SbCl3 Synthesis and Distillation (Short-path)

  Рет қаралды 113,686

Extractions&Ire

Extractions&Ire

Күн бұрын

In this video I buy some Antimony (an element I can't pronounce) and we do a high temperature distillation and put a pump in a kettle and put algae in my mouth. What could go wrong.
sciencesupply.... Have a look at this site. For full transparency, it is a bit of a sponsorship deal in the sense that I said 'hey could I have some glassware if I do something cool with it and show it off' and ScienceSupply said 'sure mate', so everything nice I say about them is genuine.
Also, if you do end up buying something from ScienceSupply, you can use the code SCIEI where it asks for a code. This wont give you a discount, and certainly doesn't give me any money, but lets you the company know that you went there because of me. That then goes on to show that KZbin Chemistry actually is a cool partner to work with, and might lead to more sponsorship things like this in future (if people think that's a good idea).
That purchase code again is SCIEI.
Cool. Anyway, Links:
Patreon: / explosionsandfire
Twitter: / explosions_fire
Subreddit: / explosionsandfire
Other Channel: / @chemicalforce

Пікірлер: 357
@haska9706
@haska9706 5 жыл бұрын
It's pronounced antimony
@ExtractionsAndIre
@ExtractionsAndIre 5 жыл бұрын
Did I eventually learn how to say it by the end of the video?? Or does it get more incorrect
@piranha031091
@piranha031091 5 жыл бұрын
@@ExtractionsAndIre Sounds like you're saying "antinomy"! ^^ think "anti-money" instead. (In french it's called "antimoine", litteraly "anti-monk"! Some say it might actually be the origin of the element's name, as quite a few monks were versed into alchemy, and might have poisoned themselves with it.
@jamesg1367
@jamesg1367 5 жыл бұрын
@@piranha031091 : At last!- the monk shortage of the mid-16th century is explained!
@piranha031091
@piranha031091 5 жыл бұрын
@@jamesg1367 "monk shortage of the mid-16th century"? Never heard of that, what are you referring too exactly?
@jamesg1367
@jamesg1367 5 жыл бұрын
@@piranha031091 : Pure humor, my friend.
@SHOCKTROOPER115
@SHOCKTROOPER115 5 жыл бұрын
Lmfaoo that quiet subtle “antimony” whisper at 2:17
@SHOCKTROOPER115
@SHOCKTROOPER115 5 жыл бұрын
2:15
@gitbig333
@gitbig333 4 жыл бұрын
Like voice acting you have a key phrase you say to get started and get ready. Like hes hyping himself up lol
@nikeipod1
@nikeipod1 Жыл бұрын
and then he pronounced it "antinomy" 1 second later. :D
@terawattyear
@terawattyear 5 жыл бұрын
Great vid. Massive color changes. Distillation of a metal salt at less than hellish temperatures. Rarely seen metalloid chemistry. Success. What more could we want? Thanks Tom!
@ExtractionsAndIre
@ExtractionsAndIre 5 жыл бұрын
Thanks for the comment! I thought this was going to be pretty boring when I first started so I'm pleased at how nice and interesting the video turned out
@PepekBezlepek
@PepekBezlepek 3 жыл бұрын
@@ExtractionsAndIre distilling inorganic stuff is VERY nice and interesting
@jabl6520
@jabl6520 2 жыл бұрын
@@ExtractionsAndIre I didn't reply that
@roymartin7713
@roymartin7713 3 жыл бұрын
I remember working in an analytical chemistry lab and being super careful with mg/L solutions of this stuff because it was toxic... here you are grinding up the raw product in your back yard 😄 I wish you a long and prosperous life.
@TomsLab
@TomsLab 5 жыл бұрын
11:12 good safe technique 👌
@jamesg1367
@jamesg1367 5 жыл бұрын
LOL. Yeah. I was thinking, "Is self-sacrifice the same as dedication?"
@ExtractionsAndIre
@ExtractionsAndIre 5 жыл бұрын
When you take as much MMS as I do, you literally cannot get a bacterial infection 😍😍😍
@danielgrantcoleman
@danielgrantcoleman 5 жыл бұрын
Probably didn’t need to pump any water through your short path. But I’ve tried that as well before. Just using an aquarium air pump works pretty well. The air cools it enough. But not too much. Cool synth tho
@ExtractionsAndIre
@ExtractionsAndIre 5 жыл бұрын
Good thought, I just didn't know how it would do with the short-path. The SbCl3 was still coming through real hot, like 100C, which was fine but without the water cooling it might have been 150C which is pretty high... Probably still fine though. Also, I don't yet have a air pump I could use here. I've got to build one for the ozone project so maybe this will be a solution I could do in future
@chilling_at_pontiff
@chilling_at_pontiff 5 жыл бұрын
"Antimoney" ... "alright we got our antinomey powder now"
@djsnowman06
@djsnowman06 4 жыл бұрын
My current job (pre covid, hopefully after I'll be back) is in the ball mill at an antimony mine. Dirty gig, but not my worst job.
@oak_meadow9533
@oak_meadow9533 4 жыл бұрын
excellent job, perfect example of use of short path condenser. congrats from San Antonio, TX USA Prof bill
@cmu5591
@cmu5591 5 жыл бұрын
It’s “heaps cool”.. Spot the south aussie...
@ExplosionsAndFire
@ExplosionsAndFire 5 жыл бұрын
Haha yeah goddamn this regional dialect
@Enjoymentboy
@Enjoymentboy 5 жыл бұрын
THANK YOU for this video!!!!! I was soaking some smd components (ie resistors, diodes capacitors etc) in hcl to get rid of the solder and it turned a deep lavender\purple colour. I also wondered what h2o2 would do and I got that same colour change to orange. Looks like I was dealing with antomony. You've saved my brain a LOT of trouble trying to figure this one out. Big thumbs up to you!!!!
@zockertwins
@zockertwins 5 жыл бұрын
I found another comment saying it might also be titanium: I will quote what Ian McClellan-Johnson wrote: That color change is possibly due to a peroxo-metal complex. I know titanium likes to do that. It dissolves at an ungodly slow speed in HCl forming a purple solution; and, when you add hydrogen peroxide, it suddenly goes a very intense and bright orange color as it forms peroxo-titanium chloride.
@Bloated_Tony_Danza
@Bloated_Tony_Danza 5 жыл бұрын
Antimony is used to harden lead alloys because it’s cheaper than tin, It also increases molten lead’s fluidity, and cavity filling properties. Hard lead is used in ammunition and lead-acid batteries. I’ve noticed that Antimony washes off of my hands VERY easily. So much more so than lead, which is by far the hardest thing to wash off my hands
@pyromen321
@pyromen321 5 жыл бұрын
I love the idea of putting the pump in a kettle! That’s some true ingenuity
@ExtractionsAndIre
@ExtractionsAndIre 5 жыл бұрын
I just kept pouring the hot water from the kettle into the foam box with the pump and then as I was doing it I just thought "........hey..."
@j_sum1
@j_sum1 4 жыл бұрын
Watching this vid again. Others have said the same, but I would like to confirm: there is Ti contaminant in the acid. I have the same brand and the same problem. It produces the same purple coloration of titanium trichloride. Then gives the orange tetraperoxo complex when the H2O2 is added.
@ExtractionsAndIre
@ExtractionsAndIre 4 жыл бұрын
I must've missed/forgotten that being mentioned, because that comes as a surprise to me. Titanium! That's a bit odd, how does it make it's way into there you think?
@j_sum1
@j_sum1 4 жыл бұрын
@@ExtractionsAndIre Yeah. Came as a surprise to me too. Not that I have done full analytics yet but nothing else I know matches. I think Ti4+ in the acid, reduces to 3+ when teacting with Mg or Zn (and other metals). Then hydrolyses to make fine cloudy precipitate. Try adding a little peroxide to the straight acid to see if complex occurs. The orange / beer bottle colour is indicative of peroxide complex. I have taken to distilling my HCl before use at the moment. The plus sude is that I am more accurate since I know the conc of the azeotrope. If I need higher concentration then I can always make some HCl gas to bubble through.
@Quickst3p
@Quickst3p 10 ай бұрын
The moment you said "trichloride" I first understood "trifluoride" and I remembered reading about Fluorantimonic acid and thought "Oh. This is gonna be interesting".
@Frostlander
@Frostlander 5 жыл бұрын
I've heard you say that the HCl you use is often contaminated with iron. Three colors associated with iron oxidation states are orange-red, green, and purple. I don't know how much iron is in the HCl, but this observation is worth considering.
@BillM1960
@BillM1960 5 жыл бұрын
If you want to make a better (and cheap) heater for your condenser re-circ water, I have found that if you use one of these generic plastic ammo boxes (or dry boxes of that style) you can drill some holes in the top and install an immersion heater. I do not mean the expensive ones from a scientific catalog but an element for a small home electric hot water heater (very cheap) through the side. You could use any container that has a top and I think probably a cooler if you wanted, but it's not necessary. You need to have a lid and a hole for a thermocouple wire. Do not let the heating element itself to touch anything but the water. You do not want it to be airtight so vapor can escape. You will need to top off the water periodically but you will worse with your open rigs. You can use a temperature controller if you like (but more expensive) but a rheostat is fine and an on/off (percentage of time) controller works just dandy for this as well. You can easily control the temperature to about 1 degree F once you get there (it takes a bit of time, but then you watch it and you have a much bigger dash pot at that temperature). Find the right place on your percentage on off controller (cheap) and boom. You can use it over and over again too. I prefer to use silicone tubing for this type of heated water though I know it's not needed and is more expensive, it is so much easier to work with and again you can use it over and over again, even for much hotter stuff. I really enjoy your channel! I don't know if that helps, but it works like a champ. Cheers!
@YodaWhat
@YodaWhat 5 жыл бұрын
One can use a simple Lamp Dimmer of appropriate wattage to control any resistive heating element, either the kind you mentioned or just incandescent lightbulbs. I have boiled water in a glass jar using the heat from a 500-watt (sealed beam) spotlight right below it, and it could go MUCH hotter with other fluids! A slight note of caution is in order if using glassware that may not withstand the temperature and/or rate of heating, and halogen bulbs will not last their rated lifetimes if used on dimmers. For additional safety, the lightbulbs could be put alongside the heated container, though there will be some loss of efficiency as the convective heating fraction will tend to be lost in that configuration. One may be tempted to 'be more efficient' by insulating the entire heater, but be wary of sealing up hot lightbulbs. They do need some cooling, and the normal wires and sockets even more so. Special bulbs, sockets and fiberglass-insulated wiring are available, as used to illuminate baking ovens; those can be run continuously at 560 K (550 ºF, 285 ºC, ) or a bit hotter. Silicon and Teflon insulated wires cannot long be used at such elevated temperatures.
@knisayusuf
@knisayusuf 3 жыл бұрын
@@YodaWhat Nicely explained.Thanks😊
@waynoswaynos
@waynoswaynos Жыл бұрын
Nice one friend, good suggestion. Also, for higher temps consider not using water at all but instead, place the element you mentioned in a metal box with sand inside. Old spiral stove elements are also good and cheap. I go to the local recycling and get such things for pretty much free. For really high temps, coat the glassware with a 1cn layer of clay that has a lot of sand worked into it so it doesn't crack too much when it dries. The clay supports the glass when it gets above the softening point. Pout a layer of Al foil around the clay to hold it all together. Regarding the element construction and if its up the the task. The outer casing is some form of steel (melts at 1500˚C), Inside is nichrome wire (also good for about 1500), surrounding the nichrome is a white powder which is magnesium oxide (good for 2700˚C). Also. I really like using the REX-C100 PID controller from ebay or aliexpress for about $10. They are great. By default they max at 400˚ but you can tweak the settings and get 1300˚C out of them. In conjunction with a simmerstat scavenged from the same old oven the element came from, and heat proof wire which I recommend you grab while you are at it.
@alllove1754
@alllove1754 Жыл бұрын
That material when you first pulled it out, it looks awesome. Like aluminum foil locked in glass.
@matty8944
@matty8944 5 жыл бұрын
Thanks for the Science supply mention It's nice to see at least some goods being produced here
@ExtractionsAndIre
@ExtractionsAndIre 5 жыл бұрын
Oh hi Matty! I was going to email this to you but you've already seen it, cool
@matty8944
@matty8944 5 жыл бұрын
@@ExtractionsAndIre Righto Thanks for the thought mate
@matty8944
@matty8944 5 жыл бұрын
@@ExtractionsAndIre Also if you ever come over to Perth and need Nitric acid go to AllChem. They sell 5L for $50
@jamesg1367
@jamesg1367 5 жыл бұрын
@@matty8944: Sweet deal! Think they'll ship a few of those to me here in the States? =-)
@ExtractionsAndIre
@ExtractionsAndIre 5 жыл бұрын
@@matty8944 That's a pretty great deal, thanks for the tip!
@Paveway-chan
@Paveway-chan Жыл бұрын
To me, "Antimony" was a girl from a webcomic about a girl going to a boarding school for science next to a magic forest. Imagine my surprise when I learned that it's an element 😆
@covodex516
@covodex516 2 жыл бұрын
11:13 I like how you spit a huge foamslime-spit into the coolant for that extra bit of zing
@theadventuresofdk
@theadventuresofdk Жыл бұрын
More inorganic Chem please! I signed up for inorganic 1 at school. It’s not required for grad school but I just wanted to take the lab. Then I found out it is only lecture and no lab! I made a solution of gallium chloride but I just filtered it and put it in a bottle after I made it becaue I didn’t know what to do next 😂(I’ve only taken 1st and 2nd semester chemistry so far, no distillations or extractions yet). But now I might try something like this. Also…. Make a gallium explosive 😁😁
@leebicmeme9455
@leebicmeme9455 5 жыл бұрын
Its ironic how i absolutely love watching you and Cody'sLab but almost failed Chem. back in high school.
@crystalmik8410
@crystalmik8410 5 жыл бұрын
Try to make some indium chloride. Just put some Indium or metallic indium waste into some hydrochloric acid and hydrogen peroxide. It sublimes at round about 418°C forming an iridescent snow as it resublimes what I think is really cool.
@ExtractionsAndIre
@ExtractionsAndIre 5 жыл бұрын
So you've done indium chemistry before? I haven't heard of many people doing things with indium
@crystalmik8410
@crystalmik8410 5 жыл бұрын
@@ExtractionsAndIre I got indium slag lying around as I melted some indium. Just for interest I decided to do some indium chemistry instead of throwing it away. The indium chloride solution was standing in my shelf for a couple of months until I was bored and looked up the properties of indium(III)-chloride. Eventually I boiled the solution in an ampoul, strongly heated the residue and saw the snow of the iridescent crystals forming as they resublime. Even though the reaction is still not that efficient due to yellowish indium oxide forming after strong heating. instagram.com/p/BnaxNGWnzsj/?igshid=4apurgb27t2v
@Rhodanide
@Rhodanide 5 жыл бұрын
@@ExtractionsAndIre And that's for good reason, Indium and its compounds are very expensive (for seemingly no reason!).
@richardsmith3199
@richardsmith3199 5 жыл бұрын
so what is a practical use for this synthesis?
@BothHands1
@BothHands1 5 жыл бұрын
What do you use it for?
@user-be4yc2vr5c
@user-be4yc2vr5c 5 жыл бұрын
The best master is an eternal student, my fren. Nice channel.
@MrAaronbill
@MrAaronbill 2 жыл бұрын
Just on my through the back log . Fuck I love your videos dude
@zenongranatnik8370
@zenongranatnik8370 Жыл бұрын
I did my engineering thesis about synthesising antimony oxides and as people said before, the white stuff is antimony oxychlorides or oxides. Main antimony source for my experiments was an old jar of SbCl3 which was very wet and hydrolysed. I had to manually scrape the white crust of oxychlorides from a few big crystals and then keep the chloride in a dessicator. I used to make solutions of SbCl3 in anhydrous ethanol and only in a beaker covered with some parafilm or the hydrolysis would occur. Maybe instead of distilling SbCl3 in dry HCl or chlorine, recrystallisation from an anhydrous solvent under nitrogen/argon wolud be enough? Also, my saples of antimony oxides/oxychlorides in ethanol would often change colour from white to orange the next day after the synth. Neither me nor my supervisor found out why it happened, but it might explain the orange colour. Probably nobody's going to read that comment after 4 years but hey, better late than never.
@ExtractionsAndIre
@ExtractionsAndIre Жыл бұрын
You underestimate how much I actually like reading comments lol. I wonder how my SbCl3 is going in the desiccator after all these years…
@zenongranatnik8370
@zenongranatnik8370 Жыл бұрын
@@ExtractionsAndIre If so, keep going mate. Great videos. I miss the ones from the first E&F channel tho. Tbh I thought that if I ever see antimony here it would be the famous *unstable* allotrope but this is a nice surprise too.
@luishoras9359
@luishoras9359 5 жыл бұрын
17:09 I'm already subscribed to both channels : )
@AsymptoteInverse
@AsymptoteInverse Жыл бұрын
Fun fact: One of antimony's historical uses was as an addition to wine at Roman banquets. They'd drink the antimonial wine, which would induce vomiting so they could eat more. en.wikipedia.org/wiki/Antimonial_cup Later, slugs of antimony were swallowed to cause bowel movements, then recovered from said movements for reuse. So that's fun.
@marcusv.443
@marcusv.443 6 ай бұрын
The "antinomy powder" broke me lol
@CAINE1984
@CAINE1984 3 жыл бұрын
I load and make my own bullets and lead wheel weights are great because it has a touch of antimony with the lead making the bullets a little harder. It's great shit!
@liamanderson6424
@liamanderson6424 5 жыл бұрын
Any advice on how to not dissolve as a person in general?
@johnmorrell3187
@johnmorrell3187 5 жыл бұрын
Cool temperatures, avoid acidic environments and avoid agitation, just the basics
@liamanderson6424
@liamanderson6424 5 жыл бұрын
@@johnmorrell3187 I'm quite a sour person so I'd dissolve more readily base
@TheOpticalFreak
@TheOpticalFreak 2 жыл бұрын
Why or when would you use antimony to use in fire proofing something, instead of using bromine?!
@TrippyFPV469
@TrippyFPV469 Жыл бұрын
2:16 *practicing off-camera": AntiMony A sec later on-camera: " Alright we got our antiNomy powder down here..." 🤣🤣🤣🤣
@vincesteffens898
@vincesteffens898 2 жыл бұрын
What if you drip perchloric acid onto it and then blowtorch it?
@Coffeemancer
@Coffeemancer Жыл бұрын
what chemical cant be doin in glass
@freehat2722
@freehat2722 2 жыл бұрын
Wasn't antimony used to start fires in matches? Specifically antimony trisulfide. Also in pyrotechnics.
@GerduoPaniroKhorma
@GerduoPaniroKhorma 3 жыл бұрын
You had me laughing at the very beginning, great content as always
@science_and_anonymous
@science_and_anonymous 5 жыл бұрын
Vacuum distillation?
@j_sum1
@j_sum1 5 жыл бұрын
Gorgeous. When you started I thought you were going to react with Cl2. Might be interesting.
@ExtractionsAndIre
@ExtractionsAndIre 5 жыл бұрын
I thought about Cl2, I don't often pass up an opportunity to use it, I've stated my love for working with it a few times before. But I think antimony is just a bit unreactive, so we'd need to heat the system too, and really dry the chlorine, and I think it looked just a bit messy. Glad I took the aqueous route
@jamesg1367
@jamesg1367 5 жыл бұрын
@@ExtractionsAndIre Aww, does this mean you're not gonna make the pentachloride? :-/
@ExtractionsAndIre
@ExtractionsAndIre 5 жыл бұрын
@@jamesg1367 I... wasn't even really aware SbCl5 existed. That's cool, maybe I will! Perhaps I should find something to chlorinate first
@wvcruffler123
@wvcruffler123 6 ай бұрын
Well thats fascinating. I want to synthesize butter of antimony from antimony trioxide instead of the elemental metal. Sb2O3 + 6HCl => 2SbCl3 + 3H2O. Have to so some stoichiometry to get it close. if I distill off the water what is left? SBCl3 and SBCl5?
@wvcruffler123
@wvcruffler123 6 ай бұрын
I should mention that the impure antimony oxychloride, chloride, and pentachloride eben hydrolysed might work for my applicaiton which is mixing it with an oil and using as a browning agent on steel rifle barrel. Butter of antimony may have been impure to begin with. And its completely removed after the fact.
@gordonlawrence1448
@gordonlawrence1448 4 жыл бұрын
Just watched this vid. Isn't Arsenick what you get if you shave your rear end with a blunt razor?
@mwilson14
@mwilson14 5 жыл бұрын
Have you been able to make the explosive form of antimony yet? :) I've got elemental antimony for my collection, but I've also got antimony I've extracted from old tire weights and bullets. I've also got arsenic from old bullets, but this is about antimony damn it. Anyhow, I don't know if it's the extremely small amount of antimony trichloride I have in solution, but the electrolysis is depositing antimony onto the cathode, but it's not explosive. It burns with that pale green flame seen with antimony, but no boom.
@waynoswaynos
@waynoswaynos Жыл бұрын
what process do you use to separate the Pb from Sb? I guess I would try dissolving with HN03 then precipitating the Pb with NaCl and if this leaves the Sb in solution maybe an iron rod would drop out the Sb..
@mwilson14
@mwilson14 Жыл бұрын
@@waynoswaynos I dissolve the lead in concentrated acetic acid with concentrated hydrogen peroxide. The antimony acetate that forms is a white solid precipitate. It is mildly soluble in water, but I know any of the white precip is not lead acetate so I can mechanically separate the two compounds from each other.
@waynoswaynos
@waynoswaynos Жыл бұрын
@@mwilson14 Legendary. Thank you friend
@waynoswaynos
@waynoswaynos Жыл бұрын
@@mwilson14 I found this recently that you might find of use. "Patent US1584151A Shimadzu Genzo, Process of manufacturing lead oxide". Quite a simple set up. Makes such a fine powderded Pb that the conversion to Lead Acetate would be almost instant. Quote "…this invention removes all these drawbacks, and consists in taking pieces of metallic lead into a revolvable drum, and revolving the drum slowly at a rate of about twenty-five revolutions per minute, blowing the air into the drum all the while. Then the heat generated by friction and oxidation (within the drum) of the lead pieces will raise the temperature within the drum and maintain it at not less than 60° C. The friction too will form new metallic surface on the lead pieces, which as soon as formed will be converted into lead suboxide by the heat and the oxygen in the air. The film of lead suboxide thus formed will be reduced to powder by abrasion, but not by lead pieces striking against one another, like in the case of a common tube mill or ball mill. When the lead suboxide film is abraded off, a new metallic surface will be formed, which as soon as formed will be abraded off as before, thus continually producing fine powder of lead suboxide intermingled with metallic lead powder directly and in dry condition. The lead suboxide powder intermingled with metallic lead powder thus, obtained is so fine and chemically active that if a lighted match be applied to part of its pile or a few drops of water be dropped on it, oxidation will instantly commence, igniting it briskly…"
@oneman7039
@oneman7039 4 жыл бұрын
whats the song at 14.22 ?
@JoshStLouis314
@JoshStLouis314 4 жыл бұрын
As far as metalloid chem goes, what should I do with 10g of tellurium?
@zeynabmahidashti3832
@zeynabmahidashti3832 4 жыл бұрын
Hi, did you distillated sbcl3 twice? The first time the excess amount of HCl was temoved? And the second time, sbcl3 itself was boiled? I didnt understand this part... Wat was the temperature? First time it was about 100 C and the second time it reached boiling point of SbCl3, i.e. 230 C? I need to synthesize SbCl3 :(
@ExtractionsAndIre
@ExtractionsAndIre 4 жыл бұрын
That's exactly it! You probably don't need to distill the SbCl3 if your antimony and HCl are pure enough. But I wanted very pure SbCl3 so I distilled it. I also just wanted to see if I could, as reaching a boiling point over 200 degrees C was a challenge!
@zeynabmahidashti3832
@zeynabmahidashti3832 4 жыл бұрын
@@ExtractionsAndIre Thanks for your reply. Yeah, I have pure Sb2O3 so I think the first distillation will be enough. And can I just use room temperature water for the first one as circulating water? And I have to add 20:80 HCl:Water ratio to my oxide to reach to the azeotrope? Right? Is the color of the azeotrope as orange as the one you showed in the video? Or your color is because of impiorities? Why should we use distillation? Cant we just let the azeotrope to evaporate freely and gather the remaining material as SbCl3?
@Arthropod108
@Arthropod108 5 жыл бұрын
Coolest video yet visually
@lidelong5513
@lidelong5513 4 жыл бұрын
Why not using a better chlorination method?
@californium-2526
@californium-2526 4 жыл бұрын
Make SbCl5. And then HSbCl6 in teflon. It is way easier to prepare than HSbF6.
@elijahberegovsky8957
@elijahberegovsky8957 4 жыл бұрын
Is there any chance, that you still have that antimony trichloride and can attempt making pentachloride by reaction with chlorine gas bubbling through the liquid? It would be awesome. Apart from numerous uses as a catalyst and oxidizer, it appears, that it can be converted to fluoroantimonic acid, if treated with concentrated HF. Always wanted to see it in work... Protonating benzene, dissolving wax... It's highly corrosive, toxic and such, but who cares when it's so cool. I'm just thinking of doing it in my lab. Is that as bad an idea as I think?
@ExtractionsAndIre
@ExtractionsAndIre 4 жыл бұрын
I can maybe make the pentachloride yeah, but no way am I working with HF!
@SuperAngelofglory
@SuperAngelofglory 5 жыл бұрын
SbF5 is used to make fluorine without electricity
@flomojo2u
@flomojo2u 4 жыл бұрын
It's very odd that antimony is somewhat toxic since I recently purchased some lead-free plumbing solder (I'm in the US) and it contains about 3% antimony (97% tin). A rather strange additive for solder used in home plumbing, perhaps it's just that unreactive in treated municipal water?
@ExtractionsAndIre
@ExtractionsAndIre 4 жыл бұрын
Yeah... hey it's a lot nicer than lead, but doesn't mean it's perfect
@TheChemicalWorkshop
@TheChemicalWorkshop 5 жыл бұрын
microwave, kettle, aquarium pump were not ment for chemistry but still work great
@AustinRichards
@AustinRichards 3 жыл бұрын
I love how he intentionally says it wrong and people still try to correct him.
@danielmclatchie5229
@danielmclatchie5229 5 жыл бұрын
0:22 whats that gem in the background...
@swaroopkunapuli7805
@swaroopkunapuli7805 5 жыл бұрын
New drinking game: Take a shot everytime he pronounces antimony wrong.
@TrapperAaron
@TrapperAaron 3 жыл бұрын
Wadda at by? I Luvs the "I heart Davy on ur slate!" Dont tell the wife but I keeps a picture of him in me shed too! Keeps the bys right suspect among the piles of emptys and girls of skidoo calendars.
@kajcio5
@kajcio5 5 ай бұрын
Isn't HCl with h2o2 piranha solution? Not reacting? Torture it with piranha solution
@Taha-hv6yj
@Taha-hv6yj 4 жыл бұрын
I didn't know gloves are necessary we touch antimony lead alloy all the time!
@dangerdackel
@dangerdackel 5 жыл бұрын
try a vac distillation
@stanwashighski3553
@stanwashighski3553 3 жыл бұрын
Do you have to obtain a special permit for a bonafide heat gun down under🤓
@pyromen321
@pyromen321 5 жыл бұрын
Antimininny trichloride
@michalchik
@michalchik 4 жыл бұрын
Antimony is a metaloid rather than a metal which is why it's brittle and easy to powder.
@Robo-xk4jm
@Robo-xk4jm 2 жыл бұрын
never heard of antimony
@interestingscience993
@interestingscience993 4 жыл бұрын
Hii bro I'm Indian master of chemistry student ❤️
@youtube.commentator
@youtube.commentator 5 жыл бұрын
And to think a war was lost against emus
@adamkilroe9840
@adamkilroe9840 3 жыл бұрын
You want to grind aluminium and magnesium just as easily? Put it in liquid nitrogen first. It will break very easily and grind very easily too as long as it's cold.
@Ubya_
@Ubya_ 5 жыл бұрын
antinomy :D
@GodlikeIridium
@GodlikeIridium 4 жыл бұрын
12:40 omg... Just air cool it xD
@SciDOCMBC
@SciDOCMBC 4 жыл бұрын
it seems you like toxic synthesis, why don't you make Phosphorus trichlorid
@b3dubbs72
@b3dubbs72 4 жыл бұрын
Make floroantimonic acid!
@scifisyko
@scifisyko Жыл бұрын
Antinamony
@vgernyc
@vgernyc 4 жыл бұрын
With Fluorine you can make one of the strongest acids ever.
@thevalorousdong7675
@thevalorousdong7675 4 жыл бұрын
Bit more complicated than just slapping the two together
@vgernyc
@vgernyc 4 жыл бұрын
@@thevalorousdong7675 I know but still
@saftplaysblitz8382
@saftplaysblitz8382 3 жыл бұрын
Antinomychloride
@borgmardunkleson2225
@borgmardunkleson2225 Жыл бұрын
Anti-money
@alexanderharrison7421
@alexanderharrison7421 3 жыл бұрын
I'm seeing a bunch of people pronouncing it Anti-money buy nobody else seems to pronounce it Anti-Mohny
@franglish9265
@franglish9265 5 жыл бұрын
🎶Antimony, antimony, antimony-chery, ... Antimony, Antimony, Anti.... mony... 🎶
@ExtractionsAndIre
@ExtractionsAndIre 5 жыл бұрын
Words have no more meaning now
@franglish9265
@franglish9265 5 жыл бұрын
@@ExtractionsAndIre it's sung to the Mary poppins Chim Chim? Song.
@franglish9265
@franglish9265 5 жыл бұрын
@@ExtractionsAndIre of course they have meaning! We all understood you, so linguistically your pronunciation was correct.
@TheGnome-Ad
@TheGnome-Ad 5 жыл бұрын
Anem meh nem meh nemony
@trevorday7923
@trevorday7923 3 жыл бұрын
Well, at least you weren't trying to make fluoroantimonic acid...
@FOATE
@FOATE 4 жыл бұрын
antiminy, antinimony, antiminey, antinimey, I believe thats all the pronounciations, all seems fine to me, but the ARSEnick dude? thats just not right
@richardsolomon5375
@richardsolomon5375 5 жыл бұрын
Should have put that in the wife's blendtech.
@Valdagast
@Valdagast 3 жыл бұрын
In the good old days they used antimony as a medicine, because why the hell not?
@someasianguy3793
@someasianguy3793 4 жыл бұрын
"Anti-moan-E"
@asmolbean9300
@asmolbean9300 3 жыл бұрын
It's pronounced an·tuh·muh·nee
@SodiumInteresting
@SodiumInteresting 2 жыл бұрын
I'm not getting any pretty colours just greenish 😏
@williamackerson_chemist
@williamackerson_chemist 5 жыл бұрын
an-tih-muh-ney
@YodaWhat
@YodaWhat 5 жыл бұрын
AN-tuh-MO-nee.
@leviwilder1205
@leviwilder1205 Жыл бұрын
anti-moan-ee
@rasiererhd2773
@rasiererhd2773 3 жыл бұрын
It is pronounced antamoany Ant-a-moan-y
@SoulsInsanity
@SoulsInsanity 3 жыл бұрын
It’s pronounced Alimony
@tmfan3888
@tmfan3888 5 жыл бұрын
I pronounce it as antimony, but my friend pronounces it like antimony, so we ask our teacher and he says we should pronounce it as antimony.
@ExplosionsAndFire
@ExplosionsAndFire 5 жыл бұрын
Wow go back and tell your teacher he is wrong and shouldn't talk to you like that
@jamesg1367
@jamesg1367 5 жыл бұрын
Wait. Repeat that...
@Rhodanide
@Rhodanide 5 жыл бұрын
Good talk. *claps*
@tmfan3888
@tmfan3888 5 жыл бұрын
@@ExplosionsAndFire *wot*
@oak_meadow9533
@oak_meadow9533 5 жыл бұрын
Antimonic acid is the most dangerous .....
@Blozox
@Blozox 4 жыл бұрын
1:59 jesus man... Your girlfriend must be a happy lady.
@3er24t4g1
@3er24t4g1 5 жыл бұрын
Dont reply to aussies
@ExtractionsAndIre
@ExtractionsAndIre 5 жыл бұрын
can't trust those aussie blokes yeah
@sazxcdewq123
@sazxcdewq123 5 жыл бұрын
@@ExtractionsAndIre pics.me.me/participate-in-australian-threads-read-australian-posts-always-respond-politely-1643255.png
@gabe97100
@gabe97100 5 жыл бұрын
Wow I'm not the only one who thinks that looks kinda like a giant meth pipe Am I ??? Sorry I know druggies are drawn to chemistry I'm clean but I love chemistry and you film in a way that is visible I had
@shootgunman1460
@shootgunman1460 7 ай бұрын
who is Anthony
@andie_pants
@andie_pants 5 жыл бұрын
I think it should be pronounced an-timma-nee. It just flows. "Ant-a-moe-nee" is like tripping on a crack in the sidewalk.
@andie_pants
@andie_pants 5 жыл бұрын
That being said, I have no urge whatsoever to pronounce alimony as "a-limma-nee", so yeah.
@whoeveriam0iam14222
@whoeveriam0iam14222 5 жыл бұрын
this guy is so rich he bought anti-money
@oitthegroit1297
@oitthegroit1297 5 жыл бұрын
I'm waiting for the woosh comments
@YodaWhat
@YodaWhat 5 жыл бұрын
We can make Anti Money, but only with great difficulty and much energy expenditure, as the coinage has to be crashed together in the light, at practically _the speed of dark._ ;)
@Ironfacebuster
@Ironfacebuster 4 жыл бұрын
That's called "investing in a kickstarter project"
@meme__supreme3373
@meme__supreme3373 4 жыл бұрын
Nah he wouldn't be able to have any of that here on Earth because the matter that makes up our air would react very violently with the antimatter that makes up the anti-cloth that the anti-people use to make their anti-money.
@TheGiselaSchumacher
@TheGiselaSchumacher 5 жыл бұрын
That color change is possibly due to a peroxo-metal complex. I know titanium likes to do that. It dissolves at an ungodly slow speed in HCl forming a purple solution; and, when you add hydrogen peroxide, it suddenly goes a very intense and bright orange color as it forms peroxo-titanium chloride.
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