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Find the Concentration of Hydrogen Peroxide by Titration with Potassium Permanganate

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NurdRage

NurdRage

Күн бұрын

In this video we find the concentration of hydrogen peroxide by titration using domestically available chemicals and equipment.
Hydrogen peroxide is titrated using potassium permanganate solution that was standardized with sodium oxalate. The titration is performed in a solution of sodium bisulfate to provide the acidic protons needed to run the reaction. Sodium oxalate is titrated with the potassium permanganate at 70 Celsius until a lingering pink or brown color is observed. The amount titrated is used to determine the actual concentration of the potassium permanganate.
Once the concentration is known, hydrogen peroxide is titrated with potassium permanganate until a lingering pink color is observed. Using the known concentration of permanganate the concentration of the hydrogen peroxide can be determined.
Related videos:
Making Sodium Oxalate: • Make Sodium Oxalate - ...
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Пікірлер: 242
@NurdRage
@NurdRage Жыл бұрын
Now you know why i made sodium oxalate.
@SHIEET817
@SHIEET817 Жыл бұрын
Years ago
@NurdRage
@NurdRage Жыл бұрын
@@SHIEET817 no i posted it last week.
@borttorbbq2556
@borttorbbq2556 Жыл бұрын
​@@NurdRage it's nice to see you back.
@borttorbbq2556
@borttorbbq2556 Жыл бұрын
​@CHICAGO TEEN you might be thinking of Nile red.
@highlander723
@highlander723 Жыл бұрын
analytical chemistry is the equivalent of flipping burgers you say..... I feel insulted.
@Alloran
@Alloran Жыл бұрын
I used to teach this error propagation to students in my IB physics and this is a fantastic example of how the error grows at each step and with each calculation. I think I'm gonna use this video as homework this semester. I want them to tell me why my measuring devices dictates my method and why using the minimum possible number of measurements or calculations to reach my end point is preferential to a possibly more accurate method that requires more steps or calculations with the measurements.
@mitchellr6819
@mitchellr6819 Жыл бұрын
I’m in a general physics series right now, my professor really pushes propogation of error and significant figures. I’m so excited to see it here!
@pierreproudhon9008
@pierreproudhon9008 Жыл бұрын
@@mitchellr6819I finished general physics a earlier this year and all the professors I've had didn't seem to care that much about it. Did some error propagating calcs in the accompanying labs but that's pretty much it.
@ianmcewan8851
@ianmcewan8851 Жыл бұрын
[As an applied mathematician with a specialty in measurement and error analysis] no evisceration necessary!! Nicely done in a half hour vid.Really no quibbles at this level.
@methyleneblue_
@methyleneblue_ Жыл бұрын
i've been watching your videos for more than a decade iirc now 😭 thank you for doing what you do!
@Saumiiiii
@Saumiiiii Жыл бұрын
same here hahaha
@ravencrovax
@ravencrovax Жыл бұрын
"Trust nothing and verify as much as you can." Sounds like how I live my life.
@GodlikeIridium
@GodlikeIridium Жыл бұрын
And you're right doing so.
@BillAnt
@BillAnt 11 ай бұрын
Especially the wifey/girlfriend. ;D
@SharpMagnets
@SharpMagnets Жыл бұрын
I remember being 10 and being OBSESSED with these nurdrage videos. Now I’m 22 and I re-found you. I’ve never been happier.
@Swannilization
@Swannilization Жыл бұрын
YES! I had to do this in a lab practical back in the day. Thanks for showing the workhorse stuff!
@kohizeri_daisuki
@kohizeri_daisuki Жыл бұрын
Thank you for the video! Now I know why I am dead set on pursuing chemistry when I start college in a few months. My head aches a bit with the intricacy of the processes and techniques, but the utter beauty and satisfaction I get when I can say for sure that this substance has this concentration and it is all thanks to my work takes all that ache away. Thank you for inspiring me along with other science youtubers to pursue this field ❤
@idontknowyet2875
@idontknowyet2875 Жыл бұрын
Man, I wish this video was out 2 months ago You explain the general process really well
@binaryblade2
@binaryblade2 Жыл бұрын
Oh shit, new nurdrage video just dropped.
@booboyBL
@booboyBL Жыл бұрын
Many years ago, I was a lab tech. for a major manufacturing chemical company. I worked in various lab departments, including 3 years in analytical services carrying out titrations and various other analysis techniques, (chromatography, photometry, spectroscopy and others). I sort of miss those days
@thomasrogers8239
@thomasrogers8239 Жыл бұрын
We used peroxide solutions in mold mitigation back in the day, you might look into IAQ 2000 or it's daughter product IAQ 6000 for a more concentrated peroxide starting solution. I'm remembering it being labeled as being either 15 percent or 30 percent peroxide and we absolutely diluted it before spraying stuff down because it had a nasty habit of burning our skin if we accidently got spray on us.
@stamasd8500
@stamasd8500 Жыл бұрын
Baquacil oxidant you can get at pool supply stores is nominally 27% H2O2. It's fairly inexpensive, $15-20 per gallon.
@MCPicoli
@MCPicoli Жыл бұрын
I can get it at 50% concentration as a pool cleaning agent here. Very cheap too. YMMV, I am in Brazil.
@Thecompanioncrate
@Thecompanioncrate Жыл бұрын
Return of the Mack. In all seriousness I appreciate these more recent videos I needed to review this stuff.
@Mpdarkguy
@Mpdarkguy Жыл бұрын
Hi I just wanted to tell you that I grew up with your videos and recently I've been tasked to narrate a specific and technical presentation. I took a lot of inspiration from your style and I've received great feedback so far! I am not in a chemistry related industry by any means, but I can somewhat easily follow what you're doing with just high school level knowledge, and I think that says a lot about the way you present your videos. Thanks a lot for giving me a boost in more than one way!
@bradleyhowes848
@bradleyhowes848 Жыл бұрын
So awesome to see! I’m a glass artist and I batch my own colors that are very sensitive to the redox of the base glass as well as the furnace atmosphere. I definitely think some of these principles and techniques can help get a more relatable color!
@KrashFries
@KrashFries 10 ай бұрын
you can actually add traces of manganese (MnO2 is cheap and convenient) to the glass and have it oxidize to a light pink or indigo!
@bradleyhowes848
@bradleyhowes848 10 ай бұрын
@@KrashFries indeed, however this depends on the redox of the glass, pushing the Mn ion to the +2 or +3, colored or colorless, and also dependent on the fluxes in the glass, sodium will tend towards brown and potassium towards purple. Further, trace amounts as a decolorizer can solarize from clear to colored over a period of years. The techniques the NurdRage uses though will help to reduce error in more complicated glasses involving the controlled growth of silver nano particles in the glass.
@ejkozan
@ejkozan Жыл бұрын
Wonderful video! And all this discussion of errors! I just love it!
@nathanhays1746
@nathanhays1746 Жыл бұрын
I did this same process including making the standard to titrate permanganate. I was surprised that my 30yo jug of h2o2 was actually _more_ concentrated. Hadn't realized that h2o evaporates faster than the peroxide degrades.
@NurdRage
@NurdRage Жыл бұрын
Wow that's pretty cool. I wonder if mine started at 5.0% and drifted upward from evaporation. Maybe I'll test it again next year to see.
@nathanhays1746
@nathanhays1746 Жыл бұрын
@@NurdRage In the h2o2 powered hobby rocket community a common way to get high test peroxide is to put a fan on an open container and leave it overnight before the launch. Loses peroxide of course, but starter 35% concentration is pretty cheap. Distilling is dangerous because you must heat it past 100C to drive off the water. Vacuum distillation is problematic out on the range and transporting high test peroxide is no bueno. Luckily, leaving the inhibitors in doesn't interfere with the permanganate-infused platinum gauze catalyst that the h2o2 passes through as it is pumped into the chamber. "Motivational" chemistry! Absolutely love your work!
@theSILKROAD210
@theSILKROAD210 Жыл бұрын
Thank you for your great work! Right now I am doing my Bachelor thesis in medicinal / synthetic chemistry, and I am watching your great videos since my apprenticeships as a Chem. Laboratory assistant. imagine I had access to this kind of educational content back then, that would have been great. future generations will be so lucky to have access to this kind content. please continue this great work, it is a big contribution towards free and accessible Science education.
@austinrosh6491
@austinrosh6491 Жыл бұрын
So happy to see you posting again keep up the good work your the reason for my chemistry career
@erikziak1249
@erikziak1249 Жыл бұрын
Not even half a minute in and I am literally "LOL" ing. This is the content I subscribed for. 🙂
@clintongryke6887
@clintongryke6887 Жыл бұрын
Really good; thorough and clear. Takes me back to A-level (U.K.).....
@Bludgeoned2DEATH2
@Bludgeoned2DEATH2 Жыл бұрын
Interesting! I work as a chemist in a manufacturing lab in one of the products we make is an H2O2 containing hair spray for the summer and to analyze it we use this potassium permanganate titration and you’re right we use sulfuric acid to acidfy the solution prior to titration!
@Carlos_GS
@Carlos_GS Жыл бұрын
Very interesting, thanks for sharing this process in such detail :D
@mitchellr6819
@mitchellr6819 Жыл бұрын
I gotta be honest, I got sooo excited when you brought up propogation of error.
@edgeeffect
@edgeeffect Жыл бұрын
I have huge "nostalgia" for Pot. Permang. - partially because your "making Pot. Permang. from batteries" video was the beginning of my KZbin science adventure. You've done wonders to improve my amateur-grade titration too - it's time to put my burette away and "go gravometric" from now on. All in all, another excellent video.
@Josue31627
@Josue31627 Жыл бұрын
"Trust as little as possible and verify as much as possible" is good life advice too. Great video as usual. I was reminded of Periodic Video's "Accidental Reaction" video near the beginning. I actually found titration fun back when I took college chemistry. But often I made too many errors in my error calculations... oopsie.
@koukouzee2923
@koukouzee2923 Жыл бұрын
I own a vial of 102% pure sodium hydroxide The purity source was the retailers "trust me bro "
@nickbonsavage2586
@nickbonsavage2586 Жыл бұрын
Great to see you're still active. Thought you retired from youtube there for a bit. This is great stuff. Thank you. About ten years ago i started getting into chemistry as a hobby, this last year I began at a university and im going for a chemistry degree. I'm 34 and figure as long as I finish before I'm 40 I'm ok haha. Anyway, your videos were what I watched all throughout the years that helped build my interest and it's just great that you're still at it. You played a large part in building my fascination and interest of chemistry. I'm sure I'm not the only one that you helped inspire.
@GQuack
@GQuack Жыл бұрын
Glad you're back, Lithium. Loved your content since the old days(2013).
@javersongoulartfilho9439
@javersongoulartfilho9439 7 ай бұрын
Now this is an amazing lecture. You got me impressed and subscribed! Regards from Brazil!
@Gauss247
@Gauss247 Жыл бұрын
This is absolutely fascinating. The level of detail and understanding you have are mind blowing! Also very didactic delivery. I love all your videos. Thanks for all of them! I hope you can keep them coming.
@vitamin9165
@vitamin9165 Жыл бұрын
Nice vid. I think this is super important stuff for the amateur chemist to know when you don't have good sources for things and the precision kinda elevates things from just fucking around in a basement to a real science in my opinion.
@bedlaskybedla6361
@bedlaskybedla6361 Жыл бұрын
Very nice video NurdRage! You well explained basics of volumetric analysis. I like that measuring of titrant with scales, it present alternative approach for someone who doesn't have a burette. If you want, I can share some experience with bromatometry, this method isn't often mentioned and it can be very useful (especially for organic chemists). I tried determination of phenols, anilines, O-alkyl phenols, hydrazines, unsaturated carboxylic acids, ascorbic acid, Sn2+ and Sb3+ salts. I also did few not well known, but interesting titrations, like Mn2+ using KMnO4, NO3- using FeSO4 or amines using HClO4. I also plan UV catalysed oxalate determination using Na3VO4.
@davidjones6661
@davidjones6661 Жыл бұрын
"Not even I have one".... "and I've got a ****ing rotovap!"
@sulaimanabdullah952
@sulaimanabdullah952 Жыл бұрын
Great video, clear, concise, informative. Thank you
@TechsavvyScientist
@TechsavvyScientist Жыл бұрын
Technically molality refers to moles of solute divided by kg of solvent (not solution) the error is not big though since it’s a dilute solution.
@GodlikeIridium
@GodlikeIridium Жыл бұрын
Do you have a source for that? I'm pretty sure molarity is defined as moles of solutes by volume of solution, SI in mol/m3 but usually in mol/L. And not all titrants and other solutions are as much diluted. For example a 1 M solution of silver nitrate is 170 g of AgNO3 in 1000 mL of solution, or in the definition you mentioned 830 g of water. That's a huge difference. Edit: And a definition in mass by mass would make it almost impossible to handle and use for titration and the dividor being solvent instead solution would make it unnecessarily complicated. I do like the way he titrated in the video though. Never seen that :D
@tbird81
@tbird81 Жыл бұрын
Molality vs molarity?
@gunstercz
@gunstercz 14 күн бұрын
I read in an article, which I unfortunately can't find anymore, that this unit of moles of substance in a kg of solution is called molamity. Some guy coined the term when researching gravimetric titrations and it has been lost in history.
@trevmac2248
@trevmac2248 Жыл бұрын
Excellent detail & presentation! Thank-you for sharing!
@apricotcharms4126
@apricotcharms4126 Жыл бұрын
Holy shit bucket the granddaddy of KZbin chemistry is still posting. I used to watch you all the time as a kid back in 09
@JoshuaNicoll
@JoshuaNicoll Жыл бұрын
I was only thinking to myself I needed to titrate my H2O2 I had concentrated a bit, your methods and justifications are always a delight to watch.
@kid_missive
@kid_missive Жыл бұрын
Thanks for the video! I do a lot of these exact titrations at my job so it was neat to see someone with your reputation discuss them. We have, in the past, used NaOH to titrate oxalic acid, then keep that around to check KMnO4 solutions. I have lately been checking NaOH against dry KHP, but it never occurred to me to use oxalate as a single primary standard for both acid/base reagents and oxidation/reduction reagents... Oxalate also has some useful chelating properties I seem to remember. That would be super if it could be standard for complexometry too.
@NurdRage
@NurdRage Жыл бұрын
Oxalic acid needs to be checked because it absorbs water, and it decomposes if you try to dry it. But sodium oxalate is great because it's stable enough to be dried. Might be worth looking into buying a certified standard version of it. At the very least it saves you two steps from KHP and NaOH.
@GodlikeIridium
@GodlikeIridium Жыл бұрын
It always depends on the exact use case. A primary reference substance for titration has to be easy to purify, stable and easy to dry (again and again). Besides that, similar to the analyte you'll be titrating after the determination of the exact molarity or a factor. So for acid-base titrations we use KHP if intended for the titration of anorganic salts. For acid-base titrations of halogen salts of organic amines we use benzoic acid (a beautiful example to teach recrystallization btw). Because of the different pH at equality. For redox reactions oxalic acid. For complexometric titrations calcium carbonate. TRIS or trizma base gets readily used too and I've even seen a very niche procedure using sulfamic acid, this one doesn't really make sense though.
@kid_missive
@kid_missive Жыл бұрын
@@NurdRage I am going to be implementing this as soon as I have time. Thanks for your insight!
@thestimpy2101
@thestimpy2101 Жыл бұрын
Me and my kids have missed your content.
@stamasd8500
@stamasd8500 Жыл бұрын
Very useful, thank you. Keep'em coming!
@picosoft2033
@picosoft2033 Жыл бұрын
oh yesss! after a long time one of my popular and inspiring chemists uploaded a new video! 😇😇😇
@Toaster0Bath
@Toaster0Bath Жыл бұрын
Hey we have the same digital scale! I watched you all the time when I was in my early teens. I always had a natural interest in chemistry, but you amplified that sir. Glad to see you are still involved in chemistry and uploading videos. I have a lot of catching up to do!
@2486jdc
@2486jdc Жыл бұрын
this is, and has for a long time been, my absolute favorite youtube channel. i would love to have even half the understanding of this shit. i got into chemistry for the wrong reasons but your videos definitely helped transform it into a healthy interest. you sir, deserve a statue.
@NurdRage
@NurdRage Жыл бұрын
thanks man. Whenever i'm feeling down, or wonder if i'm doing okay, i read comments like yours and i'm motivated again to keep going.
@2486jdc
@2486jdc Жыл бұрын
no problem man. stay genius!
@erikziak1249
@erikziak1249 Жыл бұрын
OK, even though I LOLed at least two times in the first minute of this video, the last 5 minutes were very serious and valuable to anyone doing this.
@stevensexton5801
@stevensexton5801 Жыл бұрын
"I just want you to be aware that it exists", as an engineer I love that statement.
@CHIROTHECA
@CHIROTHECA Жыл бұрын
He is back! FInally!
@KF-16-65
@KF-16-65 Жыл бұрын
Thanks for the video! Great refresher on some of the stuff I learned in an analytical chemistry class not too long ago.
@randomergy683
@randomergy683 Жыл бұрын
Yesssss! Perfect timing for this video! I've had some concentrated peroxide for awhile that I'm not sure what the concentration is and was wondering how I could go about determining the concentration.
@handpaper6871
@handpaper6871 Жыл бұрын
If you know that it contains only peroxide and water, just measuring its density will get you within ~1%.
@Marbslab
@Marbslab Жыл бұрын
Very useful.
@imikla
@imikla Жыл бұрын
This is super exciting! Thank you!
@Neofizz
@Neofizz Жыл бұрын
After watching for years, I really like your viewpoint and ingenuity. I'm curious if the PPM of a colloidal silver solution can be discovered by titration.
@Nagria2112
@Nagria2112 Жыл бұрын
nice! thats my work :D im an ANALytical chemist in pharma and we titrate alot.
@piranha031091
@piranha031091 Жыл бұрын
If you're doing gravimetric titration, you may want to use polyethylene or PTFE beakers instead of glass ones. They're much lighter, which minimizes the relative error from your scale. Also avoids overloading the scale in some cases.
@aSCrouton
@aSCrouton Жыл бұрын
Going to run through this myself, such a good crash course. Would love to see videos of testing for different functional groups, basically a way to test and identify different pure substances
@johnmyers379
@johnmyers379 10 ай бұрын
Your the only person that I can't wait until u get mad I know it's coming it makes my day lol
@jwrm22
@jwrm22 Жыл бұрын
After watching dozens of these videos, I still don't know much about chemistry. These steps are very similar to other sciences, where I'm most adept in Electronics Engineering. Nothing beats measuring the actual parameters of a component, instead of just following the datasheet.
@rafaelgcpp
@rafaelgcpp Жыл бұрын
Sir, you made me freeze to my soul, remembering my days at university physics lab, measuring stuff to learn how to deal with precision... This is the seed of nightmares!
@thebackyardspaceprogram
@thebackyardspaceprogram Жыл бұрын
He's back!
@KMyGProductions
@KMyGProductions Жыл бұрын
This video gave me flashbacks of my junior Quantitative Analysis course in college and now I’m glad I didn’t get a job as an analytical chemist
@charlesurrea1451
@charlesurrea1451 Жыл бұрын
Yep! Sounds like work.
@ScottieTheCat
@ScottieTheCat Жыл бұрын
The lab I work in uses something called the Monte Carlo simulation in order to estimate measurement uncertainty. For those who are unfamiliar, the best way I can explain this is that after taking multiple measurements of something, a computer program mathematically simulates a number of possible iterations of this measurement (say a hundred, or a thousand iterations), and we derive our measurement uncertainty estimation from there. I'd like to know what your thoughts are on this. Great video as always! :)
@AcoAegis
@AcoAegis Жыл бұрын
That's really cool, I never knew how that all worked (or why molality existed). Thank you for sharing
@frollard
@frollard Жыл бұрын
Thank you as always for sharing!
@AL6S00740
@AL6S00740 Жыл бұрын
wooohooo
@peejay1981
@peejay1981 Жыл бұрын
As an Electrical Engineer who knows nothing about chemistry this video feels just like home compared to your normal stuff! Measure and quantify everything multiple times, then crunch some numbers and figure out the errors.
@OtherWorldExplorers
@OtherWorldExplorers Жыл бұрын
Every time I watch one of these videos I feel like I'm attending villain school. Can't wait for the freaking lasers!? 😂
@-KiTToBuG
@-KiTToBuG Жыл бұрын
Quantitative analysis suuuuuuuuuks.
@djdrack4681
@djdrack4681 Жыл бұрын
I've worked in an industrial food MFG that made whey protein powder. (My job was micro testing both pre-products, finished products, and environmental [air, water lines, drains, floors and puddles on the floor, etc]) During the process, they boil off the excess water, (don't quite me) but I believe react it with H2O2, acetone, honestly I forget. But we also have lines EVERYWHERE in the plant (basically big a## hoses) to wash equipment, the concrete floor etc to try and keep the bacteria levels low. One line was plain tap water, the other was some cleaner I think was something akin to star-sans, a semi-foaming quick rinse cleaner) ANYWAYS: one of the tests we did was testing the water coming into the plant and at some of the water tanks we had (which would be used to flush some systems). It was basically titration work just like this to detect H2O2 levels, because there could be cross-contamination at times with this from one of the systems (somehow, because the plant was old as hell, and many things quite 'questionable'). Since they dind't want ppl to use sulphuric acide, we were in fact using sodium Oxalate and potassium permanganate as well. So, when I say it was very similar to this, it was VERY. I think we also used hcl if I remember correctly, but as its been years since I worked there I forget why.
@NurdRage
@NurdRage Жыл бұрын
Interesting! I think you can use HCl if you're not too concerned with accuracy since HCl chews up some permanganate before it reacts. Maybe your lab determined the error was acceptable for your application.
@djdrack4681
@djdrack4681 Жыл бұрын
@@NurdRage Lets just say the QA side had a lot of 'wide' margins for acceptable results. More than some of us may say were 'OK' lol
@gigglysamentz2021
@gigglysamentz2021 Жыл бұрын
I'd love to check B12 content in vitamin supplements!
@JanJeronimus
@JanJeronimus Жыл бұрын
When you where drying the primary perhaps also weigh during the dry process to check if it dryed completely. (Perhaps you did this, however i did not see it in the videos.) This is easy to do and also adds some reliability.
@BrendaEM
@BrendaEM Жыл бұрын
Nudge, nudge. We need an epoxy-like system that can be recycled. Bonus for it being not an endocrine disrupter. So, we need two chemicals that when mixed together harden, and resists water--yet can be readily dissolved with a 3rd chemical, which is not normally around. Hmm. I wonder if you could make an Arduino device that has an phototransistor and an LED separated by a short distance. The opacity of your solution during titration could be read numerically--instead of eyeing it. An old insulin pump or parstaltic pump could be used to dropwise additon--until the titration point is reached. Interesting videos, as always. Thank you.
@fishyerik
@fishyerik 7 ай бұрын
Great video! Not the quick and easy way to get a ballpark figure of the H2O2 concentration I was hoping for, but great video. My mind started to figuring out ways to automate the more tedious parts just while watching the video. And I suspect the video was just a small fraction of all the time it took to do for very experienced person, as the most of the most tedious parts were sped up or cut out, and the video also had great narration. I was thinking, couldn't a peristaltic pump and a camera and some software be used to automate the titration? In this particular example a light source, photoresistor and an arduino should enough to control the pump.
@NurdRage
@NurdRage 7 ай бұрын
actually, if you want a fully automated titration and you are allowed to use electronics, then looking the topic of "coulometric titration". You basically stick electrodes into the solution and measure the peroxide content by electrolyzing it. a great deal more complicated, but once you set it up, you just add in a precisely known quantity and press a button to get the results.
@fishyerik
@fishyerik 7 ай бұрын
@@NurdRage Thank you! I later realized I can just add a catalyst and measure the amount of oxygen gas.
@NvTwist
@NvTwist 8 ай бұрын
Perfect video to point anyone to when they say “woah why is lab grade cost a lot more?”
@DaNiKzz
@DaNiKzz Жыл бұрын
26:00 "Mass of Karen ego" lmaoo true
@Neptunium
@Neptunium Жыл бұрын
I wouldn't trust that cheap scale ...Analytical chemistry is far more than titration. It's important of course but it Is often tied to expensive equipment and reagent difficult to afford/obtain by the amateur .. unfortunately. Glad to see the error mention here ! Good video sir ! Thank you!
@spudd86
@spudd86 Жыл бұрын
Error gets really fun when you have to take into account the inherent error in the floating point number system that computers actually calculate in.
@BruceNJeffAreMyFlies
@BruceNJeffAreMyFlies Жыл бұрын
Wait, I'm not the only one who actually says anal ytical? My experience was genuinely starting to look like I was the only chemist on the planet with a sense of humour!
@dimaminiailo3723
@dimaminiailo3723 11 ай бұрын
Interesting moment: both Na2C2O4 and H2O2 consume 2 e per mol, thus you could totally drop KMnO4 itself and go on the ratio of the reducing agents. Speaking about the next topic, I'd want to see the determination of brass' composition via iodometry. You can use your oxalate as the primary standard although it could be a really long way to the answer which you'd probably not like
@LubeIn
@LubeIn Жыл бұрын
Great video
@wolpumba4099
@wolpumba4099 Жыл бұрын
Here's a bullet-point summary of the video: *Titration Basics* - Explains the concept of titration, a technique to determine the concentration of a substance. - Uses potassium permanganate as a titrant to determine the concentration of hydrogen peroxide. *Methodology* - Uses a gravimetric titration method, measuring mass instead of volume. - Recommends using a scale with a 10mg resolution for better accuracy. - Preloads the reaction with 90% of the expected titrant and heats the mixture to 70°C. *Equipment* - Discusses the use of burettes in titrations but opts for a scale for better precision. - Points out that milligram scales are not suitable for larger quantities. *Trust in Chemicals* - Discusses the need to trust the purity of chemicals like sodium oxalate. - Mentions that professionals use certified primary standards. *Error Analysis* - Emphasizes the importance of understanding errors in measurements. - Explains error propagation and how errors combine in mathematical operations. kzbin.info/www/bejne/gmqXYYybad-FeJI - Discusses significant figures and how they relate to error. *Experimental Design* - Explains why 1g of primary standard is used instead of 1mg to minimize error. - Discusses the trade-off between using larger quantities for accuracy and the cost involved. *Results* - Finds the concentration of the hydrogen peroxide to be 5.1% ± 0.1%. *Conclusion* - Plans to explore other titration methods in future videos. - Thanks patrons for their support and invites viewers to suggest topics for future videos.
@gamefreak2016
@gamefreak2016 Жыл бұрын
Hey, I’ve watched your videos for ages and I often watch NileRed and it got me curious of your thoughts about him? Is he a bit reckless as a chemist or do you like what he does? (I understand if you’d rather not answer btw haha)
@ivanmartindelcampo
@ivanmartindelcampo 8 ай бұрын
Can you talk about matrix effects and how analytical chemist go about that! Maybe you can quantify how much water, fat, and salt there is in common food while describing matrix effects
@jacob127409
@jacob127409 Жыл бұрын
My previous job was an analytical chemist and let me tell you I still dealt with customers but it was mostly emails and while I was yelled at a lot less I had to explain to people what numbers meant and why I need them or why they need them. Most of them were in supply chain positions so difficult to explain to them between GC TCD and GC PDID which was not fun.
@Jkauppa
@Jkauppa Жыл бұрын
proper copper electroplating setup on top of any conductive substrate
@RaistlinMaj
@RaistlinMaj Жыл бұрын
Finally someone shared an approximation of the mass of Karen Ego's
@bangbangliu2146
@bangbangliu2146 Жыл бұрын
I think a video on iodometry would be interesting too.
@-Kerstin
@-Kerstin Жыл бұрын
Interesting to hear about this rabbit hole. Would be interesting in finding out how much you can halfass it and still get the "5.1% +-0.1%" result. Like how would you speedrun finding out the concentration of hydrogen peroxide in a random bottle
@NurdRage
@NurdRage Жыл бұрын
if you half-ass it, you might still get 5.1%, but your error could go from 0.1% to 1% or more.
@realedna
@realedna Жыл бұрын
@@NurdRage So you mean, the probability that you land on 5.1% would go down then and you are more likely to deviate from it with the error going up.
@rodneyvinen1594
@rodneyvinen1594 Жыл бұрын
Very nice video. An extension would be to test the concentrating of peracetic acid. KMnO4 reacts with H2O2 but not with peracetic acid. Idometric titration gives the amount of H2O2 and peracetic acid. Finally some mathematics gives the concentration of peracetic acid. Peracetic acid is used in the food industry and is available to the amateur.
@jolioding_2253
@jolioding_2253 11 ай бұрын
In our quant analysis lab we had to qunatitatively analyse some aluminium salt using Chinolin-8-Ol which did not really work for more than 3 people in the lab because our filters just would not dry properly and get to a constant weight even after 6 drying/exiccation cycles so maybe if you have to capabilities I'd like to see you try it.
@markywarky1234
@markywarky1234 Жыл бұрын
Could you do a relatively uninteresting but academically relevant titration? Oxidising Fe2+ to Fe3+ using acidified permanganate comes up a lot at A level / IB level, and it would create a useful academic resource. Many thanks and thanks for a great video.
@dimaminiailo3723
@dimaminiailo3723 11 ай бұрын
the titration of iron requires fluorides, I'm not sure it would be interesting in the branch of amateur chemistry
@AmdMatar94
@AmdMatar94 4 ай бұрын
thanks a lot for this work .. can you explain me please why we took the molar ratio 5/2 for H2O2 from MnO4 not the (3/2 for KMnO4) , i used oxalic acid instead, in case of KMnO4 is 0.1N so would be molality is 0.0158 mol/kg ?
@gigglysamentz2021
@gigglysamentz2021 Жыл бұрын
How do you get the density of all the solutions?
@cheeseburger118
@cheeseburger118 Жыл бұрын
Analytical was my least favourite chem class in uni but this was cool! I remember titrating VO(2+) to VO2(+) in inorganic which is also self indicating (dark blue to orange-ish if I remember correctly). It was fun trying to refer to them though since we called both of them "vee oh two plus" lol
@weldmaster80
@weldmaster80 Жыл бұрын
He lives!
@claireradke7029
@claireradke7029 Жыл бұрын
'amateur chemists like us' I'm in the wrong fucking building
@ramous5182
@ramous5182 Жыл бұрын
You always have to round up when presenting errors. And we also learned to use two significant figures of the error if they start with 1 or two. So it should be 5.07% +- 0.12% (Please correct me if I'm wrong)
@jamessshep6106
@jamessshep6106 Жыл бұрын
Is there a way to make oxalic acid from obtaining calcium oxalate from leafy plants ? Would sulfuric acid be the route used to convert from calcium oxalate to oxalic acid?
@killsalot78
@killsalot78 Жыл бұрын
8:33 lol I don't even wanna know who needs this advice
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