Nitration of glicerine

[@ghostmedic86]

The classical music is a nice touch!

[@jlo13800]

now take it and throw it against a watt as hard as you can and boom.

[@TechmakeHack]

It's by Morzat

[@將軍-c9x]

因為這是諾貝爾先生那個時代所製造出的產品.背景音樂.很搭！

[@電棍說的道理]

@@將軍-c9x小知識：硝化甘油並不是諾貝爾製造出來的

[@marti2568]

Cartoons showed that nitroglicerine is far more sensitive!

[@DangerClose13E]

70% nitric acid actually works better than 93%. The extra water helps remove the hydrogen atoms from the glycerine so the nitrate groups can attach. Its also cheaper.

[@lucianoperitore6647]

I've a question, the NO2+ groups are formed thanks to the disidratation action of the sulfuric acid or thanks to the acidity of the sulfuric acid?

[@DangerClose13E]

@@lucianoperitore6647 I never heard of "disidratation". You should study the nitration processes better before attempting these procedures.

[@lucianoperitore6647]

​@@DangerClose13E you misunderstood, the sense of my question. Follow my reasoning: if you have the nitration mechanism in mind, you should know that sulfuric acid transforms nitric acid into NO2 + groups. my question is, which characteristic of sulfuric acid allows the formation of NO2 + groups? its hygroscopicity? its acidity? both?

[@NoOne-sn2si]

So many wannabe chemists... So little time... Lol!

[@pozdernoah3074]

@@lucianoperitore6647 The acidity is the main factor as it stabilizes transition states - which in return helps with the substitution of hydrogen atoms from nitro groups introduced into the glycerin, that's why sulfuric acid is a common catalyst (although you need to filter it out with alkalines afterwards

[@themanwhospeaks8010]

The classical music and your carefulness made this really funny for some reason

[@ksp6091]

When you are using conc. nitric acid, remove your gloves ! If the acid tuch it, it will instantlly burn

[@OKULT26]

True if gloves was from latex or so.. but this are heavy duty special chem resistan so no wories

[@joeestes8114]

You shouldn't be using fuming nitric acid, just 68% nitric acid!

[@ksp6091]

@@OKULT26 oh ok

[@joeestes8114]

@Gustavo S. 68% is all you need. Anyone who makes this antique explosive is asking to blow there hands off

[@alexpearson8481]

Ironically most of these reactions are fairly safe because people are so careful. Probably more injuries from playing with the nitroglycerin afterwards

[@OKULT26]

@SouthernRockCulture Like i show in video add everything including spent acids to the cold water. Aprox. ratio 1part reaction mix to 5 parts water.

[@blackbullssdin8907]

mixing with thermometer ??? what an idea .....

[@DPWrepublic]

classical trick, often during my chemistry class

[@MrBradshawbenjamin]

@@DPWrepublic Classic trick to also accidentally spill thermometer juice into your reaction mixture one day, not that that's happened to me and I have done that trick before. Other than that, works perfectly fine.

[@joeestes8114]

@@MrBradshawbenjamin nobody cares

[@MrBradshawbenjamin]

@@joeestes8114 Not many people at least apparently.

[@johnty6067]

@@MrBradshawbenjamin so what your saying is too clean thermometer before and how?

[@p.c.principal7324]

Did you put a plastic cap on the nitric acid and put that into a plastic bag?

[@zwiebacktoast8349]

Is it possible to make it from pottassium nitrate, conc. Sulfuric acid and glycerin ?

[@one_for_one]

so glad im not the only one anxious as fuck watching this

[@sciguy3128]

Would 70% nitric acid work? Perhaps if I used an excess of sulfuric acid to absorb the water?

[@Angrychemist666-g4x]

Could it just be my super hearing, or did anyone else hear a rodent riot at the end ? Im guessing this was done in India! 😅

[@tjjackson3104]

I love the choice of music lol👌

[@huckstirred7112]

why destroy your nitrating mixture ? why not just make more nitro ?

[@MrBradshawbenjamin]

Even though the product did separate out, at least somewhat, I assume it's too soluble in nitric acid so the concentration of acid was lowered by adding the water, precipitating out more product, and maybe allowing the oiled-out product to crystallize as well?

[@WizardChip]

you might want to invest $1 on a string rod.

[@kalanawaduge1014]

What is the rate chemicals are applied?

[@fiftyy1064]

1:1 i think

[@foxthemememan9747]

Where do I buy the ingredients?

[@TheMassivemarshmallo]

The funny thing is you can be any age and buy all these ingredients online

[@daslickpotato4514]

Make nitric acid with sulfuric acid and potassium nitrate, and you buy sulfuric acid as drain cleaners at lowes or home depot

[@daslickpotato4514]

@the man who changes the trash true

[@thorstenelvers7618]

and glycerine can be made from vegetable oils.

[@alke5668]

@h 90 percent of the time it is usually around 95% but due to the other ingredients it is not that reactive so just add h2o2 and boil it off

[@syahrulzahwan]

Damn u dare hit that thermometer to the flask so many times knowing the probabilities of it being set off by accident

[@OKULT26]

NG is not primary and much predictable if you know that you are dealing with and have real experience with it ,and not from tv or movies . But yes to many hits probability is posible.

[@PhilieBlunt666]

ya got guts man ,making that much at a time...

[@Wheresmy240]

7:38 that's not a lot of NG.

[@Aranak777]

its secure under liquid

[@jasonhaddeman4035]

Ok now that you have the easy part done did you make any videos on how to finish it.?nice gloves by the way I think l would take my chances with the acid before ld melt those gloves on my hand. Kinda like welding right?lol

[@michelgrenier1878]

Why the sulfuric acid ?

[@NoOne-sn2si]

To make sulfurglycerin... Way better than nitro!!

[@edwardarruda7215]

Nitric acid in a wine bottle. Hahaha

[@williamsshane21]

Cool video

[@h.Freeman]

If anyone was wondering he got 10 years in federal prison for doing this ...that's why it took him a decade to post the next vid😣

[@Zenzicubic]

Making nitroglycerin is a terrible idea and a great way to be sent to the ER.

[@Zenzicubic]

At least get a cheap stir plate and stir bar.

[@willowpine2604]

​@@Zenzicubic ER is for woudned people trying to save them not for dead one's 🤣

[@annefrank3225]

Fbi open up

[@JeffyNguyen]

So unstable... I wouldnt mess with this stuff

[@Wheresmy240]

As long as you keep the temps really low during production and only make small amounts the risk is pretty low (if you're trained or a very mindful person, we all know that one person who can break an anvil so to speak). Also, don't keep it and let it age for any extended amount of time. It degrades and as time passes, it gets more and more unstable.

[@jackhartzell6074]

Pussy

[@mahmodfarahany-qh4yf]

چرا توضیح نمیده

[@ghostraider7520]

nitroglycerin is a not professional explosive petn and RDX are very better

[@realname3538]

Tatp

[@alkahest--1135]

Nitroglycerine was the most widespread and useful explosive for a very long time, just because there are more powerful explosives doesn’t mean nitroglycerin isn’t still in use

[@OKULT26]

It will absorb water from reaction.

[@chemlab5038]

OKULT26 Can’t I mix 98% H2SO4 with KMNO4 and nitrate it that way

[@OKULT26]

no

[@NoOne-sn2si]

KMNO4 - nitrate?!? Go back to school, dweeb!!! FYI, It's KMnO4....

[@自由の翼-c9o]

dr stone bring me there

[@Laurenavan]

Clearly the person making this NG is afraid. You don't need to add one drop at a time. It won't explode if it's on ice.

[@OKULT26]

Drop wise adition is for temperature control to nitrate and not oxidate glicerin in reaction to not have runaway. It's nothing to do with fear or ng exploding in reaction☺

[@fiftyy1064]

If it goes up to 50°C then boom, and trust me it dosn't take much for that to hapen

[@DrewishAF]

Aaaaaaaaand KABOOM!

[@lukewarmwater6412]

this is great for if you have to move a stump. or maybe a rock. theses volumes dont seem like it would make more than one or two sticks of dynamite. I am not at all an expert, so I am thinking that this would be of the most use to homesteaders, not terrorists. but then again....

[@jakedaprile5798]

Terrorists don't use nitroglycerin any way cause it takes too long to make significant amounts of nitroglycerin, flash powder an amoniumnitratw fertilizer works better for them, however u still need a license

[@fudes587]

You dont need a license for flash powder or ammonium nitrate Lol Btw pure ammonium nitrate doesnt explode you need to make anfo or sum similiar

[@lukewarmwater6412]

@@fudes587 both of you who commented on my original comment are fucking idiots!! ... you figure it out.

[@johnty6067]

@@fudes587 what is anfo

[@fudes587]

@@johnty6067 lol u serious

[@Greenmachine305]

Im horrified to watch this.

[@OKULT26]

you are doing it beter....so dont watch

[@radiotriggered2096]

This *could* have been a useful video...

[@northcoastaudiovisualncavc9706]

What's happened to you okult

[@OKULT26]

Nothing every thing ok.

[@mehranfreeman6192]

ACME

[@whiteangel3594]

I don't know why this stuff is on internet. No offense but there are really whack people out there. We live in the era of information but some information would be better not be public.

[@amicuscuriae2002]

There are many cracy people who want to be in heaven-..., Hoffentlich sieht unser Verfassungs- und NGOschutz das und sperrt diese Videos!

[@ilia7276]

احمق

[@chemistryofquestionablequa6252]

That's possibly the biggest cuck bootlicker comment i've ever seen.