Fixing of Negative intensities in scan data points error in X’pert Highscore - 26

In this video, I have shown the Rietveld refinement of XRD spectra using X’pert Highscore software. When performing Rietveld refinement through X’pert Highscore software we sometimes face many types of errors including the “Negative intensities in scan data points” error. In this video, I have shown how to overcome this error when performing Rietveld refinement. If you have any questions, ask them in the comment section below. For more videos, please subscribe to NanoWorld. Thank you.
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[@hayatimukhair5941]

Thank you very much!. Its help a lot

[@ANP-]

Thank you brother. God bless you.😊

[@camilafernanda359]

Thank for your vide was really helpful :)

[@mechtechwithsk3176]

please help me for solve "No structural data for simulation/refinement" for Rietveld

[@gabrielmoreiragoncalves7012]

Muito bom, obrigado!

[@universeman80]

Hi how do I calculate miller coefficients from xrd drawing and thanks

[@ahmadnajam1]

Please help me, what should be done to fix the "Last Iteration of Rietveld module failed" and "Floating Point division by zero" errors in the Rietveld operation? Thanks in advance

[@ms.cmozahimazizalamery7880]

Good evening Can you help please... I work in the field of X-ray data analysis I have data for samples consisting of five elements or more. When I perform matching on the highscore plus program, the international matching cards do not appear for me. What is the solution? Can you help?

[@smitanand1836]

kindly provide the link of your current version of xpert highscore software 3.5

[@kpsrikanth3567]

Initially I got -97 and after doing your process as above video it is showing -143.4. Again if keep -144 again it is showing -97 why this happening. I have both cod & icdd databases

[@md.sydulislam4362]

Thanks, but how to draw/graph this refinement XRD peaks from x'pert HSP to the origin software?

[@nanoworld6122]

I'll upload a video on soon.

[@hayatimukhair5941]

@@nanoworld6122 Yes, I am facing this problem too.

[@bindushree7048]

Can you please share the link of xpert high score

[@ravivarasada540]

Can you solve the issue seen in rietveld analysis error " No structural data for simulation/refinement

[@abouzidmohamed7646]

the same problem I don't know why

[@adilabbas542]

the same problem I don't know why

[@gauravrajak007]

Well you don't have the pdf4 database. You can find appropriate CIF files on COD open database for refinement.

[@edricgamer63]

Kindly upload Z-Scan calculation

[@nanoworld6122]

I'll try.

[@edricgamer63]

@@nanoworld6122 thank you so much

[@fatenhjikhsan]

Can I know why your icdd no start with 98-... But me start with 01 or 00? Is it because of pdf?

[@nanoworld6122]

Because I'm using 2 databases, the ICDD and COD. The COD database reference number start with 96-.... while the ICDD database reference no strat with 00- or 01-...

[@fatenhjikhsan]

@@nanoworld6122 ohh no wonder... If my database already have icdd , can I add database COD?

[@nanoworld6122]

@@fatenhjikhsan Yes