Je l'aime beaucoup. Merci pour cette vidéo, c'est très chouette! :)
@danieljohnson30245 күн бұрын
I wasn't expecting a hydrogen flame.
@anadosek7 күн бұрын
HNO3, HCl, acetic acid... Maybe in USA you can buy it, in EU those are drugs/explosives precursors... So still not very accessible method.
@jam_kemist39867 күн бұрын
Except from nitric acid, HCl and acetic are very accessible in stores in all of europe
@colin3517 күн бұрын
Le electrodique, tres bueno, monsoor!
@TheoNtahonvukiye7 күн бұрын
Good but your apparatus are so old ha ha haaaaa
@megamoist72307 күн бұрын
Where did you buy your powersuplie :O and is the stand from china?
@megamoist72307 күн бұрын
I'm planing on buying a Vevor megnetic stirrer like the one you have, do you recomend it?
@xjoke69818 күн бұрын
where did u get titanium mesh?
@jam_kemist39867 күн бұрын
I ordered it on AliExpress for like 2€ a piece
@xjoke69817 күн бұрын
@jam_kemist3986 could you give me the link?
@jam_kemist39866 күн бұрын
@@xjoke6981 I'm not sure if it's the exact same because price is different but proportions are the same fr.aliexpress.com/item/1005002684818617.html?spm=a2g0n.productlist.0.0.65525fbb7mIlTr&browser_id=8835a08ff0a2470ba9ad07ee80620c50&aff_trace_key=68be88028809415f8255715a86672523-1735599978795-06327-UneMJZVf&aff_platform=msite&m_page_id=sjvhmnfkbasobdgp19419d217fafd4cfa3222873e6&gclid=&pdp_npi=4%40dis%21EUR%213.30%213.29%21%21%213.36%213.35%21%40211b629217355999866618684e7888%2112000021710723327%21sea%21FR%213937507464%21X&algo_pvid=c66d7ff1-3c44-491b-baf5-92c21c318918&search_p4p_id=2024123015062614672387598230400020833795_1
@xjoke69816 күн бұрын
@jam_kemist3986 thanks
@thesciencefurry8 күн бұрын
Who the heck is Exotic Chem Lab? They don't even have videos and I saw some other channel giving then a shoudout for helping aswell xD
@jam_kemist39868 күн бұрын
He's the most based chemist ik, he's on the discord if u wanna speak to him 😎
@thesciencefurry2 күн бұрын
@@jam_kemist3986 I just realized he actually left a comment on my video quite a while ago, saying (anhydrous) ammonia is not that dangerous. And me and my friend thought, who tf is that guy to say that. WTF😅
@jam_kemist3986Күн бұрын
@@thesciencefurry I have no experience with dry NH3 but he's pretty good at chem for sure
@alexanderkroboth33108 күн бұрын
I think you should boil the undissolved remains after decantation in water and filter it, there might be some more KMnO4 that precipitated with the MnO2, because KMnO4 has only a solubility of abou 64g/L at room temperature. Then just boil the filtrate down to a smaller volume and see if any KMnO4 crystallizes when cooling it down.
@jam_kemist39868 күн бұрын
Thanks for the advice! I plan to make some again using KClO3 this time to get better yields. Idk if I'll make a video tho
@djofoxx8 күн бұрын
You should give credit to @catboychemicalsociety who's had this method up for years on KZbin. Albeit your video is easier to follow
@mohamedbelafdal63628 күн бұрын
Très intéressant! il n'a à ma connaissance aucune vidéo qui décrit la procédure comme ta vidéo. Par contre j'apprécierai beaucoup que tu plus décrives les réaction à chaque étape et les molécules parce que j'ai du mal à te suivre! (je crois comprendre que tu essaie 2 procédure différentes? mais je ne comprends pas à quelle moment tu utilises l'alternative)
@jam_kemist39868 күн бұрын
Merci beaucoup ! Il existe qu'un autre chemtuber qui l'a fait en video (et mieux que moi d'ailleurs ,c'est @neru_chan ) je suis désolé si j'ai pas été assez clair, c'est difficile de se rendre compte quand sa fait des mois qu'on est sur le projet 😂🥲 Et dcp c'est à 7:55 que je dis que le coating ATO que j'avais fait allait pas à cause du SnCl4 qui est pas pur/ pas en bonne quantité et donc je le refait mais je refait pas les autres produits parce que eux ils sont supposés bons (j'espère) En tt cas mrc pour ton com :3
@electromagic31118 күн бұрын
0:20 Sir you forgot some stuff (ion thruster, Dark Matter and one kilogram Californium.) Just boil PbO with sodium hypochlorite Your life will be much easier.
@jam_kemist39868 күн бұрын
This reaction makes PbO2 but it won't adhere properly to the electrode so it's probably useless unless I'm missing something? Anyway thanks for the comment !
@electromagic31118 күн бұрын
@@jam_kemist3986 will buddy after I saw this video I realized it easier to make nuclear weapons then PbO2 electrodes. Lol just kidding
@Moritz___9 күн бұрын
Yoo real nice Still struggling to get my chlorate cell to work though... Seems to be my computer cable that shuts off above 3A so gonna get a proper powersupplie. What is yours called? Just found the big ones with 30V5A
@jam_kemist39868 күн бұрын
I don't remember the name but I know you can probably find it on amazon, the prices have increased a lot tho since I bought it, it's prolly 50-60€ now Gl to you !
@Farben-X9 күн бұрын
finally, good job waiting for the perchlorate
@jam_kemist39869 күн бұрын
@@Farben-X thanks !
@Salt_and_Peroxide9 күн бұрын
lets goo mr jam
@jam_kemist39869 күн бұрын
@@Salt_and_Peroxide yessirrr
@Mohannova9 күн бұрын
Hello sir, past days I'm watching your videos it's really awesome 👍🏻, lots of love from India Keep rocking 🎉
@jam_kemist39869 күн бұрын
@@Mohannova thanks a lot !
@Tyresio129 күн бұрын
Generating in situ HF in a glass vessel and hoping it will not be used up in side reactions... Quite an optimist, aren't you ;)
@jam_kemist39869 күн бұрын
It's only there as a catalyst so I'm not worried at all since it's all gonna react with the titanium and not the glass 👍
@mathh52249 күн бұрын
Comment t'arrives a avoir du h2o2 aussi concentré en france ?? J'en trouve mais jamais autant concentré 😢
@jam_kemist39869 күн бұрын
@@mathh5224 tu peux plus mtn, c'était donné avec une piscine enterrée que mes parents avaient acheté y'a 10 ans
@ScrapScience9 күн бұрын
Really nice! While I'm not a fan of working with lead myself, it's really good to see someone make a proper lead dioxide electrode that's not just anodising lead metal (which of course, is a disaster of an electrode). Good luck for the perchlorate cell!
@jam_kemist39869 күн бұрын
@@ScrapScience thanks a lot ! I really like your videos too
@kerimkstati9 күн бұрын
MMO cheap, even on amazon the сhinese make them on an industrial scale for chlorinating water, I bought real good ones on Aliexpress, and on Amazon for $50 10x10cm size
@jam_kemist39869 күн бұрын
@@kerimkstati yes I have one too but it only makes chlorates and not perchlorates hehe
@kerimkstati9 күн бұрын
@@jam_kemist3986 Why can't perchlorates be obtained?
@jam_kemist39869 күн бұрын
@@kerimkstati well unless your mmo is the very rare kind made of platinum group metal oxides it just can't produce the ClO4- ion
@kerimkstati9 күн бұрын
@jam_kemist3986 are there other types of mmo electrodes? I have one like this, and I haven't heard of any other options, I know there are some with manganese oxide, but I don't think they are as good, I think like lead oxide
@mohamedbelafdal63628 күн бұрын
@@kerimkstati there are many types of MMO, I know the most common is Ru-Ir but there's also tantalum and maybe platinum. regardless, they still "classified" as MMO meaning they function similarly to the classic Ru-Ir MMO anodes with few tweaks here and there...
@isabutchers55919 күн бұрын
is it possible to just use a sheet of lead metal as an anode and run a very low current through it in sulphuric acid?
@jam_kemist39869 күн бұрын
@@isabutchers5591 it will make PbO2 yes, but idk if it holds well because it doesn't have the intermediate coating. I've heard tho that's it's possible to use big strips of Pb metal as electrodes for chlorate to perchlorate and even if it gets destroyed, it also makes PbO2 on the anode and so the perchlorate can be formed but they don't last very long. Try and research on Sciencemadness forum if you want more information;)
@synth10029 күн бұрын
Yea Cerium..you can obtain it in every hardware store...
@jam_kemist39869 күн бұрын
@@synth1002 still better then antimony lol
@zenongranatnik83706 күн бұрын
You can literally buy it in hardware stores, CeO2 is often sold as a window polishing powder
@Leucine759 күн бұрын
Nice man
@jam_kemist39869 күн бұрын
Thanks ;)
@Uncharted_Escapes099 күн бұрын
Dont car batteries have both lead and lead dioxide electrodes in them? Cant they be used for perchlorate synthesys? Or am i missing a,detail
@jam_kemist39869 күн бұрын
They do have PbO2 in a Pb frame but they are not hard coated PbO2 and will fall out very quickly so u can't make anything with them. You could recycle the Pb to plate tho
@Uncharted_Escapes099 күн бұрын
@jam_kemist3986 thanks for explaining
@AwdeInho9 күн бұрын
Chlorate still dominates perchlorate in my opinion, i mean who doesn’t love a whiff of medicinal chlorine dioxide or doesn’t like the radioactive yellow colour of chloric acid?? (no seriously never breathe in chlorine dioxide pls)
@jam_kemist39869 күн бұрын
They are more funny imo but perchlorate are the more formel ones because stronger and safer
@AwdeInho9 күн бұрын
@ I mean they both have their pros and cons, perchlorate is more oxygen rich but chlorate needs lower activation energies (less stable since stability of chlorine oxide ions increases the more oxygen you add for some reason), my brain thinks that if smth doesn’t react immediately with concentrated sulfuric acid, it’s not powerful, so it thinks its a bad oxidizer since it’s very stable, but that’s just me
@PyroRob699 күн бұрын
Where are you? France?
@jam_kemist39869 күн бұрын
Yessir 🇫🇷
@FredericoMirandaBrandaoAlves9 күн бұрын
Thanks for the demonstration. It contains many useful chemical reactions and I've seen Cerium being mentioned in many redox reactions and I'm glad to see it's affordable.
@jam_kemist39869 күн бұрын
With pleasure ;)
@FredericoMirandaBrandaoAlves11 күн бұрын
This video is the useful one when it comes to addressing the query "how to make benzene". It does not make sense to make something so low-cost (going for less than a thousand dollars for every teragram of it) from an expensive starting material. Sadly it did not pop-up immediately at my first query search, but the algorithm eventually figured it out that this is the correct one for "how to make benzene".
@trinitro596813 күн бұрын
Question is there still some sodium chlorate contamination? Flame looks rather orange to yellow, instead of the usual potassium based flame.
@jam_kemist398613 күн бұрын
Yes there is indeed some. If u want pure KClO3 for pyrotechnics for exemple you need to électrolyse KCl directly instead of NaClO3
@trinitro596813 күн бұрын
@jam_kemist3986 right on! Thanks for the video!
@terra-ants152515 күн бұрын
W ostatnim czasie też rozważałem czy taki nikiel będzie aktywny w reakcji uwodornienia. Eksperymentuje z niklem otrzymanym w wyniku reakcji NiCl2 + Al, rozkładu szczawianu i zawiesiną która powstaje na skutek reakcji NaBH4 z NiCl2.
@terra-ants152515 күн бұрын
Szukam też odpowiedniej metody produkcji H2 in situ i rozkład mrowczanu amonu wydaje się być ciekawy.
@AwdeInho19 күн бұрын
It looks like there is some sodium impurity from the orange flame at the end, you could start with KCl, then boil it to decompose the hypochlorite, then add more water until all of it dissolves at room temperature (or maybe around 30-40c), then filter it to remove all insoluble particles, after that, boil the water again until you reach your starting volume of solution, or even less if you don’t have a lot of chloride left in solution (you can check with the density of the solution or if your voltage starts to rise and your current drops), after that, let it cool in the freezer at 0c (im pretty sure it will not freeze because the kcl lowers its melting point by quite a bit but it really depends on the concentration of chloride and temperature of your freezer) and thats it! No sodium contamination at all!
@jam_kemist398619 күн бұрын
@@AwdeInho yeah I figured, but I don't really mind because I don't need it pure anyway 🤷 thanks for the comment !