suggestions that how to disperse ferric pyrophosphate in liquid solutions because it quickly segement.

[@aparna6707]

And how to decide ml of FeCl3 and sodium pyrophosphate required for reaction

[@mohamedanwar7548]

Sir are we can exchange ethylene glycol with propylene glycol ?

[@harshithapatel8253]

Namaste sir My desertation topic is synthesis of nanoparticles by organic method What is the difference beware organic & inorganic methods may you explain please 🙏

[@WorldofNanotechnology]

Please subscribe to my channel and post your comments. If you want to see any other synthesis of nanomaterials then write in the comment section.

[@aparna6707]

Role of ethylene glycol in making ferric pyrophosphate nanoparticles?

[@WorldofNanotechnology]

ethylene glycol is used to avoid agglomeration of the particles.

[@aparna6707]

Sir if you have any suggestions to figure out this problem or please suggest me any teacher or research paper which can help to solve the problem because it is very important for my project.

[@aparna6707]

Is biopolymers stabilzed ferric pyrophosphate in disperse in liquid solutions or is this any other method .Sir plz help me solve this problem to disperse nanoparticles on liquid solutions.

[@WorldofNanotechnology]

I have not worked with pyrophosphate, but I guess they are dispersed in water, or you can use alcohol water mixture

[@aparna6707]

Sir uplode the video of preparation of iron oxide nanopaticle by diffent method i.e. using teflon sealed autoclave.

[@soniaahlawat9130]

Sir ...please tell me how to make ZnFe2O4 nanoparticle by hydrothermal method if I take zinc nitrate and iron nitrate ....I want to synthesize 5 g ZnFe2O4 ....how we calculate amount of zinc nitrate and iron nitrate for 5 g ZnFe2O4.....please sir give me answer

[@WorldofNanotechnology]

Ok, I will send you an email soon

[@jigarpandya2563]

Sir, I want ferric iron phosphate seperated approx. 100% pure powder hoe can I achieve?

[@WorldofNanotechnology]

For what purpose you want to get the powdered form. Send me an email. [e-mail]

[@aparna6707]

How telfon sealed autoclave is different form autoclave?can I kept nanoparticles solution in glass vial and kept in autoclave ? in research paper written that transfer the solution in teflon sealed autoclave kept at 160c for 3 h . Where to kept autoclave in oven or elsewhere.

[@WorldofNanotechnology]

Teflon lined autoclave is different than autoclave used in bio lab for sterilization. Teflon lined autoclave is also known as hydrothermal bomb. It is used for doing reaction at high temperature and high pressure. It uses the autogenous vapor pressure of the solvent used in the synthesis. You can search for how to use this apparatus. I will upload the video in 2 weeks.

[@aparna6707]

Sir how to determine that amount of ferric chloride and ferrous sulphate like how much molarity is needed for iron oxide preparation.in different research paper their ml and molarity are different if any book regarding this plz suggest me

[@WorldofNanotechnology]

3.24 g of FeCl3 and 1.83 g of FeSO4 were dissolved in 100mL of distilled water, respectively. Then add 5%PEG and stirred for 10 minutes. Then the mixture was heated to 75◦C, followed by the addition of 2 mol/L NaOH solution until the pH value of the mixture reached about 11.5. Continue stirring for 2 hours at 60◦C. The resulting particles were separated by magnetic field separation, washed several times with distilled water, and dried at 80◦C.

[@aparna6707]

Sir for morphological examination of iron oxide nanoparticles using TEM and zeta potential .Can you suggest institute where TEM and zeta potential instruments

[@WorldofNanotechnology]

You can search in google for TEM and zeta potential facility in your city, in Delhi NCR you can go to JNU or IIT

[@aparna6707]

Sir can you plz tell me chemical equilibrium reaction of making ferric pyrophosphate nanoparticles

[@WorldofNanotechnology]

3 Na4P2O7(aq) + 4 FeCl3(aq) → Fe4(P2O7)3(s) + 12 NaCl(aq)

[@aparna6707]

Sir how you decide that taking 0.01 M FeCl3 and 0.01M OF SODIUM PYROPHOSPHATE AND 15MI ETHYLENE GLYCOL

[@WorldofNanotechnology]

I just made these solutions based on the method described in a paper. However, you should calculate based on molar ration in the chemical reaction.

[@aparna6707]

Sir is any way by which colour of iron oxide become white and it dissolves in water.

[@WorldofNanotechnology]

No, Iron oxide cannot be white, but it can be suspended in water. Search for Iron oxide colloid.

[@aparna6707]

Is this any way to extract iron from leaves ( spinach)

[@WorldofNanotechnology]

Read this paper "Extraction of ferredoxin from spinach leaves and its effect on Clostridium perfringens (anaerobe) growth " European Journal of Experimental Biology, 2013, 3(4):267-285

[@westernalliance3035]

sir we want to setup manufacture Ferric Pyrophosphate food grade unit in India can you help us for the same

[@WorldofNanotechnology]

I can definitely help you, send me an email [e-mail]

[@aparna6707]

Sir what is the range of theta(2O) for XRD of ferric pyrophosphate nanoparticles

[@WorldofNanotechnology]

You can scan between 10 degree to 60 degree. You may not get sharp peaks as the structure may be amorphous.

[@aparna6707]

Sir In your institute partical size and zeta potential determination is possible I can send my sample for analysis.

[@WorldofNanotechnology]

No we don't have

[@aparna6707]

Sir is any process that to decrease the specific gravity of nanoparticles?

[@WorldofNanotechnology]

I have not worked on these aspect of nanoparticles, please search the literature

[@aparna6707]

And the specific gravity of water is 1 and specific gravity of nanoparticles is around 1.5 or more.Thats why it settle down in water not dispersed in water.

[@sagarsharma3346]

Is this method of preparation called coprecipitation?

[@WorldofNanotechnology]

It is simply precipitation. Co-precipitation is when you have two sources of cations.

[@mansikale7939]

What is the amount of fecl3 is added in distilled water..?

[@WorldofNanotechnology]

If you are doing research then you should be able to calculate the amount based on molarity and volume. The Molarity and volume is given in the description of the video.

[@mansikale7939]

@@WorldofNanotechnology pls tell me ..amount of fecl3..i want to do project on this topic...plss its urgent

[@WorldofNanotechnology]

@@mansikale7939 If you are a high school student or college student and you dont know the formula of molarity then doing research does not make sense. First you need to understand the basics. Molarity = (Mass/Molar mass)/(vol. in litre) 0.01 = (X / 162.2) / 0.40 (If you are using anhydrous FeCl3, otherwise check the molecular wt. on the bottle) You calculate the X

[@aparna6707]

From the reaction mean that if we are taking sodium pyrophosphate 3M than 4M of ferric chloride and ratio is always 3/4

[@WorldofNanotechnology]

Yes, you can keep the volume same, and molar ratio 3:4

[@aparna6707]

Thanks

[@aparna6707]

Sir uplode the video on what is the purpose of telfon sealed autoclave and how it help in nanoparticles preparation. I have to give answer to my guide that how it help in nanoparticles preparation so sir plz uplode as soon as possible.

[@aparna6707]

Sir uplode video of synthesis of iron oxide nanoparticles via Teflon sealed autoclave.use of teflon sealed autocalve in video.

[@WorldofNanotechnology]

I will upload the video soon. Meanwhile you can see this video about how to use teflon lined autoclave. kzbin.info/www/bejne/b6HCg56sd916nqM

[@raghav484]

Sir can you please tell the process to make Ferric Pyrophosphate in bulk?

[@WorldofNanotechnology]

Send me an email [e-mail]

[@aparna6707]

Thanks sir

[@aparna6707]

Thank sir

[@aparna6707]

Sir your video is very helpful for my project, l am working on nanoparticles .Sir may l get your email for further communication.

[@WorldofNanotechnology]

[e-mail]

[@aparna6707]

Sir Please give me response as soon as possible. Thank you.

[@hamadzahur7443]

APARNA do you have sir whatsapp or email?

[@WorldofNanotechnology]

@@hamadzahur7443 [e-mail]

[@aparna6707]

Thank sir

[@aparna6707]

Thanks sir

[@aparna6707]

Thanks sir

[@aparna6707]

Thanks sir

[@aparna6707]

Thanks sir