How To Do Buchner Funnel Vacuum Filtration

[@samanthadavis3739]

I've always found it easier to mix the solvent and filter media in a separate flask and then pour the slurry into the buchner with the vacuum on, you get a more even filter cake. As long as you keep the vacuum on, you can add layers of other media on top the same way and they'll also come out even. I've also sworn off the fritted buchner funnels in favor of pore plates, you'll never get the carbon/polymers out of the frit unless you use piranha solution.

[@kevinweeks3824]

What exactly do you mean by a "pore plate" i am guessing a ceramic buchner? or perhaps a lenticular housing? thank you for the insight

[@birtday6326]

@@kevinweeks3824 The plate is perforated rather than fritted

[@birtday6326]

Couldnt agree more with everything you said. This video is an example of how not to prepare a DE cake.

[@michael2963]

What particle size is the celite 545 and what grit disk are you using in that buchner funnel? I know G3 wouldn’t be sufficient to filter out the celite 545 in most cases and I can’t imagine a 4-1 of ethanol to material going through a g4 that quick…

[@SotoAdvert]

Make a video how to clean the filtration flask

[@dis_guy7]

please listen to this comment pleaseeee make a video

[@brutusjb3814]

Probably paranna solution

[@stevevet3652]

I found the best way to evaporate alcohol is to take an aquarium air pump and place the air hose into glass container (I used a 1 Qt ball jar) and set the container on a coffee cup warmer. The coffee warmer is a small hot plate that is used to keep your cup of coffee warm. In less than two hours, 90% of the alcohol had evaporated. The remaining fluid is very oily. Be sure to partially cover the opening of the glass container with a lid but do not cover it entirely. You will need room for the alcohol to exit the container. Also, due to the bubbling, the alcohol will splatter out.

[@stevevet3652]

@Big Papi Oh...., okay.

[@thegoldenchild4657]

That's an expensive way of doing it and certainly not "the best"

[@Andrew-tk5yh]

What kind of cold trap are you using for this? Is it the small glass one? Or the metal canister one?

[@garydoherty7043]

My celite pattys keep cracking, any idea where i might be going wrong?

[@gdubya6039]

Do you use aper filter in funnel before the powder? If not How does the powder not go through the holes?

[@Jmarosii]

This specific funnel has a glass fritted filter disc welded in. The fritted glass is typically used for applications where standard filter paper would be destroyed by the solution to be filtered. The glass filter is 10-15µm. You can use an ashless filter paper or an unbleached coffee filter on top of the fritted disc, keeping fat and lipids or any other undesirables/debris out of the fritted glass disc to prolong its life. Feel free to give us a call at [phone] to speak with a tech.

[@patwilliamson5080]

OK guys I hope you all see where this gentlemen went wrong,He was expecting the liquid to be clear the first time,it never was ,so he cleaned everything out hoping the second time it would be clear ,it never did? One simple mistake, you half to use a filtration filter paper. you cant just throw the carbon down on the cellulite that come with the funnel because it will go thru.You can see he was expecting it to be clear.

[@vancouverguy2533]

Actually you dont have to use filter paper with fritted glass funnels. It does help with clean up of your funnel, but thats about it. Not sure what you talking about cellulite that comes with the funnel? Uh? The carbon shouldnt and isnt going through at all. Not if you are using the corrent funnel with the right micron size. The black going through the filter isnt the activated carbon, its whatever was in the solution in the first place.

[@92_SA]

Vancouver Guy I think he meant to separate the celite and activated carbon with filter paper and I would recommend to place the filter paper on the bottom, between the celite and activated carbon and to be really careful on top. Also be careful when pouring the ethanol mixture. Very careful! A cold ethanol mixture will work better (-40c). Good luck!

[@generalingwer4341]

Maybe its just me ,whats the solution?what are u filtering out of it?

[@SilverSin]

This is a underrated video.

[@Jmarosii]

If you have a video request, let us know! Thank you!

[@SilverSin]

How about a mixed solution extraction and filtration. Maybe a video on removal of chlorophyll!?!

[@Jmarosii]

A post-extraction dewax and chlorophyll removal? I'll pass along your request! You can do this during extracting using a dewax sleeve. The cold makes the hydrocarbon solvent less aggressive towards the fats, lipids, and chlorophyll, leaving them behind in the biomass. kzbin.info/www/bejne/aYXCiGyar8tgb9E Feel free to give us a call at [phone] to speak with a tech.

[@SilverSin]

@@Jmarosii I should've been a little more specific. I meant the remove of chlorophyll by UV and UVA spectrum lights.

[@Jmarosii]

@gene pattenson We have not done any research on the light spectrum and its effects on post-processed biomass.

[@gsquad599]

mix the carbon directly with the solution and stir and then filter

[@Jmarosii]

Towards the end of the video, you'll see he does precisely that. He adds the carbon to the solution and then places it on a hot plate to use its stirring setting. In this video, we wanted to demonstrate how to set layered media into a Buchner funnel properly.

[@jamieinlima]

@extractionkings517 Thanks you for your time and video showing these processes

[@Jmarosii]

Thank you for watching and supporting this channel!

[@mattymac2123]

Agreed..thanks for the efforts

[@Themadfranklin]

Thank you for the guidance.

[@alirzavt1917]

What micron is the glass filter?

[@masonrunning]

Do you have to use ethanol to make the celite patty? Can I use dcm?

[@Jmarosii]

@Mason best to use the solvent your solution is made up of. DCM can certainly be used to settle the celite patty.

[@chimmeychonga8987]

Could you give an Amazon link for a good buchner vacuum kit?

[@genghischuan4886]

how about fucking put that in your search on amazon, fuck people are lazy

[@breal1577]

@@genghischuan4886 ive seen you on a few of these filtration videos lately......you trying to get some clear shatter? Lol

[@genghischuan4886]

@@breal1577 clear shatter no but good filtering is always make a better tasting product for edibles. besides why make shatter when diamonds are easy and you get a separation of the THC into crystals. then you can break those down and make it even more pure. I make my own edibles, they have no taste and I know exactly the dose. But seriously why you here, trying to make your shatter clear? Must be cause you are here and that was your supposed insult to me so you did the obvious thing squeakers and entitled women do.... deflect

[@stannowak5086]

How do you get the rest of the carbon out of your extraction ?

[@Jmarosii]

@stannowak5086 using a buchner funnel along with 1 micron ashless filter paper. You'll continue filtering the solution until the carbon is removed.

[@potatoaimboy2387]

youre doing it wrong

[@cynicaldudeMe]

if anyone still watches this video. when you filter out the chlorophyll, approximately how much thc is also removed in the process?

[@genghischuan4886]

honestly this video is a fucking disaster

[@gsquad599]

None

[@uh2642]

how u applied the vacuum? what was the pressure?

[@vancouverguy2533]

doesnt really matter man. you could use a water aspirator, you could use a simple vacuump pump, you can use a nice lab vacuum pump. You just need a vacuum source, the pressue doesnt matter a whole lot since its not going to be all tha thigh in any of those cases

[@Sp-fe1eo]

thanks for the video

[@mr.statler1701]

I love your equipment. I had my own diy equipment Wich work just great but didn't look as cool.

[@trupyrodice4462]

Uh, that was 9 scoops there buddy, not 8. What you tryna pull? 😅🤣

[@christopheranderson8275]

I’m curious does the activated carbon absorb the oils in that solution? If so what is to be expected for a loss?

[@Jmarosii]

Yes it does, but its a very small amount.

[@dronesightingsmith3979]

Hey man as long as it gets the pesticides an poison out.

[@SoggyCashew]

Will this get rid of the strong chlorophyll taste?

[@Jmarosii]

@SoggyCashew using the right filter aid will remove chlorophyll. Removing the smell and taste of the plant. When extracting using ethanol, activated charcoal exhibits selective adsorption, meaning it can selectively target and adsorb specific compounds like chlorophyll while allowing other desired components of the plant extract to pass through. This helps in removing chlorophyll while preserving other valuable constituents.

[@thegoldenchild4657]

What if you wanted to use paper filters instead? What size would they be?

[@Jmarosii]

You can use an ashless filter paper or an unbleached coffee filter on top of the fritted disc, keeping fat and lipids or any other undesirables/debris out of the fritted glass disc to prolong its life. For dewaxing fat and lipids, use a 20µm filter (BIO-41). For holding filter media back, use a 5µm or below (BIO-42, BIO-44). Feel free to give us a call at [phone] to speak with a tech.

[@thegoldenchild4657]

@@Jmarosii I figured it out. Thanks

[@TravisBrown42]

Doesnt activated charcoal degrade indiscriminately?

[@normandobinkier363]

Looks like the circumference edge of.the filter is leaking.

[@nimo517]

Good work sorry for the late comment

[@ordinaryperson4862]

hi everybody, i want to extract caffeine. which size is the right one? Pls help me! G1 G2 G3 G4 G5

[@MrKarae]

Looks the same

[@sarahlarick3055]

Watch the celite 545 video this guy didnt doit right you need to let that powder patty dry after it settles and your supposed to doit it with water its to soupy to hold anything back yes it gets wet when you introduce you tincture to it but letting it dry an settle creates a solidly packed patty hes got a wet sloppy patty watch the celite 545 video it does work if you doit correctly and the guy in that vid does it correctly

[@anatol1204]

How many microns is the filter?

[@Jmarosii]

@anatol1204 the fritted disc filter inside this buchner funnel has a 20-25um design. It was intended to mimic a coffee filter. We have since changed our design and use a porcelain buchner funnel with ashless filter paper instead. The filter paper we sell comes in fast (20-25um), medium (11um), and slow (3um).

[@breal1577]

What filter are you dropping the celite onto?

[@Jmarosii]

This specific funnel has a glass fritted filter disc welded in. The glass filter is 10-15µm. This type of funnel is typically used for applications where standard filter paper would be destroyed by the solution to be filtered. You can use an ashless filter paper or an unbleached coffee filter on top of the fritted disc, keeping fat and lipids or any other undesirables/debris out of the fritted glass disc to prolong its life. Feel free to give us a call at [phone] to speak with a tech.

[@melnoyesespinoza4724]

Whats the measurement on your little yellow scoop?

[@Jmarosii]

Melanie Noyes 5cc. Or one teaspoon.

[@twistedsocal]

just an fyi, the way the funnel is pronounced is is ewe not uck not that many people seem to care but it makes people sound like they are clueless

[@jerrybear3081]

Buickner funnel

[@toscataurus9319]

No, actually it's Büüüüüchner. Try to form your mouth as if you want to whistle - that's the "ü". And the 'ch" sounds like a hissing cat. No "i" or "k" in its name. (I know: German is an ugly language! But what can I do? It's mine. 😏) www.howtopronounce.com/german/b%C3%BCchner en.wikipedia.org/wiki/B%C3%BCchner_funnel?wprov=sfla1

[@mad-b264]

Can you get the same result pressing with heat, I used to make my own RSO well isopropyl extracted cannabis oils, And just heat off the solvents, But then I got a cheap heat press, I would of bought a NugSmasher if I was rich enough, lol, It is expensive enough just making Cannabis Rosin, I think though with Alcohol extraction or solvents, you get all the (of) what you want than when you do heat press, It is just too dangerous for me not having the equiupment I need to stay safe, So I use a heat press, Plus it is a faster process, And cleaner with zero solvents at all, Still though if I had all the things I needed to get solventless extraction, The purger and not living in a block of flats, I am not putting other peoples safety at risk from fire, Let alone mine, So yeah using a Heat Press like a NugSmasher is probably the best way for most people to extract, Unless you in a setting that is safe....

[@chasew020]

do you still put a filter paper in or does this replace that all together?

[@WaffleStaffel]

No paper necessary with a sintered glass filter.

[@Jmarosii]

This replaces the filter paper all together

[@石头-d4f]

Putting a filter paper will save time on cleaning. Also is important to put every layer evenly and flat. And if you want, you can also add another filter paper on top to not disturb the kieselguhr and the charcoal.

[@sarahlarick3055]

No no it doesnt sorry bvv you do want that filter paper the correct way to do this is to put a filter paper in then your powder then WATER vac the water out to form a patty let that patty DRY do not put you tincture thru that soupy mess you guys.... It didnt even hold the color back that hole patty is yellow and if it alll the way thru the patty its making it back into the receiving flask... This is redundant idk if you telling them wrong on purpose bc im sure you poeple are smart enough to know that powder patty has to settle and drso it can actually hold back sediments caratons chlorophyll ect... Watch the celite 545 video that guy does it correctly amd theres a night and day change not a slight change

[@mattymac2123]

@@sarahlarick3055 nice post

[@olajohns2529]

He should have used more carbon in the funnel and added the carbon to the solution in the first place . it works better if u let it drip and tack your time .

[@foreveryoung8807]

BVV Color Bleach T41 What does this do?

[@okccitizen4400]

Thanks for all the vids keep them coming please! Will sub and get views!

[@sarahlarick3055]

I will be post starting a series in about a month start to finish wash purge then vac purge how to keep different textures then onto advanced polishing for high potency vape carts not those liquifiers that you add tw*ce as much too i have a 7% mix recipe rather than 66% recipe keep an eye out for me

[@flickmybic911]

@@sarahlarick3055 were your videos still dont see any

[@ryancameron1979]

How many micron filter?

[@Jmarosii]

The fritted disc on this unit is 20-25 micron.

[@E_Rico]

How to make a fresh cup of coffee

[@Jmarosii]

Pour over coffee

[@lenasnell1734]

Can this work for doing whey protien and filter it into isolate?

[@moosehead4497]

what a mess, so many things wrong, put the charcoal in the solvent and stir, never pour your mixture directly onto the puck, you ruined it, so much wrong

[@Paul-q3m7k]

What’s it like having no life ?

[@bastovanicjuric1924]

Hes just 100% right and why your acting aggresive on a konstruktiv Comment? All good in my eyes here

[@glenraymond379]

It looks like you have a lot of water in there..

[@Jmarosii]

Are you referring to the resin suspended in the pure ethanol or the filter media? During this demonstration, the media used was not baked a second time. We did this to show how effective the media is right out of the bag. It is, and we do recommend you to bake your media before use. Removing ALL the moisture WILL make the media more effective, allowing for less media to be used. Feel free to give us a call at [phone] to speak with a tech.

[@glenraymond379]

@@Jmarosii I mean the white cloud that formed in the collection flask. You get the same cloud rinsing equipment with water. Also this method of filtration should give you yellow or almost clear solution but what you have is brown that's why I think you have water in your methanol. You should really make a new video about these medias because they work really good for me. Just by curiosity what do you mean by baking the media? Why do we need to bake these media?

[@tommagnum2819]

sloppy and incorrect

[@djefferson5669]

Your mother doesn't work here. Who cleans up after you??

[@Jmarosii]

She actually does!

[@balkan-baraba]

ahahahahahahahahhaahahhahaahahahah same color after 1 h extraction🤣🤣🤣🤣🤣🤣🤣 i think the vakuum pump is to strong

[@paulmcnally7631]

99% alchol

[@Jmarosii]

@paulmcnally7631 we have 710 denatured alcohol, certified 200 proof alcohol, and isopropanols. Check out our website shopbvv.com

[@iPsychlops]

Weirdest coffee making video ever.

[@Jmarosii]

Pour over drip coffee is the best coffee ever. ☕️

[@wuddayaat]

Your bad at this. Just sayin.

[@Jmarosii]

@wuddayaat thanks for watching. This is a simple demo video on how to use a buchner funnel with filter media.