Crystallites (grain) size from XRD data using Scherrer equation - 09

Reference paper:
www.sciencedirect.com/science...
In this video, I have shown the method for the calculation of crystallite (grain) size from XRD using the Scherrer equation. For more videos, Please subscribe to NanoWorld. If you have any questions, feel free to ask me in the comment section below.
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Music Source
Unconditionally by Broken Elegance 🎩 / brokenelegance Creative Commons - Attribution 3.0 Unported - CC BY 3.0 creativecommons.org/licenses/b... Music promoted by Audio Library • Unconditionally - Brok...

[@evaristosalaya5111]

Thank you so much. Excellent video, easy to follow and well-explained.

[@sennali7634]

Written in a very detailed! Thank you so much!!

[@From_Crowd_to_Nation]

Very good sir 👍 Nice effort I was using origion+Excel but followed long procedure , you made a good effort and short path to find FWHM and average crystallite size I appreciate you

[@yu-kaiwu7323]

Thank you so much, it's really helpful!

[@9715256854]

Your video was helpful to calculate the crystalline size. Thank You.

[@techanddesignnikhil]

thank you so much for your really well explained video.

[@SaidAZ-pf2zo]

Thank you very much, Really It was very well explained, With image and music

[@joharamin3640]

Thank you so much. A simple question, what are the parameters used for the fitting until converged. I got the COD(R^2) less than 0.5 and the fitting graph is so far of the beaks. I hope you all the best thank you.

[@sanjeevkumarnitrourkela6637]

thank you sir....excellent explanation...for beginers

[@tiffanyk5259]

So informative! Thanks a lot!

[@shahinaawan7338]

Thank you so much, its very helpful. Thanks alot

[@naas1634]

How to decide the y-scale when selecting the peaks? If I try different heights of the peaks while selecting them, the value turns out different.

[@ayuulss7011]

thank you sir....excellent explanation...

[@meriembouhbou6992]

Thank you so much, very useful ==> Great Job (y)

[@vv-ky4bi]

fantastic man...hatsoff u...

[@gauravjamwal8095]

Can you please show the strain and crystallite size from Williamson hall methods for uniform deformation model? Thanks.

[@malihaparvin4224]

appreciate your work. really helpful :)

[@nanoworld6122]

Thank you

[@dr.m.bhuvaneshwaran6904]

Thank you so much sir, its very helpful. Thanks a lot

[@tsungomm1914]

Thank you so much... Made my day

[@cuonglevan134]

Thank you for sharing, this really helpful, Respect !!

[@nanoworld6122]

Glad it was helpful!

[@Josimar.quimico]

Thank you!

[@runfatan7086]

谢谢，非常有用！

[@saghar_ghasemi]

Thank you very much for the helpful tutorial. May I know if we can consider this size as the nanocrystals size of our structure? In fact is there a difference between the crystallite size and particle size?

[@bruceliu9436]

sure, you could call this one domain size, which would be better differntiated from the particle size in terms of names.

[@vadelrionneskara4623]

Thank you. Your video helped me prove D value in today’s mid term exam. It was 30 marks.

[@nanoworld6122]

All the best

[@ranjithvia]

Very useful one sir. thank you

[@magicalphysics9038]

Really nice, one small suggestion if u take this tutorial along with a clear oral explanation of yours it wil be more effective. Congratulations for such upcoming videos... Good luck👍

[@user-wx1mx6ki9p]

thank you so much for your really well-explained video @@@!!!

[@nanoworld6122]

Glad it was helpful!

[@dr.poojashandilya6885]

Your video is so helpful, I really want to appreciate your efforts...thanks alot.....

[@nanoworld6122]

Glad to hear that

[@samikchagurung6359]

How do I do the same in origin 6? There is no Peak and Baseline option available

[@ericzhao2687]

Thanks a lot. It is useful

[@lifesciences3889]

Helpful video.... thank you sir

[@nihelruiz3343]

thank you my friend

[@imyemouna9664]

I am very happy when i watch the video 😁

[@lalitarai9958]

thank you so much, it was very helpful. can you plz upload videos about DSC.

[@cigdemdikbas4573]

Thank you very much👏

[@shrinathghadge854]

Very informative!! Can you please show the Rietveld refinement for calculation of atomic occupancy? Thanks.

[@baoyuzhou7539]

真的很有用，特别是对于新手来说。

[@nanoworld6122]

谢谢

[@linshinat148]

Thank You so much

[@aliyayousaf8383]

thank u so much for such a helpful video.

[@nanoworld6122]

My pleasure 😊

[@TheBAbert]

Thank you! Excellent Video!! I only have some doubts. In my X-ray diffraction pattern appear 2 different TiO2 phases (anatse and rutile), 1.- Can I use this method if I want to measure just the anatase peaks? 2.- Do the rutile peaks affects this measurements?. 3.- Would it be valid if I select anatase and rutile peaks and calculate an average crystallite size for both phases?. Regards!!

[@AMVCreativity]

I found myself in a similar position but for an ferrous alloy lol. What did u do?

[@dontseewhatyouwannasee3658]

thank you.

[@prg2457]

Habibi...classic job

[@vishwajeet1211]

Thank you for making such a great work, I'm not getting precise Values of crystal size , they differ very large from each other so average is very much different, please guide 🙏🙏🙏

[@innayk]

Thank you

[@vv-ky4bi]

Sir how can we measure the phase present in the NaOH treated natural fiber?? Or how can we analyse the natural fiber?

[@thanhle-tr1ys]

Hey, thank you verry much

[@erikatallyta4796]

Very good. Super easy to reproduce. Thank you.

[@nanoworld6122]

Glad it helped!

[@abdullahiadamu7688]

Hi.. thank you for the knowledge you've been sharing with us. Please I couldn't analyse my xrd data using Origin. The graph doesn’t converge. It shows that mutual dependency exists between parameters. What is the solution please?

[@manjupriya6574]

I Had the same issue, when i zoomed the peaks and aligned the peak fit to the narrow line of the peak after some trials my graph converged.

[@ichahalwa8754]

i have poject witch i should use this logicial can you help me how i used for the begining how i importe cif file and how i used XRD please

[@AbuIyaadAF]

Very much beneficial

[@AnotherPlanet12]

You are fitting a Gauss for a Lorentzian function?

[@aouaffanoufal9726]

Thank you do much great work

[@nanoworld6122]

You are very welcome

[@idarssy]

Thankyou, for this great video, this so help me a lot ☀ thxx

[@nanoworld6122]

You’re welcome 😊

[@idarssy]

@@nanoworld6122 thankyou again, because i can pass my exam last week 😄😝

[@atanughosh8312]

Can you upload videos on XPS spectra , nanowire I-V characterization etc.

[@CrazyPhysics1]

for your reference you can refer kzbin.info/www/bejne/l2HQYa2ZepqebLc

[@ideasbyNTR]

When you collected peak position and FWHM values either it's 5 peaks on same plot, or same should be conducted for 5 samples separately?? Or 5/8 peaks from the single peak of any sample would be enough?

[@NoorMohmed-ty6ty]

thanks a lot

[@muhammadsaqib9392]

great job sir

[@muhammadumair9214]

hello Muhammad saqib? hope youll be fine, dear i have one thing to discus do you know how to calculate the miller indices through any way?

[@sagarrawal8332]

How to find the corresponding value of y axix acrroding to peak position i.e x value?

[@trialunlock8706]

For converting angle theta to radian while determining the crystallite size from powder xrd spectrum why we are taking half circumference not full

[@alihasnain6204]

in data 2theta value is given so we need the value of theta so we divide the value of 2theta with 2, to get the value of theta so that we can put value of theta in scherrer formula

[@dahcari6548]

Hi NanoWorld, I have question about size of material in video, I calculate size of material using Scherrer equation same in video but why 1/ My result after calculate in excel (the raw material has lower size than the material after treatment with H2SO4)- in my experiments H2SO4 will reduce size of material. I hope I would receive your answer soon. Thanks NanoWorld so much.

[@zahrasharifi8611]

Thank you for your very helping video. Would you mind filming how to draw W-H plot?

[@heryantobinhaeruddin2382]

kzbin.info/www/bejne/eZnQfmaFfcyWrMk

[@helpinghands5493]

Very nicely explained👍

[@nanoworld6122]

Thanks for liking

[@lizatanggw2967]

Salute you!

[@deepkumar92]

thanks bro

[@magicofscience8899]

EXCELLANT👍👍👍

[@muhammedmusharaf7966]

Thank you

[@navinvijeyraj7713]

bro can you explain sin2psi technique for residual stress calculation of metal

[@rafiqshaheen1158]

Its soo helpful for my exam preparation

[@nanoworld6122]

Glad to hear that

[@HelenL93]

is there a way to do this in an exam without using software? just estimate the particle size from the PXRD pattern? i have been given this as a past paper question

[@ZaratustraCoDM]

Thankyou very much :)

[@nanoworld6122]

Welcome!

[@varshinipreethi3189]

Sir this video is very useful. I prepared my sample by synthesis a zinc oxide nanoparticle but when I put my result in xpert highscore it shows copper and silicon oxide

[@joseluisxochihuajuan7586]

Excellent video... I wanted to request the help to estimate the size of the TiO2 crystallite according to my XRD analysis. I have a problem, in the software of origin that I have installed, the commands do not appear.

[@muhammadumair9214]

download the latest version of the software, i hope this will help you.

[@SauravKumar2]

hi.. can you help me in XRD analysis

[@prasannahemz]

Thanks again, help me in calculating lattice constant.....

[@nanoworld6122]

I'll upload a video soon.

[@mdmazbahuddin5592]

Which method among DSC and XRD do you think would be more accurate for % crystallinity estimates and why? Do you think crystallinity depends on the crystal size? please explain a bit of detail. I have just begun studying, thnks

[@thiagorsvful]

No, crystallinity depends upon the intensity of the peaks and the lower the noises in the graph

[@jasminm9165]

can you show how langevin fit done in origin using VSM data

[@hema2503]

How to identify /remove FTO peaks from spectra, plz help

[@alanch2660]

I have a question in the Scherrer equation the value of theta, Is not necessary divide for two? Thank you for your good video.

[@nanoworld6122]

It is essential, you must divide it by 2.

[@MelomaniacEarth]

Which software?

[@sharinmariathomas3718]

thank you

[@nanoworld6122]

Welcome!

[@gabrielamendoza8016]

Hello, for FWHM the peak 2 I always get 2. something in comparison with other peaks. I must say, in the graph the second peak is very close to the first one that the connection does not touch the base line.

[@juttwaryah..pindaywalyjutt5958]

Which software you used

[@manuja6889]

Very helpful video Sir I followed the same method but I am not getting multiple peak values . I am getting only one FWHM value. Please answer me

[@nanoworld6122]

Your data might need a baseline correction. But I'm not sure yet, because I have not seen it yet. If you want me to have a look over your data, then send it to me at thenanoworld.com/contact-us/

[@user-xx5pq8hg3k]

Thank you for good video. But, I have a wondering that about your data that you had used. Is it raw data or normalised data?? If it were normalized, then I want to know what was the normallization process. Please tell me...

[@bhulidhaker8745]

PLEASE EXPLAIN ALL TYPE OF ERROR IN XRD

[@amanbayad17]

How to select Multiple peaks ?

[@satishbarhate4790]

Which crystal you used?

[@nanoworld6122]

ZnO

[@aamirahmed8389]

Can you plz tell me how to get the JCPDS file for a material.

[@nanoworld6122]

Send me an email, and tell me your required card no. like 01-023-0456 etc..

[@darshanameena9776]

Sir please tell me that which method is best for finding crystalline size modified scherrer or W-H plot.

[@nanoworld6122]

W-H plot is the best method

[@darshanameena9776]

@@nanoworld6122 why?

[@echuen4149]

Thank you very much for this... I have a question: when you select the peaks, i noticed that the y value is changing depending on where you click on the graph (the y value doesn't correspond to the x value in the curve)...do we need to make sure we click on the correct y value on the graph? or do we just care about the peak position(x value?)

[@guerfisouad7837]

Please help I cannot designate the vertices for each pik with a straight line. Whenever I designate a peak, it reads the values of x and y, but it does not draw a pik.

[@listyamaulita5977]

Can anyone know where i can get origin?

[@abdellahrahmani]

can you give the scientific interpretation of this graph ??

[@muhsinkhan2431]

how u are selecting c[y] and A[X].

[@nanoworld6122]

Keep pressing the control button in your keyboard

[@user-ry8rv7li6n]

사랑해요

[@nanoworld6122]

Thank you.

[@belisariomartin3876]

excuse me, shouldn't FWHM be in 2Theta units too?

[@kharoumdairies]

appreciate it nice video..but music is irritating.

[@rabiulislam3448]

what should be the unit of the calculated crystallite size? i think its not nm,it should be Angstrom

[@Mixvideos1941]

thankssssssssssssssssss