Indexing XRD peaks with hkl values using X'pert highscore - 25

In my previous video (link is given below), I have shown how to label XRD peaks with Miller Indices (hkl) values using OriginLab software. Indexing XRD peaks through OriginLab could only be done manually, while the X’pert Highscore software could do the same task automatically.
In this video, I have shown the labeling (indexing) method only. For a detailed analysis of XRD data through X’pert Highscore and OriginLab, please watch my other videos links are given below. If you have any questions, ask them in the comment section below. For more videos, please subscribe to NanoWorld. Thank you.
#NanoWorld
______________________________________
For more updates follow us on,
Facebook: / fascinatingnanoworld
Twitter: / nanoworld8
Instagram: / nanoworld85
Contact: [e-mail]
______________________________________
Interpretation of SAED pattern | estimation of d-spacing & (khl) values
• Interpretation of SAED...
How to put a scale bar on SEM & TEM images (SEM/TEM data analysis)
• How to put a scale bar...
No valid atomic position available (Rietveld refinement through X’pert Highscore)
• Fixing of valid atomic...
Negative intensities in scan data points (Rietveld refinement through X’pert Highscore)
• Fixing of Negative int...
Indexing XRD peaks with Miller indices (hkl) values using X’pert Highscore software
• Indexing XRD peaks wit...
How to plot JCPDS card with the XRD data using OriginLab software
• How to plot JCPDS card...
XRD data analysis using X’pert Highscore software
• XRD data analysis usin...
Deconvolution of photoluminescence PL spectra (PL peaks fitting)
• Deconvolution of photo...
How to find peak position and FWHM of XRD data
• How to find peak posit...
How to calculate crystallites (grain) size from XRD data?
• Crystallites (grain) s...
Estimation of grain size through modifies Scherrer equation
• Grain (crystallites) s...
Crystallites size and strain using W-H plot method
• crystallites (grain) s...
Calculation of nanoparticle size through SEM image
• nanoparticles size fro...
How to find Miller indices of XRD peaks?
• How to label XRD peaks...
How to calculate d-spacing from XRD data?
• How to calculate d-spa...
How to calculate lattice constant (a, b, c) values from the XRD data?
• How to calculate latti...
How to calculate microstrain and dislocation density from XRD data?
• strain and dislocation...
How to calculate crystallinity from XRD data?
• how to calculate cryst...
How to smooth XRD data?
• How to smooth data (XR...
Baseline correction for XRD data
• Baseline correction fo...
Cyclic Voltammetry Data Analysis
• CV Data Analysis throu...
How to find bandgap energy using the Tauc plot method?
• Band gap energy from a...
How to calculate bandgap energy using the Kubelka Munk function?
• Bandgap energy using K...
Understanding Tauc plot, 1240 (constant) and 2.303 constant
• Band gap energy (Tauc ...
How to know a material either have direct or indirect bandgap energy?
• How to know a material...
DSC Data Analysis
• DSC Analysis Through O...
TGA Data Analysis
• TGA Analysis Through O...
How to plot the double Y-axis in a single graph?
• TGA & DSC double plot ...
Electron paramagnetic resonance (EPR) data analysis (calculation of g-factor)
• Electron paramagnetic ...
_________________________________________
Music Source Unconditionally by Broken Elegance 🎩 / brokenelegance Creative Commons - Attribution 3.0 Unported - CC BY 3.0 creativecommons.org/licenses/b... Music promoted by Audio Library • Unconditionally - Brok...

[@anupamphysicist1]

Very nice... eagerly waiting for your next video...

[@hamidghaithan9650]

You are great. Thank you very much.

[@md.sydulislam4362]

Thanks, eagerly waiting for your next video. Could you please make some Detailed tutorial videos on VESTA software and also FullProf for Rietveld analysis..?

[@panconqueso1444]

Excellent video. Thanks a lot!!!

[@nanoworld6122]

Glad you liked it!

[@KundanYadav-xv7bu]

great help thanks a lot

[@MaryamHosseinpour]

Hi, thank you for your so much useful videos. I followed the steps as you said, but I get this error in the rietveld step: No structural data for simulstion/ negative intensities in scan data point. Can you please help me. Thank you.

[@MONIKASHRIVASTAV-bu3jk]

Hello Sir, I am not able to do the reitvield refinefinement as you shown in your video. Always a pop window opens which says no structural data available for reitvield refinement. Please help.

[@tapankumarpani]

Please upload a video about how to install x pert high score software.

[@erdinalmuqoddas9032]

How to show William-Hull in X'Pert HighScore sir?

[@user-il2ur7ps9y]

Hi sir, How can I calculate the value of young's modulus and Poisson's ratio from XRD data?

[@fadeelahchundekat35]

Hi, Thanks for the great video, but I have some queries regarding the hkl values. I have the same hkl values for zinc oxide as in this video, but they do not match the literature data. For example, in literature, the first three planes are namely (100),(002), and (101). But in the Xpert report, we can find that it is (010),(002), and (011). Can you explain these discrepancies?

[@jeongshim1018]

Hi, Thanks for this video with indexing the Miller indices. I have a question. If miller indices on experimental spectra are different from reference data (on the pattern list), what does this mean? something wrong?

[@nanoworld6122]

Then either you are matching it with the wrong JCPDS card, or your sample is not successfully synthesized.

[@hemapalleth7687]

sir. thanks for this video. but I am not able to do reitveld refinement. once I do start refinement it shows No data for refinement. How to solve this. please do help

[@shreyjain6447]

Why did you strip Ka-(alpha2) frequencies in this video? you didnt strip them in your previous video

[@johnsonjoel5856]

HI sir i am new to origin and xpert highscore . pls tell the procedure how you create the file ZN1(XRD).ASC FOR ME IT IS SAVING FILE AS OPJU

[@smitanand1836]

kindly provide the link of your current version of xpert highscore software 3.5

[@hiraiftikhar3524]

which file format of origin open in Xpert highScore plus??

[@arunavachatterjee2433]

Hi! Thanks for the great video. Performing the K-alpha 2 stripping generates a negative peak in my diffractogram, which prevents Rietveld refinement. Please advise!

[@sajidchem4u]

Hlw sir

[@sajidchem4u]

I need your help

[@faheemwani1996]

sir how to calculate lattice parameter of composite film Polyvinyl Achohol (PVA)-LaFeO3 with different concentrations

[@sakshithakur8927]

Thanks for the video, xpert highscore is not working in my case? any solution?

[@islamkhaaalil9451]

Thanks a lot, could u make.a video for how to calculate the ratio between the pahses in one material? for example I have Monoclinic... and tetragonal Phase in my.material and I.need to calculate the ratio between them either by XRD or retieveled refienment, Thanks a lot

[@nanoworld6122]

Noted! I will upload soon.

[@humairabibi4062]

Hi sir..I have followed same steps that you have told for background removal but instead of removal, background became more prominent... please guide what's the mistake in it?

[@sajidchem4u]

Please any one reply which file of xrd u open in it sir

[@shruthikn7477]

can you share me the data base which supports xpert highscore 3v

[@shuzukatoxicme2343]

Hello sir....how can I add more JCPDS data in XPERT High Score PLUS

[@hrishikeshdeodhar4698]

pls drop the link to this version of xpert highscore

[@ahmadaziz5263]

Thank you very much, very helpful video, but, why when I click start Rietveld refinement, then I keep getting no valid atom positions available?

[@nanoworld6122]

Here is the solution kzbin.info/www/bejne/pqGvoI2sn8yUmpI

[@ahmadaziz5263]

@@nanoworld6122 Thank you very much. You are very helpful.

[@pratikchoudhuri1694]

rietveld refinement is not working in my xpert high score plus, so I can't find (h k l) values. please solve the issue.

[@physicsworld2628]

@NanoWorld I try to Label XRD Peaks with Miller Indices (hkl). But there is not any option in of rietvield in Analysis. Can you help me what is the problem ?

[@namanshah9216]

same issue, the analysis tab contains only two features, cluster analysis (hidden) & search and match

[@sharminewz5632]

is ur issue solve? i got same issue

[@physicsworld2628]

@@sharminewz5632 NO still same issue

[@dr.shahidramay6728]

How to save four data files in one .ASC file? or to export all the data files after plotting in Highscore and then export it in origin?

[@sajidchem4u]

Sir only ASc file will open in it can we open any other file in it please reply sir

[@sajidchem4u]

Please can u provide me your mail please sir

[@dharmendrabarman6747]

Hi Sir, I am facing a problem in Rietveld refinement..Errors are coming at the time of Rietveld analysis..Could you please tell me how to do Rietveld analysis?

[@Chemist.FatmaFawzy]

I have the same problem . Please if you solve it tell me how?

[@nourihsane8886]

❤️👍

[@Kohli92]

In my software execute option is not opening what to do sir please

[@dikshathakur5695]

Hi sir in my analysis, match result is showing that no Candidate found . What do to in such cases.

[@sajidchem4u]

Sir after selecting metal from periodic table when I proceed next it's show no result found i have some issue with my high score

[@alkareddy1535]

Sir while refinement...my report shows problem.can you tell me what it is and it is due to what. Problem is No structural data for simulation Negative intensities in scan data point. Please give me solution

[@Chemist.FatmaFawzy]

I have the same problem . Please if you solve it tell me how?

[@satishkanna9428]

I'm facing an problem report stating negative intensity in scan data points so how to resolve this and add peeks of hkl value can anyone please help me out

[@kumarishalini4279]

Can we find hkl values in excel ?

[@nanoworld6122]

No

[@sheebasharon1360]

Sir, when I give rietveld, it is showing as no valid atom positions available. What to do Sir

[@MounaimBenhaddouche]

Did you get the answer ?

[@mravi76467]

Hello, sir when i go to rietveled - start to rietveled then it shows No structural data for simulation/refinement. What can i do sir?

[@mravi76467]

Sir, Can you share your X'pert Highscore software link to download