Interpretation of SAED pattern | estimation of d-spacing & (khl) values - 29

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NanoWorld

NanoWorld

3 жыл бұрын

In this video, I have shown how to analyze Selected Area Electron Diffraction (SAED) pattern using ImageJ software. Like my other videos, this is the only available video on the internet, which shows some very important and simple tricks for interpretation of the SAED pattern.
After watching this video, you will be able to calculate the following parameter from the SAED pattern:
1) 1/D (per nm)
2) 1/r (per nm)
3) r (nm)
4) d-spacing (Å)
5) Miller indices (hkl)
6) Indexing SAED pattern
If you have any questions, ask them in the comment section below. For more videos, please subscribe to NanoWorld. Thank you.
#NanoWorld
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Пікірлер: 112
@saharjafari2484
@saharjafari2484 Жыл бұрын
thank you for the useful and complete information.
@Hkvlogs1154
@Hkvlogs1154 2 жыл бұрын
Really Very helpful videos......... Clearly explained all things that we have to do
@ANP-
@ANP- Жыл бұрын
Thank you very much Sir. Please do make more videos on Characterization to help people like us. You are a very good teacher.
@juanca17063
@juanca17063 2 жыл бұрын
Thanks a lot, very well explained.! Regards from Mexico
@alexandrerodriguessimoes8020
@alexandrerodriguessimoes8020 Жыл бұрын
Thank you!! God bless you!
@dr.poojashandilya6885
@dr.poojashandilya6885 Жыл бұрын
Thank you so much your video is wonderful.
@MrShkolololo
@MrShkolololo 3 жыл бұрын
Thank for your tutorial, it was very helpfull!
@nanoworld6122
@nanoworld6122 3 жыл бұрын
You are welcome!
@gaanak6595
@gaanak6595 2 жыл бұрын
Thank you for this video
@HongNguyen-mb3io
@HongNguyen-mb3io 2 жыл бұрын
Thank very much for your usefull video
@clauberdalmas
@clauberdalmas 3 жыл бұрын
Excellent! Thank you
@nanoworld6122
@nanoworld6122 3 жыл бұрын
You are welcome!
@anishajoseph2353
@anishajoseph2353 Жыл бұрын
Very Informative video. Sir please put this type of analysis for all characterization methods
@fionajoylinemascarenhas5266
@fionajoylinemascarenhas5266 11 ай бұрын
Thank you very much for the video sir
@souravpan3068
@souravpan3068 3 жыл бұрын
You are doing really nice work.
@nanoworld6122
@nanoworld6122 3 жыл бұрын
Thank you! Cheers!
@priyankadogra3258
@priyankadogra3258 7 ай бұрын
Thankyou sir your vdieo help me alot❤
@fayzahtalbi3348
@fayzahtalbi3348 3 жыл бұрын
Many thanks. Please make a video on the Single crystal SAED pattern .
@ahmadaziz5263
@ahmadaziz5263 3 жыл бұрын
Thank you. awesome!
@nanoworld6122
@nanoworld6122 3 жыл бұрын
Glad you liked it!
@harishchandranishad6041
@harishchandranishad6041 2 жыл бұрын
Thank you for making this very informative video. I would like to thank you from the bottom of my heart. and one request is to please, kindly make one video on monocrystalline TEM SAED pattern analysis and spacing.
@nanoworld6122
@nanoworld6122 2 жыл бұрын
Noted
@vedant2136
@vedant2136 2 жыл бұрын
Nicely explained work . Thanks 🎉🎉
@nanoworld6122
@nanoworld6122 2 жыл бұрын
Thanks and welcome
@aryanfathoniamri956
@aryanfathoniamri956 2 жыл бұрын
Thank you very much for the tutorial. Please make a video about the SAED pattern of LRTEM. There is no scale in the SAED pattern
@Vinodpanwar94
@Vinodpanwar94 3 жыл бұрын
Thank you!!
@nanoworld6122
@nanoworld6122 3 жыл бұрын
Welcome!
@majidraza346
@majidraza346 24 күн бұрын
Thank you sir
@dhanyanp666
@dhanyanp666 3 жыл бұрын
Very useful videos, go ahead.
@nanoworld6122
@nanoworld6122 3 жыл бұрын
Many many thanks
@ahmedmalik9974
@ahmedmalik9974 2 ай бұрын
Nano world plz make such more videos
@asmasiddiqa8098
@asmasiddiqa8098 4 ай бұрын
thats great
@suranjanapatowary9524
@suranjanapatowary9524 Жыл бұрын
While indexing Miller indices in Microsoft paint, you have indexed the plane corresponding to the least r-value to the outermost circle. I am confused at this point.
@zahirmuhammad9133
@zahirmuhammad9133 3 жыл бұрын
Great job sir
@nanoworld6122
@nanoworld6122 3 жыл бұрын
Thanks
@DrHaffeast
@DrHaffeast 6 ай бұрын
Can I know why the biggest radius on the small circle or inside circle. Instead of outer circle? Suppose (200) should be place at outer circle. I am new to this can you clarify.
@mariappankaruppiah177
@mariappankaruppiah177 3 жыл бұрын
How pair hkls, When more than one hkl for a calculated d spacing?
@simransapra823
@simransapra823 3 жыл бұрын
Awesome..Really helpful...
@nanoworld6122
@nanoworld6122 3 жыл бұрын
Glad to hear that
@nanoworld6122
@nanoworld6122 3 жыл бұрын
Glad to hear that
@simransapra823
@simransapra823 3 жыл бұрын
Please make video for how to index spot pattern for HRTEM
@mariappankaruppiah177
@mariappankaruppiah177 3 жыл бұрын
If the d spacing lower than 1A How to identify the hkl?
@seenaselvam3326
@seenaselvam3326 10 ай бұрын
Kindly provide the JCPDS No for MXene..wonderful video
@rcfychemistry3082
@rcfychemistry3082 Жыл бұрын
How can we interpret the HRTEM images of nanoparticles and quantum dots..? Can u explain it in hindi..?
@adelal-salihy9451
@adelal-salihy9451 8 ай бұрын
1/r = 2(1/2r) Therefore, when calculating (1/r), you should have multiplied (1/2r) x 2, but I noticed that you are dividing by 2. Can you explain that please?
@TanvirAhmed-fh7mw
@TanvirAhmed-fh7mw 8 ай бұрын
Yes. I also noticed this.
@jinzhou4327
@jinzhou4327 2 жыл бұрын
Could you please also make a video on how to index spot diffraction pattern? Really appreciate it.
@muhammaddanishiman1951
@muhammaddanishiman1951 6 ай бұрын
hello there, do you know how to index spot diffraction pattern?
@aakashhossain7993
@aakashhossain7993 Жыл бұрын
I do not have any access to the JCPDS card for my use !! Is there any public domain from where I can access the JCPDS file ?
@Vinodpanwar94
@Vinodpanwar94 3 жыл бұрын
Please make a video on Single-crystal SAED pattern as well!
@nanoworld6122
@nanoworld6122 3 жыл бұрын
Noted
@shobhnathgupta2618
@shobhnathgupta2618 3 жыл бұрын
Waiting
@inamali2729
@inamali2729 3 жыл бұрын
Why you divide 1/2r values to find 1/r values ?
@priyankaphalswal482
@priyankaphalswal482 2 жыл бұрын
It should be multiplied by 2 not divide
@kavitayadav8351
@kavitayadav8351 3 жыл бұрын
Hello sir, will you plzz make a vedio on the wemple -Didomenico for determining the non- linear refractive index
@rajshekhar616
@rajshekhar616 5 ай бұрын
Going from 1/2r to 1/r, you should have multiplied 2 not divided 2. I do not know how you got the right answer?
@ranjitkate8396
@ranjitkate8396 2 жыл бұрын
Please upload the videos on d spacing calculation from HRTEM image and XPS convolution and deconvolution
@user-jq2kg4hl6o
@user-jq2kg4hl6o 3 жыл бұрын
Thank you for the informative video. Why didn't you use the formula L•lambda=R•d to find d - spacing?
@pinakmiku4999
@pinakmiku4999 Жыл бұрын
Is this that you are mentioning the bragg equation?
@LAURASILVANASALASCHAVEZ
@LAURASILVANASALASCHAVEZ 5 ай бұрын
no tienes el word editable ?
@harry-ho9ti
@harry-ho9ti 3 жыл бұрын
Sir pls upload more tutorials. Pls upload Vesta software tutorial.
@sanchiakharphanbuh251
@sanchiakharphanbuh251 2 жыл бұрын
Thank you for this video. Can I have JCPDS file for Mn2o3 and MnO
@solankianitaba9399
@solankianitaba9399 2 жыл бұрын
please gave information that my XRD data match with which number JCPDS FILE NUMBER
@kalpanagarg1301
@kalpanagarg1301 Жыл бұрын
How to get the jcpds card can you provide the link of your video in comment box?
@tariqmslihsaadalhgre9775
@tariqmslihsaadalhgre9775 Жыл бұрын
Great explanation, Can I have JCPDS file for Bi2O3
@bharathimeti7753
@bharathimeti7753 2 жыл бұрын
Thank you for this tutorial. Kindly give me all values for PCMO , jcpds no. is 89-795. Also for BCMO Jcpds no. is 57- 767.
@Mosesnewtechnology
@Mosesnewtechnology Жыл бұрын
Thank you for the tutorial, the math for converting 1/2r into 1/r may not be right. I think you are supposed to multiply not divide by 2. i.e 1/2r is a smaller value than 1/r. please check, thank you for the information
@dperea
@dperea Жыл бұрын
I think you are right, if 1/2r=n; then 1/r=2n. But then why it seems to be right when compared with the standard values in the card?
@harry-ho9ti
@harry-ho9ti 3 жыл бұрын
Sir wht ll b d next video. Pls upload next one.
@subinkc3539
@subinkc3539 2 жыл бұрын
JCPDS 44-0141 ?? can u pls share the jcpds file of alpha- MnO2
@meemalli3328
@meemalli3328 Жыл бұрын
Hi, could you please share me the terbium JCPDS data?
@research8540
@research8540 4 ай бұрын
Sir, 1/r = 2 times of 1/2r . Then How you did the half of 1/2r for 1/r ???
@anjalibaburajan2963
@anjalibaburajan2963 Жыл бұрын
Thank you soo muchh sir...can you please provide jCPDS card of Ceo2
@harry-ho9ti
@harry-ho9ti 3 жыл бұрын
Please do a vdo on ac conductivity fitting and how to calculate the atomic positions of a sample for rietveld refinement. Pls. suggest the site.
@nanoworld6122
@nanoworld6122 3 жыл бұрын
Noted
@ashwinichavan7447
@ashwinichavan7447 7 ай бұрын
Hi can u pls provide jcpdf of 15-0087.
@ahmedmalik9974
@ahmedmalik9974 2 ай бұрын
Plz make more videos.Very less videos on this channel are.
@sanmilankalita9058
@sanmilankalita9058 Жыл бұрын
Why did you divide 1/2r to find 1/r?????
@skylerxing7548
@skylerxing7548 2 жыл бұрын
Very brilliant video. But I am wondering if I am wrong about the 1/2r and 1/r in relative values, if anyone can tell.
@trithien3t
@trithien3t Жыл бұрын
I am also think that, 1/2r=a => r= 1/2a, but in this case r is calculated reversely
@SP-qv9ui
@SP-qv9ui Жыл бұрын
1/2r is not a 1÷ (2r) its 2r in reciprocal plane
@dongmeimaylin4188
@dongmeimaylin4188 3 жыл бұрын
from C column to D column , it should be 1/2r *2 = 1/r
@nanoworld6122
@nanoworld6122 3 жыл бұрын
You are right, But his is not the mistake. The actual mistake is, I measured 2R but mistakenly labeled it as 1/2R in the first place and then use R instead of I/R. However, the method and calculation is accurate. But you need just to consider the 1/2R as 2R, 1/R as R.
@sharafpc786
@sharafpc786 Жыл бұрын
@@nanoworld6122 yes.. i was wondering the same thing
@debashissarmah6390
@debashissarmah6390 Жыл бұрын
Required JCPDS Card.
@pratikshatanwade3781
@pratikshatanwade3781 2 жыл бұрын
When saed scale is 10 1/nm then what will be the calculations and to decide that?
@mehdikhadem2576
@mehdikhadem2576 2 жыл бұрын
just in the Image-J, Analysis>set Scale change 2 to 10. the rest of the process remains the same
@anjalisuryavanshi6971
@anjalisuryavanshi6971 8 ай бұрын
Hello sir can you provide jcpds card
@lakshmikantasain5667
@lakshmikantasain5667 4 ай бұрын
Could you please provide jcpds file of reduced graphene oxide and graphitic carbon nitride
@richasharma5993
@richasharma5993 2 жыл бұрын
Thanku sir very informative video. Sir please send me the JCPDS File for ZnO
@RohitSharma-yp5mg
@RohitSharma-yp5mg Жыл бұрын
Respected sir can you please provide me this standard values card ..???
@goyenkaneelam
@goyenkaneelam 3 жыл бұрын
How to index saed of crystalline materials
@nanoworld6122
@nanoworld6122 3 жыл бұрын
This video was for polycrystalline SAED pattern. However, I will upload soon a video on the interpretation of single crystalline SAED pattern.
@andreachan8944
@andreachan8944 3 жыл бұрын
@@nanoworld6122 Thanks a lot! I am looking forward to watching your new video.
@shobhnathgupta2618
@shobhnathgupta2618 3 жыл бұрын
Thank you sir. We are eagerly waiting for this.
@sanjeevip6701
@sanjeevip6701 3 жыл бұрын
Analyse single crystal SAED pattern!!
@nanoworld6122
@nanoworld6122 3 жыл бұрын
I will upload soon
@TheAbhi23456
@TheAbhi23456 3 жыл бұрын
Thanks for the tutorial, it was helpful. Can you please help me in my SAED pattern through mail, I have some specific questions about it.
@Ayu-rx3dz
@Ayu-rx3dz 2 жыл бұрын
Thank u so much for your guide sir. Sir, do you have JCPDS card no. 52-0875 for Ti3AlC2?
@nanoworld6122
@nanoworld6122 2 жыл бұрын
email respomded
@Ayu-rx3dz
@Ayu-rx3dz 2 жыл бұрын
@@nanoworld6122 Thank u so much sir, This really helped my research
@gunntea9545
@gunntea9545 2 жыл бұрын
Why d=1/R ?? I only know that d.R=L.landa Could you tell my why L.landa=1 ?
@chetanawasthi5610
@chetanawasthi5610 2 жыл бұрын
Please provide data for JCPDS file No. 290914
@nirmalkundu164
@nirmalkundu164 3 жыл бұрын
jcpds card no- 411445 for sno2
@BreakThroughBB
@BreakThroughBB 3 жыл бұрын
Sir.. please help me to analyse .. I calculated the d spacing but due to lack of jcpds card, I couldn't do it.. will you please provide your email address?
@nanoworld6122
@nanoworld6122 3 жыл бұрын
email address is available at the end of video.
@BreakThroughBB
@BreakThroughBB 3 жыл бұрын
@@nanoworld6122 got it sir❤️🔥
@sukanyaguharoy2739
@sukanyaguharoy2739 11 ай бұрын
What is your email ID?
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